Characterization of niobium pentoxide synthesized by spray pyrolysis technique and comparison with hydrothermal method
Niobium pentoxide (Nb2O5) is a polymorphic ceramic with semiconductor characteristics applied in various fields of study. In this work, the Nb2O5 synthesis by the spray pyrolysis route was compared to the hydrothermal technique. The obtained materials were characterized by N2 physisorption (BET‐N2),...
Gespeichert in:
| Veröffentlicht in: | Canadian journal of chemical engineering 2024-02, Vol.102 (2), p.738-747 |
|---|---|
| Hauptverfasser: | , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 747 |
|---|---|
| container_issue | 2 |
| container_start_page | 738 |
| container_title | Canadian journal of chemical engineering |
| container_volume | 102 |
| creator | Andrade Schaffner, Rodolfo Oliveira, Elson Domingues, Roberta Carolina Pelissari Rizzo Conceição, Leandro Yamamoto, Carlos Itsuo Muniz, Graciela Inêz Bolzon Alves, Helton José |
| description | Niobium pentoxide (Nb2O5) is a polymorphic ceramic with semiconductor characteristics applied in various fields of study. In this work, the Nb2O5 synthesis by the spray pyrolysis route was compared to the hydrothermal technique. The obtained materials were characterized by N2 physisorption (BET‐N2), average particle size distribution by dynamic light scattering (DLS), X‐ray diffractometry (XRD), transmission electron microscopy (TEM), and X‐ray fluorescence (XRF) spectroscopy. The material synthesized by the spray pyrolysis technique presented high specific area and pore volume, high crystallinity, homogeneity, and nanometric particles, thus representing a potential technique for the Nb2O5 synthesis. |
| doi_str_mv | 10.1002/cjce.25073 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2909367048</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2909367048</sourcerecordid><originalsourceid>FETCH-LOGICAL-c2603-65d9924b0dfcd2702b558f4ae7d21affc4e262f5a1c3b86fdf015c1631d43ff23</originalsourceid><addsrcrecordid>eNp9kMtKxDAUhoMoOI5ufIKAO6HjSdLrUsp4Y8CNgruQ5kIztE1NOo6dp7djXbs6HPj-_xw-hK4JrAgAvZNbqVc0gYydoAUpWBEBKT5O0QIA8igGFp-jixC200ohJgv0VdbCCzlobw9isK7DzuDOusruWtzrbnDfVmkcxm6odbAHrXA14tB7MeJ-9K4Zgw140LLu7OdOY9EpLF3bC2_DVLa3Q43rUXk3xX0rGtzqoXbqEp0Z0QR99TeX6P1h_VY-RZvXx-fyfhNJmgKL0kQVBY0rUEYqmgGtkiQ3sdCZokQYI2NNU2oSQSSr8tQoAySRJGVExcwYypboZu7tvZveCwPfup3vppOcFlCwNIM4n6jbmZLeheC14b23rfAjJ8CPXvnRK__1OsFkhve20eM_JC9fyvWc-QFFXX5K</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2909367048</pqid></control><display><type>article</type><title>Characterization of niobium pentoxide synthesized by spray pyrolysis technique and comparison with hydrothermal method</title><source>Wiley Online Library Journals Frontfile Complete</source><creator>Andrade Schaffner, Rodolfo ; Oliveira, Elson ; Domingues, Roberta Carolina Pelissari Rizzo ; Conceição, Leandro ; Yamamoto, Carlos Itsuo ; Muniz, Graciela Inêz Bolzon ; Alves, Helton José</creator><creatorcontrib>Andrade Schaffner, Rodolfo ; Oliveira, Elson ; Domingues, Roberta Carolina Pelissari Rizzo ; Conceição, Leandro ; Yamamoto, Carlos Itsuo ; Muniz, Graciela Inêz Bolzon ; Alves, Helton José</creatorcontrib><description>Niobium pentoxide (Nb2O5) is a polymorphic ceramic with semiconductor characteristics applied in various fields of study. In this work, the Nb2O5 synthesis by the spray pyrolysis route was compared to the hydrothermal technique. The obtained materials were characterized by N2 physisorption (BET‐N2), average particle size distribution by dynamic light scattering (DLS), X‐ray diffractometry (XRD), transmission electron microscopy (TEM), and X‐ray fluorescence (XRF) spectroscopy. The material synthesized by the spray pyrolysis technique presented high specific area and pore volume, high crystallinity, homogeneity, and nanometric particles, thus representing a potential technique for the Nb2O5 synthesis.