Ethers and Their Oligomeric Derivatives Obtained from 2,4,6,8-Tetra(hydroxymethyl)glycoluril

In this work, a series of 2,4,6,8-tetra(alkoxymethyl)glycoluril esters and their derivatives was synthesized for the first time, starting from 2,4,6,8-tetra(hydroxymethyl)glycoluril, the properties and spectral data of the synthesized compounds were described. Individual oligomers, derivatives of 2,...

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Veröffentlicht in:	Russian journal of general chemistry 2023-12, Vol.93 (Suppl 2), p.S456-S462
Hauptverfasser:	Panshina, S. Yu, Ponomarenko, О. V., Bakibaev, A. A., Malkov, V. S., Zhortarova, A. A.
Format:	Artikel
Sprache:	eng
Schlagworte:	Chemistry Chemistry and Materials Science Chemistry/Food Science Dimerization Esters Ethers Infrared spectroscopy NMR spectroscopy Oligomerization Synthesis
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container_title	Russian journal of general chemistry
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creator	Panshina, S. Yu Ponomarenko, О. V. Bakibaev, A. A. Malkov, V. S. Zhortarova, A. A.
description	In this work, a series of 2,4,6,8-tetra(alkoxymethyl)glycoluril esters and their derivatives was synthesized for the first time, starting from 2,4,6,8-tetra(hydroxymethyl)glycoluril, the properties and spectral data of the synthesized compounds were described. Individual oligomers, derivatives of 2,4,6,8-tetra(methoxymethyl)glycoluril, were isolated and identified, their structures were described using HPLC analysis and IR and NMR spectroscopy. A similar possibility for the dimerization/oligomerization reactions of 2,4,6,8-tetra(ethoxymethyl)-, 2,4,6,8-tetra(isopropoxymethyl)-, and 2,4,6,8-tetra(butoxymethyl) derivatives of glycoluril with the release of macrocomponents was shown.
doi_str_mv	10.1134/S1070363223150069
format	Article
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subjects	Chemistry Chemistry and Materials Science Chemistry/Food Science Dimerization Esters Ethers Infrared spectroscopy NMR spectroscopy Oligomerization Synthesis
title	Ethers and Their Oligomeric Derivatives Obtained from 2,4,6,8-Tetra(hydroxymethyl)glycoluril
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