Synthesis and properties of UV-curable hyperbranched polyurethane acrylate oligomers containing photoinitiator
The hyperbranched polyurethane acrylate oligomers containing photoinitiator were synthesized by modifying the second-generation hyperbranched poly(amine-ester) with isophorone diisocyanate-2-hydroxyethylacrylate and isophorone diisocyanate-2-hydroxy-2-methylpropiophenone at different feed ratio. The...
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| Veröffentlicht in: | Polymer bulletin (Berlin, Germany) Germany), 2012-02, Vol.68 (3), p.729-743 |
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| container_title | Polymer bulletin (Berlin, Germany) |
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| creator | Han, Wensong Lin, Baoping Zhou, Yidan Song, Jiangang |
| description | The hyperbranched polyurethane acrylate oligomers containing photoinitiator were synthesized by modifying the second-generation hyperbranched poly(amine-ester) with isophorone diisocyanate-2-hydroxyethylacrylate and isophorone diisocyanate-2-hydroxy-2-methylpropiophenone at different feed ratio. The elemental analysis, FT-IR and NMR methods are used for structural characterization, molecular weights, and polydispersities, photosensitive groups and thermal properties of the oligomers were analyzed by gel permeation chromatography, UV–Vis spectra and thermogravimetric analysis, respectively. UV-curing properties were characterized by FT-IR at different curing time. In addition, the solubilities of the oligomers were also examined. |
| doi_str_mv | 10.1007/s00289-011-0576-y |
| format | Article |
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The elemental analysis, FT-IR and NMR methods are used for structural characterization, molecular weights, and polydispersities, photosensitive groups and thermal properties of the oligomers were analyzed by gel permeation chromatography, UV–Vis spectra and thermogravimetric analysis, respectively. UV-curing properties were characterized by FT-IR at different curing time. 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Bull</addtitle><description>The hyperbranched polyurethane acrylate oligomers containing photoinitiator were synthesized by modifying the second-generation hyperbranched poly(amine-ester) with isophorone diisocyanate-2-hydroxyethylacrylate and isophorone diisocyanate-2-hydroxy-2-methylpropiophenone at different feed ratio. The elemental analysis, FT-IR and NMR methods are used for structural characterization, molecular weights, and polydispersities, photosensitive groups and thermal properties of the oligomers were analyzed by gel permeation chromatography, UV–Vis spectra and thermogravimetric analysis, respectively. UV-curing properties were characterized by FT-IR at different curing time. In addition, the solubilities of the oligomers were also examined.</description><subject>Applied sciences</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical analysis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Complex Fluids and Microfluidics</subject><subject>Curing</subject><subject>Diisocyanates</subject><subject>Energy consumption</subject><subject>Exact sciences and technology</subject><subject>Gel chromatography</subject><subject>Hydrocarbons</subject><subject>Molecular weight</subject><subject>Nitrogen</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Oligomers</subject><subject>Organic Chemistry</subject><subject>Organic polymers</subject><subject>Original Paper</subject><subject>Photoinitiators</subject><subject>Photosensitivity</subject><subject>Physical Chemistry</subject><subject>Physicochemistry of polymers</subject><subject>Polycondensation</subject><subject>Polymer Sciences</subject><subject>Polymerization</subject><subject>Polyurethane resins</subject><subject>Preparation, kinetics, thermodynamics, mechanism and catalysts</subject><subject>Reagents</subject><subject>Soft and Granular Matter</subject><subject>Structural analysis</subject><subject>Thermodynamic properties</subject><subject>Thermogravimetric analysis</subject><subject>Ultraviolet radiation</subject><issn>0170-0839</issn><issn>1436-2449</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kElPBCEQhYnRxHH5Ad5IjEeUohfgaIxbYuLB5Upopnq6TQsjMIf-9zIZoydPUMWrV4-PkDPgl8C5vEqcC6UZB2C8kS2b98gC6qploq71PllwkJxxVelDcpTSBy9128KC-JfZ5wHTmKj1S7qOYY0xj5ho6OnbO3ObaLsJ6TCXfhetdwMWWZjmTcQ8WI_UujhPNiMN07gKnxgTdcFnO_rRr-h6CDmUax5tDvGEHPR2Snj6cx6Tt7vb15sH9vR8_3hz_cRcVbeZoeJNp3pYQqfQ6s4trdZCSdHrrpTYy7pTGhxUurXoliAaLbR0veS1UJ2ojsn5zrd86GuDKZuPsIm-rDRCgyxOjW6KCnYqF0NKEXuzjuOnjbMBbrZYzQ6rKVjNFquZy8zFj7NNzk79FsmYfgdF00gAtU0gdrpUnvwK41-C_82_ASz8i2A</recordid><startdate>20120201</startdate><enddate>20120201</enddate><creator>Han, Wensong</creator><creator>Lin, Baoping</creator><creator>Zhou, Yidan</creator><creator>Song, Jiangang</creator><general>Springer-Verlag</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope></search><sort><creationdate>20120201</creationdate><title>Synthesis