Synthesis of Ag2O-TiO2-Kaolinite Clay Nanocomposite for Efficient Removal of Mn2+, Fe3+, Cu2+, and Pb2+ and Pathogens in Mining Wastewater
Synthesis of Ag 2 O-TiO 2 -kaolinite clay nanocomposite was undertaken to eliminate some selected heavy metals released into the environment from mining wastewater. Silver nitrate and titanium-tetra-isopropoxide were employed as the bulk reagents for the Ag 2 O-TiO 2 nanoparticles synthesis, using a...
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| Veröffentlicht in: | Water, air, and soil pollution air, and soil pollution, 2024, Vol.235 (1), p.42-42, Article 42 |
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| creator | Ajala, Mary Adejoke Abdulkareem, Ambali Saka Kovo, Abdulsalami Sanni Tijani, Jimoh Oladejo Ajala, Elijah Olawale |
| description | Synthesis of Ag
2
O-TiO
2
-kaolinite clay nanocomposite was undertaken to eliminate some selected heavy metals released into the environment from mining wastewater. Silver nitrate and titanium-tetra-isopropoxide were employed as the bulk reagents for the Ag
2
O-TiO
2
nanoparticles synthesis, using an aqueous extract of
Parkia biglobossa
leaf (green synthesis method)
.
The Ag
2
O-TiO
2
nanoparticles were supported on acid-activated kaolinite clay via wet impregnation method, to develop the nanocomposite and were characterized for phase structure, morphology, and oxidation states. The functionality of the nanocomposite for the sequestration of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions from mining wastewater was examined by adsorption studies. The XRD pattern of the Ag
2
O-TiO
2
-kaolinite clay reveals the synthesis of the rutile phase of TiO
2
embedded in the kaolinite clay. While the HRSEM shows an evenly distributed arrangement of hemispherical stacks of kaolinites. The oxidation states of Ag
2
O and TiO
2
revealed by the XPS are + 1 and + 4 respectively either as binary or ternary nanocomposite. The Ag
2
O-TiO
2
-clay nanocomposite adsorbed 99.85%, 97.85% 95.18%, and 40% of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions at 120 min from the mining wastewater respectively. The synergetic efforts of the Ag
2
O-TiO
2
-clay were responsible for the adsorptive capability of the nanocomposite for the removal of the selected heavy metal ions.
Graphical abstract |
| doi_str_mv | 10.1007/s11270-023-06811-w |
| format | Article |
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2
O-TiO
2
-kaolinite clay nanocomposite was undertaken to eliminate some selected heavy metals released into the environment from mining wastewater. Silver nitrate and titanium-tetra-isopropoxide were employed as the bulk reagents for the Ag
2
O-TiO
2
nanoparticles synthesis, using an aqueous extract of
Parkia biglobossa
leaf (green synthesis method)
.
The Ag
2
O-TiO
2
nanoparticles were supported on acid-activated kaolinite clay via wet impregnation method, to develop the nanocomposite and were characterized for phase structure, morphology, and oxidation states. The functionality of the nanocomposite for the sequestration of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions from mining wastewater was examined by adsorption studies. The XRD pattern of the Ag
2
O-TiO
2
-kaolinite clay reveals the synthesis of the rutile phase of TiO
2
embedded in the kaolinite clay. While the HRSEM shows an evenly distributed arrangement of hemispherical stacks of kaolinites. The oxidation states of Ag
2
O and TiO
2
revealed by the XPS are + 1 and + 4 respectively either as binary or ternary nanocomposite. The Ag
2
O-TiO
2
-clay nanocomposite adsorbed 99.85%, 97.85% 95.18%, and 40% of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions at 120 min from the mining wastewater respectively. The synergetic efforts of the Ag
2
O-TiO
2
-clay were responsible for the adsorptive capability of the nanocomposite for the removal of the selected heavy metal ions.
