Comparison of niobium-93m results obtained by two independent destructive analytical procedures and measured by low energy gamma spectrometry and liquid scintillation counting
This article presents two newly developed radiochemical procedures for the destructive analysis of niobium plates irradiated in the core of water-water energetic nuclear reactor (WWER), as well as determination of the specific activity of the generated during the irradiation metastable isotope 93m N...
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| Veröffentlicht in: | Journal of radioanalytical and nuclear chemistry 2024, Vol.333 (1), p.297-304 |
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| creator | Dobrev, Lyuben Dimitrov, Dobromir Mitev, Mladen Nonova, Tzvetana Geleva-Dimitrova, Elena Slavchev, Bozhidar Dimitrova, Desislava Zahariev, Zahari Krstevski, Srgjan |
| description | This article presents two newly developed radiochemical procedures for the destructive analysis of niobium plates irradiated in the core of water-water energetic nuclear reactor (WWER), as well as determination of the specific activity of the generated during the irradiation metastable isotope
93m
Nb. The procedures were developed and tested using standard samples containing
93m
Nb and
94
Nb. Measurements were made by low energy gamma spectrometry (LEGS) and liquid scintillation counting (LSC) and the obtained data were verified by interlaboratory comparison. All the results were compared with the calculated ones to confirm and evaluate the accuracy and superiority of the two measurement methods. |
| doi_str_mv | 10.1007/s10967-023-09236-1 |
| format | Article |
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93m
Nb. The procedures were developed and tested using standard samples containing
93m
Nb and
94
Nb. Measurements were made by low energy gamma spectrometry (LEGS) and liquid scintillation counting (LSC) and the obtained data were verified by interlaboratory comparison. All the results were compared with the calculated ones to confirm and evaluate the accuracy and superiority of the two measurement methods.</description><identifier>ISSN: 0236-5731</identifier><identifier>EISSN: 1588-2780</identifier><identifier>DOI: 10.1007/s10967-023-09236-1</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Chemistry ; Chemistry and Materials Science ; Diagnostic Radiology ; Hadrons ; Heavy Ions ; Inorganic Chemistry ; Irradiation ; Measurement methods ; Niobium ; Nuclear Chemistry ; Nuclear energy ; Nuclear facilities ; Nuclear Physics ; Nuclear reactors ; Physical Chemistry ; Radiochemical analysis ; Scintillation counters ; Spectrometry ; Spectrum analysis</subject><ispartof>Journal of radioanalytical and nuclear chemistry, 2024, Vol.333 (1), p.297-304</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>COPYRIGHT 2024 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c309t-c609978a62f289297487bfdb504b616b48a354e727c2b30d152e100ae13170873</cites><orcidid>0000-0001-8347-4217</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10967-023-09236-1$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10967-023-09236-1$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Dobrev, Lyuben</creatorcontrib><creatorcontrib>Dimitrov, Dobromir</creatorcontrib><creatorcontrib>Mitev, Mladen</creatorcontrib><creatorcontrib>Nonova, Tzvetana</creatorcontrib><creatorcontrib>Geleva-Dimitrova, Elena</creatorcontrib><creatorcontrib>Slavchev, Bozhidar</creatorcontrib><creatorcontrib>Dimitrova, Desislava</creatorcontrib><creatorcontrib>Zahariev, Zahari</creatorcontrib><creatorcontrib>Krstevski, Srgjan</creatorcontrib><title>Comparison of niobium-93m results obtained by two independent destructive analytical procedures and measured by low energy gamma spectrometry and liquid scintillation counting</title><title>Journal of radioanalytical and nuclear chemistry</title><addtitle>J Radioanal Nucl Chem</addtitle><description>This article presents two newly developed radiochemical procedures for the destructive analysis of niobium plates irradiated in the core of water-water energetic nuclear reactor (WWER), as well as determination of the specific activity of the generated during the irradiation metastable isotope
93m
Nb. The procedures were developed and tested using standard samples containing
93m
Nb and
94
