A modular table-top setup for ultrafast x-ray diffraction
We present a table-top setup for femtosecond time-resolved x-ray diffraction based on a Cu Kα (8.05 keV) laser driven plasma x-ray source. Due to its modular design, it provides high accessibility to its individual components (e.g., x-ray optics and sample environment). The Kα-yield of the source is...
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creator | Lu, W. Nicoul, M. Shymanovich, U. Tarasevitch, A. Horn-von Hoegen, M. von der Linde, D. Sokolowski-Tinten, K. |
description | We present a table-top setup for femtosecond time-resolved x-ray diffraction based on a Cu Kα (8.05 keV) laser driven plasma x-ray source. Due to its modular design, it provides high accessibility to its individual components (e.g., x-ray optics and sample environment). The Kα-yield of the source is optimized using a pre-pulse scheme. A magnifying multilayer x-ray mirror with Montel–Helios geometry is used to collect the emitted radiation, resulting in a quasi-collimated flux of more than 105 Cu Kα photons/pulse impinging on the sample under investigation at a repetition rate of 10 Hz. A gas ionization chamber detector is placed right after the x-ray mirror and used for the normalization of the diffraction signals, enabling the measurement of relative signal changes of less than 1% even at the given low repetition rate. Time-resolved diffraction experiments on laser-excited epitaxial Bi films serve as an example to demonstrate the capabilities of the setup. The setup can also be used for Debye–Scherrer type measurements on poly-crystalline samples. |
doi_str_mv | 10.1063/5.0181132 |
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Due to its modular design, it provides high accessibility to its individual components (e.g., x-ray optics and sample environment). The Kα-yield of the source is optimized using a pre-pulse scheme. A magnifying multilayer x-ray mirror with Montel–Helios geometry is used to collect the emitted radiation, resulting in a quasi-collimated flux of more than 105 Cu Kα photons/pulse impinging on the sample under investigation at a repetition rate of 10 Hz. A gas ionization chamber detector is placed right after the x-ray mirror and used for the normalization of the diffraction signals, enabling the measurement of relative signal changes of less than 1% even at the given low repetition rate. Time-resolved diffraction experiments on laser-excited epitaxial Bi films serve as an example to demonstrate the capabilities of the setup. The setup can also be used for Debye–Scherrer type measurements on poly-crystalline samples.</description><identifier>ISSN: 0034-6748</identifier><identifier>EISSN: 1089-7623</identifier><identifier>DOI: 10.1063/5.0181132</identifier><identifier>PMID: 38190494</identifier><identifier>CODEN: RSINAK</identifier><language>eng</language><publisher>United States: American Institute of Physics</publisher><subject>Gas ionization ; Geometrical optics ; Ionization chambers ; Modular design ; Multilayers ; Repetition ; X ray mirrors ; X ray optics ; X ray sources ; X-ray diffraction</subject><ispartof>Review of scientific instruments, 2024-01, Vol.95 (1)</ispartof><rights>Author(s)</rights><rights>2024 Author(s). 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Due to its modular design, it provides high accessibility to its individual components (e.g., x-ray optics and sample environment). The Kα-yield of the source is optimized using a pre-pulse scheme. A magnifying multilayer x-ray mirror with Montel–Helios geometry is used to collect the emitted radiation, resulting in a quasi-collimated flux of more than 105 Cu Kα photons/pulse impinging on the sample under investigation at a repetition rate of 10 Hz. A gas ionization chamber detector is placed right after the x-ray mirror and used for the normalization of the diffraction signals, enabling the measurement of relative signal changes of less than 1% even at the given low repetition rate. Time-resolved diffraction experiments on laser-excited epitaxial Bi films serve as an example to demonstrate the capabilities of the setup. The setup can also be used for Debye–Scherrer type measurements on poly-crystalline samples.</description><subject>Gas ionization</subject><subject>Geometrical optics</subject><subject>Ionization chambers</subject><subject>Modular design</subject><subject>Multilayers</subject><subject>Repetition</subject><subject>X ray mirrors</subject><subject>X ray optics</subject><subject>X ray sources</subject><subject>X-ray diffraction</subject><issn>0034-6748</issn><issn>1089-7623</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp90E9LwzAYBvAgipvTg19ACl5U6MybNE1yHMN_MPCi55CmCXS0S01ScN9-HZsePPhensuPh5cHoWvAc8AlfWRzDAKAkhM0BSxkzktCT9EUY1rkJS_EBF3EuMbjMYBzNKECJC5kMUVykXW-HlodsqSr1ubJ91m0aegz50M2tClop2PKvvOgt1ndOBe0SY3fXKIzp9tor445Q5_PTx_L13z1_vK2XKxyQwua8sqNyaHixgAtqtJqbpkTzGmgvGTMMFoLx0ilMQeoa1ICAydAM2FqWRk6Q3eH3j74r8HGpLomGtu2emP9EBWRQBgpJC1HevuHrv0QNuN3ewWMUCr5qO4PygQfY7BO9aHpdNgqwGq_p2LquOdob46NQ9XZ-lf-DDiChwOIpkl6v8s_bTtHDnrl</recordid><startdate>20240101</startdate><enddate>20240101</enddate><creator>Lu, W.