Graphical abstract</description><identifier>ISSN: 0049-6979</identifier><identifier>EISSN: 1573-2932</identifier><identifier>DOI: 10.1007/s11270-023-06811-w</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Activated clay ; adsorption ; Adsorptivity ; air ; Atmospheric Protection/Air Quality Control/Air Pollution ; Clay ; Climate Change/Climate Change Impacts ; Copper ; Earth and Environmental Science ; Environment ; Environmental monitoring ; Ferric ions ; Heavy metals ; Hydrogeology ; Iron ; Kaolinite ; Lead ; leaves ; Metal ions ; Nanocomposites ; Nanoparticles ; Oxidation ; Parkia ; Pathogens ; Reagents ; Removal ; Rutile ; Silver ; Silver nitrate ; soil ; Soil Science & Conservation ; Solid phases ; Synthesis ; Titanium ; Titanium dioxide ; Wastewater ; water ; Water Quality/Water Pollution</subject><ispartof>Water, air, and soil pollution, 2024, Vol.235 (1), p.42-42, Article 42</ispartof><rights>The Author(s), under exclusive licence to Springer Nature Switzerland AG 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c233t-3fa5baf09b9732e3eedab722fdf8fb1be90faa9a73fdb2378a122ef0ae682e393</cites><orcidid>0009-0006-5346-4783</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11270-023-06811-w$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11270-023-06811-w$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Ajala, Mary Adejoke</creatorcontrib><creatorcontrib>Abdulkareem, Ambali Saka</creatorcontrib><creatorcontrib>Kovo, Abdulsalami Sanni</creatorcontrib><creatorcontrib>Tijani, Jimoh Oladejo</creatorcontrib><creatorcontrib>Ajala, Elijah Olawale</creatorcontrib><title>Synthesis of Ag2O-TiO2-Kaolinite Clay Nanocomposite for Efficient Removal of Mn2+, Fe3+, Cu2+, and Pb2+ and Pathogens in Mining Wastewater</title><title>Water, air, and soil pollution</title><addtitle>Water Air Soil Pollut</addtitle><description>Synthesis of Ag
2
O-TiO
2
-kaolinite clay nanocomposite was undertaken to eliminate some selected heavy metals released into the environment from mining wastewater. Silver nitrate and titanium-tetra-isopropoxide were employed as the bulk reagents for the Ag
2
O-TiO
2
nanoparticles synthesis, using an aqueous extract of
Parkia biglobossa
leaf (green synthesis method)
.
The Ag
2
O-TiO
2
nanoparticles were supported on acid-activated kaolinite clay via wet impregnation method, to develop the nanocomposite and were characterized for phase structure, morphology, and oxidation states. The functionality of the nanocomposite for the sequestration of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions from mining wastewater was examined by adsorption studies. The XRD pattern of the Ag
2
O-TiO
2
-kaolinite clay reveals the synthesis of the rutile phase of TiO
2
embedded in the kaolinite clay. While the HRSEM shows an evenly distributed arrangement of hemispherical stacks of kaolinites. The oxidation states of Ag
2
O and TiO
2
revealed by the XPS are + 1 and + 4 respectively either as binary or ternary nanocomposite. The Ag
2
O-TiO
2
-clay nanocomposite adsorbed 99.85%, 97.85% 95.18%, and 40% of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions at 120 min from the mining wastewater respectively. The synergetic efforts of the Ag
2
O-TiO
2
-clay were responsible for the adsorptive capability of the nanocomposite for the removal of the selected heavy metal ions.
Graphical abstract</description><subject>Activated clay</subject><subject>adsorption</subject><subject>Adsorptivity</subject><subject>air</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Clay</subject><subject>Climate Change/Climate Change Impacts</subject><subject>Copper</subject><subject>Earth and Environmental Science</subject><subject>Environment</subject><subject>Environmental monitoring</subject><subject>Ferric ions</subject><subject>Heavy metals</subject><subject>Hydrogeology</subject><subject>Iron</subject><subject>Kaolinite</subject><subject>Lead</subject><subject>leaves</subject><subject>Metal ions</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Oxidation</subject><subject>Parkia</subject><subject>Pathogens</subject><subject>Reagents</subject><subject>Removal</subject><subject>Rutile</subject><subject>Silver</subject><subject>Silver nitrate</subject><subject>soil</subject><subject>Soil Science & Conservation</subject><subject>Solid phases</subject><subject>Synthesis</subject><subject>Titanium</subject><subject>Titanium dioxide</subject><subject>Wastewater</subject><subject>water</subject><subject>Water Quality/Water 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of Ag2O-TiO2-Kaolinite Clay Nanocomposite for Efficient Removal of Mn2+, Fe3+, Cu2+, and Pb2+ and Pathogens in Mining Wastewater</title><author>Ajala, Mary Adejoke ; Abdulkareem, Ambali Saka ; Kovo, Abdulsalami Sanni ; Tijani, Jimoh Oladejo ; Ajala, Elijah