Development of a new certified reference material of tinidazole for quality and safety of agro-products
s Two independent approaches involving mass balance (MB) method and quantitative nuclear magnetic resonance (qNMR) technique were employed to measure the purity of a new certified reference material (CRM) of tinidazole. The mass fraction of pure tinidazole CRM was assigned to be 99.7 % with an expan...
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| Veröffentlicht in: | Accreditation and quality assurance 2016-10, Vol.21 (5), p.341-349 |
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| container_title | Accreditation and quality assurance |
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| creator | Yang, Mengrui Wang, Min Zhou, Jian Song, Yinqing Wang, Tongtong |
| description | s
Two independent approaches involving mass balance (MB) method and quantitative nuclear magnetic resonance (qNMR) technique were employed to measure the purity of a new certified reference material (CRM) of tinidazole. The mass fraction of pure tinidazole CRM was assigned to be 99.7 % with an expanded uncertainty of 0.6 % (
k
= 2). Sample preparation, qualitative analysis, certifying methods optimization, characterization, homogeneity testing, stability monitoring, and uncertainty evaluation were systemically and comprehensively studied in development of tinidazole CRM. The results indicate that the CRM is homogenous and stable at 4 °C for at least 6 months which satisfy the requirements of CRM. The new CRM (GBW(E)090756) can be applicable to instrument calibration and analytical method validation, especially for assurance of accuracy result of tinidazole determination in the program of nationwide routine monitoring and risk assessment for agro-products by Ministry of Agriculture (MOA) in China. |
| doi_str_mv | 10.1007/s00769-016-1221-0 |
| format | Article |
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Two independent approaches involving mass balance (MB) method and quantitative nuclear magnetic resonance (qNMR) technique were employed to measure the purity of a new certified reference material (CRM) of tinidazole. The mass fraction of pure tinidazole CRM was assigned to be 99.7 % with an expanded uncertainty of 0.6 % (
k
= 2). Sample preparation, qualitative analysis, certifying methods optimization, characterization, homogeneity testing, stability monitoring, and uncertainty evaluation were systemically and comprehensively studied in development of tinidazole CRM. The results indicate that the CRM is homogenous and stable at 4 °C for at least 6 months which satisfy the requirements of CRM. The new CRM (GBW(E)090756) can be applicable to instrument calibration and analytical method validation, especially for assurance of accuracy result of tinidazole determination in the program of nationwide routine monitoring and risk assessment for agro-products by Ministry of Agriculture (MOA) in China.</description><identifier>ISSN: 0949-1775</identifier><identifier>EISSN: 1432-0517</identifier><identifier>DOI: 10.1007/s00769-016-1221-0</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Analytical Chemistry ; Biochemistry ; Chemistry ; Chemistry and Materials Science ; Chromatography ; Commercial Law ; Ecotoxicology ; Food Science ; Homogeneity ; Marketing ; Mass balance ; Monitoring ; NMR ; Nuclear magnetic resonance ; Nuclear safety ; Practitioner's Report ; Product safety ; Qualitative analysis ; Reference materials ; Risk assessment ; Sensors ; Stability analysis ; Uncertainty ; Variance analysis ; VOCs ; Volatile organic compounds</subject><ispartof>Accreditation and quality assurance, 2016-10, Vol.21 (5), p.341-349</ispartof><rights>Springer-Verlag Berlin Heidelberg 2016</rights><rights>Springer-Verlag Berlin Heidelberg 2016.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-25d64e4dd6560bf9f384c002828e8b5322dcaa074bf7dedf4da1bbea854ddb463</citedby><cites>FETCH-LOGICAL-c316t-25d64e4dd6560bf9f384c002828e8b5322dcaa074bf7dedf4da1bbea854ddb463</cites><orcidid>0000-0002-0973-2748</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00769-016-1221-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2917929783?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21388,21389,27924,27925,33530,33744,41488,42557,43659,43805,51319,64385,64389,72469</link.rule.ids></links><search><creatorcontrib>Yang, Mengrui</creatorcontrib><creatorcontrib>Wang, Min</creatorcontrib><creatorcontrib>Zhou, Jian</creatorcontrib><creatorcontrib>Song, Yinqing</creatorcontrib><creatorcontrib>Wang, Tongtong</creatorcontrib><title>Development of a new certified reference material of tinidazole for quality and safety of agro-products</title><title>Accreditation and quality assurance</title><addtitle>Accred Qual Assur</addtitle><description>s
Two independent approaches involving mass balance (MB) method and quantitative nuclear magnetic resonance (qNMR) technique were employed to measure the purity of a new certified reference material (CRM) of tinidazole. The mass fraction of pure tinidazole CRM was assigned to be 99.7 % with an expanded uncertainty of 0.6 % (
k