and properties of UV-curable hyperbranched polyurethane acrylate oligomers containing photoinitiator</title><author>Han, Wensong ; Lin, Baoping ; Zhou, Yidan ; Song, Jiangang</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c346t-e805b8f1d1b8ea9bcda992872f9ba9bef74b891c1396aecd1259297cf70428b23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Applied sciences</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical analysis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Complex Fluids and Microfluidics</topic><topic>Curing</topic><topic>Diisocyanates</topic><topic>Energy consumption</topic><topic>Exact sciences and technology</topic><topic>Gel chromatography</topic><topic>Hydrocarbons</topic><topic>Molecular weight</topic><topic>Nitrogen</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Oligomers</topic><topic>Organic Chemistry</topic><topic>Organic polymers</topic><topic>Original Paper</topic><topic>Photoinitiators</topic><topic>Photosensitivity</topic><topic>Physical Chemistry</topic><topic>Physicochemistry of polymers</topic><topic>Polycondensation</topic><topic>Polymer Sciences</topic><topic>Polymerization</topic><topic>Polyurethane resins</topic><topic>Preparation, kinetics, thermodynamics, mechanism and catalysts</topic><topic>Reagents</topic><topic>Soft and Granular Matter</topic><topic>Structural analysis</topic><topic>Thermodynamic properties</topic><topic>Thermogravimetric analysis</topic><topic>Ultraviolet radiation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Han, Wensong</creatorcontrib><creatorcontrib>Lin, Baoping</creatorcontrib><creatorcontrib>Zhou, Yidan</creatorcontrib><creatorcontrib>Song, Jiangang</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><jtitle>Polymer bulletin (Berlin, Germany)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Han, Wensong</au><au>Lin, Baoping</au><au>Zhou, Yidan</au><au>Song, Jiangang</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and properties of UV-curable hyperbranched polyurethane acrylate oligomers containing photoinitiator</atitle><jtitle>Polymer bulletin (Berlin, Germany)</jtitle><stitle>Polym. Bull</stitle><date>2012-02-01</date><risdate>2012</risdate><volume>68</volume><issue>3</issue><spage>729</spage><epage>743</epage><pages>729-743</pages><issn>0170-0839</issn><eissn>1436-2449</eissn><coden>POBUDR</coden><abstract>The hyperbranched polyurethane acrylate oligomers containing photoinitiator were synthesized by modifying the second-generation hyperbranched poly(amine-ester) with isophorone diisocyanate-2-hydroxyethylacrylate and isophorone diisocyanate-2-hydroxy-2-methylpropiophenone at different feed ratio. The elemental analysis, FT-IR and NMR methods are used for structural characterization, molecular weights, and polydispersities, photosensitive groups and thermal properties of the oligomers were analyzed by gel permeation chromatography, UV–Vis spectra and thermogravimetric analysis, respectively. UV-curing properties were characterized by FT-IR at different curing time. In addition, the solubilities of the oligomers were also examined.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer-Verlag</pub><doi>10.1007/s00289-011-0576-y</doi><tpages>15</tpages></addata></record> |
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| subjects | Applied sciences Characterization and Evaluation of Materials Chemical analysis Chemistry Chemistry and Materials Science Complex Fluids and Microfluidics Curing Diisocyanates Energy consumption Exact sciences and technology Gel chromatography Hydrocarbons Molecular weight Nitrogen NMR Nuclear magnetic resonance Oligomers Organic Chemistry Organic polymers Original Paper Photoinitiators Photosensitivity Physical Chemistry Physicochemistry of polymers Polycondensation Polymer Sciences Polymerization Polyurethane resins Preparation, kinetics, thermodynamics, mechanism and catalysts Reagents Soft and Granular Matter Structural analysis Thermodynamic properties Thermogravimetric analysis Ultraviolet radiation |
| title | Synthesis and properties of UV-curable hyperbranched polyurethane acrylate oligomers containing photoinitiator |
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