</description><identifier>ISSN: 0008-4034</identifier><identifier>EISSN: 1939-019X</identifier><identifier>DOI: 10.1002/cjce.25073</identifier><language>eng</language><publisher>Hoboken, USA: John Wiley & Sons, Inc</publisher><subject>Homogeneity ; hydrothermal ; Nb2O5 ; niobium ; Niobium oxides ; Particle size distribution ; Photon correlation spectroscopy ; Spray pyrolysis ; Synthesis</subject><ispartof>Canadian journal of chemical engineering, 2024-02, Vol.102 (2), p.738-747</ispartof><rights>2023 Canadian Society for Chemical Engineering.</rights><rights>2024 Canadian Society for Chemical Engineering</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c2603-65d9924b0dfcd2702b558f4ae7d21affc4e262f5a1c3b86fdf015c1631d43ff23</cites><orcidid>0000-0002-9435-2693</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fcjce.25073$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fcjce.25073$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids></links><search><creatorcontrib>Andrade Schaffner, Rodolfo</creatorcontrib><creatorcontrib>Oliveira, Elson</creatorcontrib><creatorcontrib>Domingues, Roberta Carolina Pelissari Rizzo</creatorcontrib><creatorcontrib>Conceição, Leandro</creatorcontrib><creatorcontrib>Yamamoto, Carlos Itsuo</creatorcontrib><creatorcontrib>Muniz, Graciela Inêz Bolzon</creatorcontrib><creatorcontrib>Alves, Helton José</creatorcontrib><title>Characterization of niobium pentoxide synthesized by spray pyrolysis technique and comparison with hydrothermal method</title><title>Canadian journal of chemical engineering</title><description>Niobium pentoxide (Nb2O5) is a polymorphic ceramic with semiconductor characteristics applied in various fields of study. In this work, the Nb2O5 synthesis by the spray pyrolysis route was compared to the hydrothermal technique. The obtained materials were characterized by N2 physisorption (BET‐N2), average particle size distribution by dynamic light scattering (DLS), X‐ray diffractometry (XRD), transmission electron microscopy (TEM), and X‐ray fluorescence (XRF) spectroscopy. The material synthesized by the spray pyrolysis technique presented high specific area and pore volume, high crystallinity, homogeneity, and nanometric particles, thus representing a potential technique for the Nb2O5 synthesis.</description><subject>Homogeneity</subject><subject>hydrothermal</subject><subject>Nb2O5</subject><subject>niobium</subject><subject>Niobium oxides</subject><subject>Particle size distribution</subject><subject>Photon correlation spectroscopy</subject><subject>Spray pyrolysis</subject><subject>Synthesis</subject><issn>0008-4034</issn><issn>1939-019X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9kMtKxDAUhoMoOI5ufIKAO6HjSdLrUsp4Y8CNgruQ5kIztE1NOo6dp7djXbs6HPj-_xw-hK4JrAgAvZNbqVc0gYydoAUpWBEBKT5O0QIA8igGFp-jixC200ohJgv0VdbCCzlobw9isK7DzuDOusruWtzrbnDfVmkcxm6odbAHrXA14tB7MeJ-9K4Zgw140LLu7OdOY9EpLF3bC2_DVLa3Q43rUXk3xX0rGtzqoXbqEp0Z0QR99TeX6P1h_VY-RZvXx-fyfhNJmgKL0kQVBY0rUEYqmgGtkiQ3sdCZokQYI2NNU2oSQSSr8tQoAySRJGVExcwYypboZu7tvZveCwPfup3vppOcFlCwNIM4n6jbmZLeheC14b23rfAjJ8CPXvnRK__1OsFkhve20eM_JC9fyvWc-QFFXX5K</recordid><startdate>202402</startdate><enddate>202402</enddate><creator>Andrade Schaffner, Rodolfo</creator><creator>Oliveira, Elson</creator><creator>Domingues, Roberta Carolina Pelissari Rizzo</creator><creator>Conceição, Leandro</creator><creator>Yamamoto, Carlos Itsuo</creator><creator>Muniz, Graciela Inêz Bolzon</creator><creator>Alves, Helton José</creator><general>John Wiley & Sons, Inc</general><general>Wiley Subscription Services, Inc</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0002-9435-2693</orcidid></search><sort><creationdate>202402</creationdate><title>Characterization of niobium pentoxide synthesized by spray pyrolysis technique and comparison with hydrothermal method</title><author>Andrade Schaffner, Rodolfo ; Oliveira, Elson ; Domingues, Roberta Carolina Pelissari Rizzo ; Conceição, Leandro ; Yamamoto, Carlos Itsuo ; Muniz, Graciela Inêz Bolzon ; Alves, Helton José</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2603-65d9924b0dfcd2702b558f4ae7d21affc4e262f5a1c3b86fdf015c1631d43ff23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Homogeneity</topic><topic>hydrothermal</topic><topic>Nb2O5</topic><topic>niobium</topic><topic>Niobium oxides</topic><topic>Particle size distribution</topic><topic>Photon correlation spectroscopy</topic><topic>Spray pyrolysis</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Andrade Schaffner, Rodolfo</creatorcontrib><creatorcontrib>Oliveira, Elson</creatorcontrib><creatorcontrib>Domingues, Roberta Carolina Pelissari Rizzo</creatorcontrib><creatorcontrib>Conceição, Leandro</creatorcontrib><creatorcontrib>Yamamoto, Carlos Itsuo</creatorcontrib><creatorcontrib>Muniz, Graciela Inêz Bolzon</creatorcontrib><creatorcontrib>Alves, Helton José</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Canadian journal of chemical engineering</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Andrade Schaffner, Rodolfo</au><au>Oliveira, Elson</au><au>Domingues, Roberta Carolina Pelissari Rizzo</au><au>Conceição, Leandro</au><au>Yamamoto, Carlos Itsuo</au><au>Muniz, Graciela Inêz Bolzon</au><au>Alves, Helton José</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterization of niobium pentoxide synthesized by spray pyrolysis technique and comparison with hydrothermal method</atitle><jtitle>Canadian journal of chemical engineering</jtitle><date>2024-02</date><risdate>2024</risdate><volume>102</volume><issue>2</issue><spage>738</spage><epage>747</epage><pages>738-747</pages><issn>0008-4034</issn><eissn>1939-019X</eissn><abstract>Niobium pentoxide (Nb2O5) is a polymorphic ceramic with semiconductor characteristics applied in various fields of study. In this work, the Nb2O5 synthesis by the spray pyrolysis route was compared to the hydrothermal technique. The obtained materials were characterized by N2 physisorption (BET‐N2), average particle size distribution by dynamic light scattering (DLS), X‐ray diffractometry (XRD), transmission electron microscopy (TEM), and X‐ray fluorescence (XRF) spectroscopy. The material synthesized by the spray pyrolysis technique presented high specific area and pore volume, high crystallinity, homogeneity, and nanometric particles, thus representing a potential technique for the Nb2O5 synthesis.</abstract><cop>Hoboken, USA</cop><pub>John Wiley & Sons, Inc</pub><doi>10.1002/cjce.25073</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-9435-2693</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0008-4034 |
| ispartof | Canadian journal of chemical engineering, 2024-02, Vol.102 (2), p.738-747 |
| issn | 0008-4034 1939-019X |
| language | eng |
| recordid | cdi_proquest_journals_2909367048 |
| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Homogeneity hydrothermal Nb2O5 niobium Niobium oxides Particle size distribution Photon correlation spectroscopy Spray pyrolysis Synthesis |
| title | Characterization of niobium pentoxide synthesized by spray pyrolysis technique and comparison with hydrothermal method |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-10T20%3A16%3A31IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Characterization%20of%20niobium%20pentoxide%20synthesized%20by%20spray%20pyrolysis%20technique%20and%20comparison%20with%20hydrothermal%20method&rft.jtitle=Canadian%20journal%20of%20chemical%20engineering&rft.au=Andrade%20Schaffner,%20Rodolfo&rft.date=2024-02&rft.volume=102&rft.issue=2&rft.spage=738&rft.epage=747&rft.pages=738-747&rft.issn=0008-4034&rft.eissn=1939-019X&rft_id=info:doi/10.1002/cjce.25073&rft_dat=%3Cproquest_cross%3E2909367048%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2909367048&rft_id=info:pmid/&rfr_iscdi=true |