Olawale</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c233t-3fa5baf09b9732e3eedab722fdf8fb1be90faa9a73fdb2378a122ef0ae682e393</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Activated clay</topic><topic>adsorption</topic><topic>Adsorptivity</topic><topic>air</topic><topic>Atmospheric Protection/Air Quality Control/Air Pollution</topic><topic>Clay</topic><topic>Climate Change/Climate Change Impacts</topic><topic>Copper</topic><topic>Earth and Environmental Science</topic><topic>Environment</topic><topic>Environmental monitoring</topic><topic>Ferric ions</topic><topic>Heavy metals</topic><topic>Hydrogeology</topic><topic>Iron</topic><topic>Kaolinite</topic><topic>Lead</topic><topic>leaves</topic><topic>Metal ions</topic><topic>Nanocomposites</topic><topic>Nanoparticles</topic><topic>Oxidation</topic><topic>Parkia</topic><topic>Pathogens</topic><topic>Reagents</topic><topic>Removal</topic><topic>Rutile</topic><topic>Silver</topic><topic>Silver nitrate</topic><topic>soil</topic><topic>Soil Science & Conservation</topic><topic>Solid phases</topic><topic>Synthesis</topic><topic>Titanium</topic><topic>Titanium dioxide</topic><topic>Wastewater</topic><topic>water</topic><topic>Water Quality/Water Pollution</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ajala, Mary Adejoke</creatorcontrib><creatorcontrib>Abdulkareem, Ambali Saka</creatorcontrib><creatorcontrib>Kovo, Abdulsalami Sanni</creatorcontrib><creatorcontrib>Tijani, Jimoh Oladejo</creatorcontrib><creatorcontrib>Ajala, Elijah 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pollution</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ajala, Mary Adejoke</au><au>Abdulkareem, Ambali Saka</au><au>Kovo, Abdulsalami Sanni</au><au>Tijani, Jimoh Oladejo</au><au>Ajala, Elijah Olawale</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Ag2O-TiO2-Kaolinite Clay Nanocomposite for Efficient Removal of Mn2+, Fe3+, Cu2+, and Pb2+ and Pathogens in Mining Wastewater</atitle><jtitle>Water, air, and soil pollution</jtitle><stitle>Water Air Soil Pollut</stitle><date>2024</date><risdate>2024</risdate><volume>235</volume><issue>1</issue><spage>42</spage><epage>42</epage><pages>42-42</pages><artnum>42</artnum><issn>0049-6979</issn><eissn>1573-2932</eissn><abstract>Synthesis of Ag
2
O-TiO
2
-kaolinite clay nanocomposite was undertaken to eliminate some selected heavy metals released into the environment from mining wastewater. Silver nitrate and titanium-tetra-isopropoxide were employed as the bulk reagents for the Ag
2
O-TiO
2
nanoparticles synthesis, using an aqueous extract of
Parkia biglobossa
leaf (green synthesis method)
.
The Ag
2
O-TiO
2
nanoparticles were supported on acid-activated kaolinite clay via wet impregnation method, to develop the nanocomposite and were characterized for phase structure, morphology, and oxidation states. The functionality of the nanocomposite for the sequestration of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions from mining wastewater was examined by adsorption studies. The XRD pattern of the Ag
2
O-TiO
2
-kaolinite clay reveals the synthesis of the rutile phase of TiO
2
embedded in the kaolinite clay. While the HRSEM shows an evenly distributed arrangement of hemispherical stacks of kaolinites. The oxidation states of Ag
2
O and TiO
2
revealed by the XPS are + 1 and + 4 respectively either as binary or ternary nanocomposite. The Ag
2
O-TiO
2
-clay nanocomposite adsorbed 99.85%, 97.85% 95.18%, and 40% of Mn
2+
, Fe
3+
, Cu
2+
, and Pb
2+
ions at 120 min from the mining wastewater respectively. The synergetic efforts of the Ag
2
O-TiO
2
-clay were responsible for the adsorptive capability of the nanocomposite for the removal of the selected heavy metal ions.
Graphical abstract</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s11270-023-06811-w</doi><tpages>1</tpages><orcidid>https://orcid.org/0009-0006-5346-4783</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0049-6979 |
| ispartof | Water, air, and soil pollution, 2024, Vol.235 (1), p.42-42, Article 42 |
| issn | 0049-6979 1573-2932 |
| language | eng |
| recordid | cdi_proquest_journals_2907587178 |
| source | SpringerLink Journals |
| subjects | Activated clay adsorption Adsorptivity air Atmospheric Protection/Air Quality Control/Air Pollution Clay Climate Change/Climate Change Impacts Copper Earth and Environmental Science Environment Environmental monitoring Ferric ions Heavy metals Hydrogeology Iron Kaolinite Lead leaves Metal ions Nanocomposites Nanoparticles Oxidation Parkia Pathogens Reagents Removal Rutile Silver Silver nitrate soil Soil Science & Conservation Solid phases Synthesis Titanium Titanium dioxide Wastewater water Water Quality/Water Pollution |
| title | Synthesis of Ag2O-TiO2-Kaolinite Clay Nanocomposite for Efficient Removal of Mn2+, Fe3+, Cu2+, and Pb2+ and Pathogens in Mining Wastewater |
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