= 2). Sample preparation, qualitative analysis, certifying methods optimization, characterization, homogeneity testing, stability monitoring, and uncertainty evaluation were systemically and comprehensively studied in development of tinidazole CRM. The results indicate that the CRM is homogenous and stable at 4 °C for at least 6 months which satisfy the requirements of CRM. The new CRM (GBW(E)090756) can be applicable to instrument calibration and analytical method validation, especially for assurance of accuracy result of tinidazole determination in the program of nationwide routine monitoring and risk assessment for agro-products by Ministry of Agriculture (MOA) in China.</description><subject>Analytical Chemistry</subject><subject>Biochemistry</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Commercial Law</subject><subject>Ecotoxicology</subject><subject>Food Science</subject><subject>Homogeneity</subject><subject>Marketing</subject><subject>Mass balance</subject><subject>Monitoring</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Nuclear safety</subject><subject>Practitioner's Report</subject><subject>Product safety</subject><subject>Qualitative analysis</subject><subject>Reference materials</subject><subject>Risk assessment</subject><subject>Sensors</subject><subject>Stability analysis</subject><subject>Uncertainty</subject><subject>Variance analysis</subject><subject>VOCs</subject><subject>Volatile organic compounds</subject><issn>0949-1775</issn><issn>1432-0517</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kEtPwzAQhC0EEqXwA7hZ4mzwK3FyROUpVeICZ8uJ11WqNG5tB1R-PY6CxInL7h6-mdEOQteM3jJK1V3Mo6wJZSVhnDNCT9CCScEJLZg6RQtay5owpYpzdBHjllJWVEws0OYBPqH3-x0MCXuHDR7gC7cQUuc6sDiAgwBDC3hnEoTO9BOVuqGz5tv3gJ0P-DCavktHbAaLo3GQz8lqEzzZB2_HNsVLdOZMH-Hqdy_Rx9Pj--qFrN-eX1f3a9IKVibCC1tKkNaWRUkbVztRyZZSXvEKqqYQnNvWGKpk45QF66Q1rGnAVEXWNLIUS3Qz--bgwwgx6a0fw5AjNa-ZqnmtKpEpNlNt8DHmH_U-dDsTjppRPfWp5z517lNPfWqaNXzWxMwOGwh_zv-LfgAGunnx</recordid><startdate>20161001</startdate><enddate>20161001</enddate><creator>Yang, Mengrui</creator><creator>Wang, Min</creator><creator>Zhou, Jian</creator><creator>Song, Yinqing</creator><creator>Wang, Tongtong</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7XB</scope><scope>88C</scope><scope>8FE</scope><scope>8FG</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>M0T</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><orcidid>https://orcid.org/0000-0002-0973-2748</orcidid></search><sort><creationdate>20161001</creationdate><title>Development of a new certified reference material of tinidazole for quality and safety of agro-products</title><author>Yang, Mengrui ; Wang, Min ; Zhou, Jian ; Song, Yinqing ; Wang, Tongtong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-25d64e4dd6560bf9f384c002828e8b5322dcaa074bf7dedf4da1bbea854ddb463</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Analytical Chemistry</topic><topic>Biochemistry</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Commercial Law</topic><topic>Ecotoxicology</topic><topic>Food Science</topic><topic>Homogeneity</topic><topic>Marketing</topic><topic>Mass balance</topic><topic>Monitoring</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Nuclear safety</topic><topic>Practitioner's Report</topic><topic>Product safety</topic><topic>Qualitative analysis</topic><topic>Reference materials</topic><topic>Risk assessment</topic><topic>Sensors</topic><topic>Stability analysis</topic><topic>Uncertainty</topic><topic>Variance analysis</topic><topic>VOCs</topic><topic>Volatile organic compounds</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Mengrui</creatorcontrib><creatorcontrib>Wang, Min</creatorcontrib><creatorcontrib>Zhou, Jian</creatorcontrib><creatorcontrib>Song, Yinqing</creatorcontrib><creatorcontrib>Wang, Tongtong</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Healthcare Administration Database (Alumni)</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Healthcare Administration Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><jtitle>Accreditation and quality assurance</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Mengrui</au><au>Wang, Min</au><au>Zhou, Jian</au><au>Song, Yinqing</au><au>Wang, Tongtong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development of a new certified reference material of tinidazole for quality and safety of agro-products</atitle><jtitle>Accreditation and quality assurance</jtitle><stitle>Accred Qual Assur</stitle><date>2016-10-01</date><risdate>2016</risdate><volume>21</volume><issue>5</issue><spage>341</spage><epage>349</epage><pages>341-349</pages><issn>0949-1775</issn><eissn>1432-0517</eissn><abstract>s
Two independent approaches involving mass balance (MB) method and quantitative nuclear magnetic resonance (qNMR) technique were employed to measure the purity of a new certified reference material (CRM) of tinidazole. The mass fraction of pure tinidazole CRM was assigned to be 99.7 % with an expanded uncertainty of 0.6 % (
k
= 2). Sample preparation, qualitative analysis, certifying methods optimization, characterization, homogeneity testing, stability monitoring, and uncertainty evaluation were systemically and comprehensively studied in development of tinidazole CRM. The results indicate that the CRM is homogenous and stable at 4 °C for at least 6 months which satisfy the requirements of CRM. The new CRM (GBW(E)090756) can be applicable to instrument calibration and analytical method validation, especially for assurance of accuracy result of tinidazole determination in the program of nationwide routine monitoring and risk assessment for agro-products by Ministry of Agriculture (MOA) in China.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s00769-016-1221-0</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0002-0973-2748</orcidid></addata></record> |
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| subjects | Analytical Chemistry Biochemistry Chemistry Chemistry and Materials Science Chromatography Commercial Law Ecotoxicology Food Science Homogeneity Marketing Mass balance Monitoring NMR Nuclear magnetic resonance Nuclear safety Practitioner's Report Product safety Qualitative analysis Reference materials Risk assessment Sensors Stability analysis Uncertainty Variance analysis VOCs Volatile organic compounds |
| title | Development of a new certified reference material of tinidazole for quality and safety of agro-products |
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