Nb. Measurements were made by low energy gamma spectrometry (LEGS) and liquid scintillation counting (LSC) and the obtained data were verified by interlaboratory comparison. All the results were compared with the calculated ones to confirm and evaluate the accuracy and superiority of the two measurement methods.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Diagnostic Radiology</subject><subject>Hadrons</subject><subject>Heavy Ions</subject><subject>Inorganic Chemistry</subject><subject>Irradiation</subject><subject>Measurement methods</subject><subject>Niobium</subject><subject>Nuclear Chemistry</subject><subject>Nuclear energy</subject><subject>Nuclear facilities</subject><subject>Nuclear Physics</subject><subject>Nuclear reactors</subject><subject>Physical Chemistry</subject><subject>Radiochemical analysis</subject><subject>Scintillation counters</subject><subject>Spectrometry</subject><subject>Spectrum analysis</subject><issn>0236-5731</issn><issn>1588-2780</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9Uctq3TAUNKWF3qb5gawEXTs5kmxLWoZLXxDopl0LWT42CrbkSHKDv6q_WOW6kF0RSJxhZjijqaobCrcUQNwlCqoTNTBeg2K8q-mb6kRbKWsmJLytTvACtoLT99WHlB4BQEnJT9Wfc1hWE10KnoSReBd6ty214guJmLY5JxL6bJzHgfQ7yc-BOD_giuXymQyYctxsdr-RGG_mPTtrZrLGYHHYikNBB7KgSWW4OMzhmaDHOO1kMstiSFrR5hgWzHG_sGf3tLmBJOt8dvNssiu72bCVyU8fq3ejmRNe_3uvql9fPv88f6sffnz9fr5_qC0HlWvbgVJCmo6NTCqmRCNFPw59C03f0a5vpOFtg4IJy3oOA20Zlo80SDkVIAW_qj4dviXK01ZS6sewxZIwaaZo13Dg0BTW7cGazIza-THkaGw5Ay7OBo-jK_i9EEqolrWqCNghsDGkFHHUa3SLibumoF-a1EeTuvSlL01qWkT8EKVC9hPG113-o_oL5SSktw</recordid><startdate>2024</startdate><enddate>2024</enddate><creator>Dobrev, Lyuben</creator><creator>Dimitrov, Dobromir</creator><creator>Mitev, Mladen</creator><creator>Nonova, Tzvetana</creator><creator>Geleva-Dimitrova, Elena</creator><creator>Slavchev, Bozhidar</creator><creator>Dimitrova, Desislava</creator><creator>Zahariev, Zahari</creator><creator>Krstevski, Srgjan</creator><general>Springer International Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0001-8347-4217</orcidid></search><sort><creationdate>2024</creationdate><title>Comparison of niobium-93m results obtained by two independent destructive analytical procedures and measured by low energy gamma spectrometry and liquid scintillation counting</title><author>Dobrev, Lyuben ; Dimitrov, Dobromir ; Mitev, Mladen ; Nonova, Tzvetana ; Geleva-Dimitrova, Elena ; Slavchev, Bozhidar ; Dimitrova, Desislava ; Zahariev, Zahari ; Krstevski, Srgjan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c309t-c609978a62f289297487bfdb504b616b48a354e727c2b30d152e100ae13170873</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Diagnostic Radiology</topic><topic>Hadrons</topic><topic>Heavy Ions</topic><topic>Inorganic Chemistry</topic><topic>Irradiation</topic><topic>Measurement methods</topic><topic>Niobium</topic><topic>Nuclear Chemistry</topic><topic>Nuclear energy</topic><topic>Nuclear facilities</topic><topic>Nuclear Physics</topic><topic>Nuclear reactors</topic><topic>Physical Chemistry</topic><topic>Radiochemical analysis</topic><topic>Scintillation counters</topic><topic>Spectrometry</topic><topic>Spectrum analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Dobrev, Lyuben</creatorcontrib><creatorcontrib>Dimitrov, Dobromir</creatorcontrib><creatorcontrib>Mitev, Mladen</creatorcontrib><creatorcontrib>Nonova, Tzvetana</creatorcontrib><creatorcontrib>Geleva-Dimitrova, Elena</creatorcontrib><creatorcontrib>Slavchev, Bozhidar</creatorcontrib><creatorcontrib>Dimitrova, Desislava</creatorcontrib><creatorcontrib>Zahariev, Zahari</creatorcontrib><creatorcontrib>Krstevski, Srgjan</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Dobrev, Lyuben</au><au>Dimitrov, Dobromir</au><au>Mitev, Mladen</au><au>Nonova, Tzvetana</au><au>Geleva-Dimitrova, Elena</au><au>Slavchev, Bozhidar</au><au>Dimitrova, Desislava</au><au>Zahariev, Zahari</au><au>Krstevski, Srgjan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Comparison of niobium-93m results obtained by two independent destructive analytical procedures and measured by low energy gamma spectrometry and liquid scintillation counting</atitle><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle><stitle>J Radioanal Nucl Chem</stitle><date>2024</date><risdate>2024</risdate><volume>333</volume><issue>1</issue><spage>297</spage><epage>304</epage><pages>297-304</pages><issn>0236-5731</issn><eissn>1588-2780</eissn><abstract>This article presents two newly developed radiochemical procedures for the destructive analysis of niobium plates irradiated in the core of water-water energetic nuclear reactor (WWER), as well as determination of the specific activity of the generated during the irradiation metastable isotope
93m
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93m
Nb and
94
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| subjects | Chemistry Chemistry and Materials Science Diagnostic Radiology Hadrons Heavy Ions Inorganic Chemistry Irradiation Measurement methods Niobium Nuclear Chemistry Nuclear energy Nuclear facilities Nuclear Physics Nuclear reactors Physical Chemistry Radiochemical analysis Scintillation counters Spectrometry Spectrum analysis |
| title | Comparison of niobium-93m results obtained by two independent destructive analytical procedures and measured by low energy gamma spectrometry and liquid scintillation counting |
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