</creator><creator>Nicoul, M.</creator><creator>Shymanovich, U.</creator><creator>Tarasevitch, A.</creator><creator>Horn-von Hoegen, M.</creator><creator>von der Linde, D.</creator><creator>Sokolowski-Tinten, K.</creator><general>American Institute of Physics</general><scope>AJDQP</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0003-2621-8000</orcidid><orcidid>https://orcid.org/0000-0003-3451-1979</orcidid><orcidid>https://orcid.org/0000-0003-4498-733X</orcidid><orcidid>https://orcid.org/0000-0003-0324-3457</orcidid><orcidid>https://orcid.org/0000-0001-5618-3879</orcidid><orcidid>https://orcid.org/0000-0002-7979-5357</orcidid><orcidid>https://orcid.org/0000-0002-2573-5738</orcidid></search><sort><creationdate>20240101</creationdate><title>A modular table-top setup for ultrafast x-ray diffraction</title><author>Lu, W. ; Nicoul, M. ; Shymanovich, U. ; Tarasevitch, A. ; Horn-von Hoegen, M. ; von der Linde, D. ; Sokolowski-Tinten, K.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c343t-bfc3471b7cc134b6ea7e5f85fa137655c53d8f52ba0711dd26151f81a58cd9bc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Gas ionization</topic><topic>Geometrical optics</topic><topic>Ionization chambers</topic><topic>Modular design</topic><topic>Multilayers</topic><topic>Repetition</topic><topic>X ray mirrors</topic><topic>X ray optics</topic><topic>X ray sources</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lu, W.</creatorcontrib><creatorcontrib>Nicoul, M.</creatorcontrib><creatorcontrib>Shymanovich, U.</creatorcontrib><creatorcontrib>Tarasevitch, A.</creatorcontrib><creatorcontrib>Horn-von Hoegen, M.</creatorcontrib><creatorcontrib>von der Linde, D.</creatorcontrib><creatorcontrib>Sokolowski-Tinten, K.</creatorcontrib><collection>AIP Open Access Journals</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Review of scientific instruments</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lu, W.</au><au>Nicoul, M.</au><au>Shymanovich, U.</au><au>Tarasevitch, A.</au><au>Horn-von Hoegen, M.</au><au>von der Linde, D.</au><au>Sokolowski-Tinten, K.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A modular table-top setup for ultrafast x-ray diffraction</atitle><jtitle>Review of scientific instruments</jtitle><addtitle>Rev Sci Instrum</addtitle><date>2024-01-01</date><risdate>2024</risdate><volume>95</volume><issue>1</issue><issn>0034-6748</issn><eissn>1089-7623</eissn><coden>RSINAK</coden><abstract>We present a table-top setup for femtosecond time-resolved x-ray diffraction based on a Cu Kα (8.05 keV) laser driven plasma x-ray source. Due to its modular design, it provides high accessibility to its individual components (e.g., x-ray optics and sample environment). The Kα-yield of the source is optimized using a pre-pulse scheme. A magnifying multilayer x-ray mirror with Montel–Helios geometry is used to collect the emitted radiation, resulting in a quasi-collimated flux of more than 105 Cu Kα photons/pulse impinging on the sample under investigation at a repetition rate of 10 Hz. A gas ionization chamber detector is placed right after the x-ray mirror and used for the normalization of the diffraction signals, enabling the measurement of relative signal changes of less than 1% even at the given low repetition rate. Time-resolved diffraction experiments on laser-excited epitaxial Bi films serve as an example to demonstrate the capabilities of the setup. The setup can also be used for Debye–Scherrer type measurements on poly-crystalline samples.</abstract><cop>United States</cop><pub>American Institute of Physics</pub><pmid>38190494</pmid><doi>10.1063/5.0181132</doi><tpages>12</tpages><orcidid>https://orcid.org/0000-0003-2621-8000</orcidid><orcidid>https://orcid.org/0000-0003-3451-1979</orcidid><orcidid>https://orcid.org/0000-0003-4498-733X</orcidid><orcidid>https://orcid.org/0000-0003-0324-3457</orcidid><orcidid>https://orcid.org/0000-0001-5618-3879</orcidid><orcidid>https://orcid.org/0000-0002-7979-5357</orcidid><orcidid>https://orcid.org/0000-0002-2573-5738</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Gas ionization Geometrical optics Ionization chambers Modular design Multilayers Repetition X ray mirrors X ray optics X ray sources X-ray diffraction |
title | A modular table-top setup for ultrafast x-ray diffraction |
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