Effect of ZrSnO4 solid solution on the crystallization behavior of Li2O–Al2O3–SiO2 glasses
Herein, the crystallization behavior of a Li2O–Al2O3–SiO2 (LAS) glass system with the addition of ZrO2 and SnO2 as nucleating agents was investigated using X‐ray diffraction, differential scanning calorimetry, four‐dimensional scanning transmission electron microscopy, and X‐ray absorption fine‐stru...
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| Veröffentlicht in: | International journal of applied glass science 2024-01, Vol.15 (1), p.31-43 |
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| container_title | International journal of applied glass science |
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| creator | Kajihara, Takato Hijiya, Hiroyuki Yoshida, Satoshi Ninomiya, Kakeru Nishibori, Maiko Saito, Hikaru Fujino, Shigeru Hata, Satoshi |
| description | Herein, the crystallization behavior of a Li2O–Al2O3–SiO2 (LAS) glass system with the addition of ZrO2 and SnO2 as nucleating agents was investigated using X‐ray diffraction, differential scanning calorimetry, four‐dimensional scanning transmission electron microscopy, and X‐ray absorption fine‐structure measurements. At lower heat‐treatment temperatures, the addition of ZrO2 and SnO2 afforded a ZrSnO4 solid solution (SS), whereas at higher heat‐treatment temperatures, the ZrSnO4 SS decomposed, affording tetragonal ZrO2 and tetragonal SnO2. LAS‐based crystalline phases, such as β‐quartz and β‐spodumene phases SS, were formed after the formation of the ZrSnO4 SS. ZrSnO4 SS particles a few nanometers in size were present in contact with the β‐quartz SS particles a few dozen nanometers in size. This suggests that the ZrSnO4 SS served as a crystal nucleus for the β‐quartz SS, promoting its growth. |
| doi_str_mv | 10.1111/ijag.16644 |
| format | Article |
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At lower heat‐treatment temperatures, the addition of ZrO2 and SnO2 afforded a ZrSnO4 solid solution (SS), whereas at higher heat‐treatment temperatures, the ZrSnO4 SS decomposed, affording tetragonal ZrO2 and tetragonal SnO2. LAS‐based crystalline phases, such as β‐quartz and β‐spodumene phases SS, were formed after the formation of the ZrSnO4 SS. ZrSnO4 SS particles a few nanometers in size were present in contact with the β‐quartz SS particles a few dozen nanometers in size. This suggests that the ZrSnO4 SS served as a crystal nucleus for the β‐quartz SS, promoting its growth.</description><identifier>ISSN: 2041-1286</identifier><identifier>EISSN: 2041-1294</identifier><identifier>DOI: 10.1111/ijag.16644</identifier><language>eng</language><publisher>Westerville: Wiley Subscription Services, Inc</publisher><subject>4D‐STEM ; Aluminum oxide ; Crystallization ; DSC ; Heat treatment ; Li2O–Al2O3–SiO2 glass ceramics ; Lithium oxides ; Quartz ; Reagents ; Scanning transmission electron microscopy ; Silicon dioxide ; Solid solutions ; Spodumene ; Tin dioxide ; XAFS ; XRD ; Zirconium dioxide ; ZrSnO4</subject><ispartof>International journal of applied glass science, 2024-01, Vol.15 (1), p.31-43</ispartof><rights>2023 The American Ceramic Society and Wiley Periodicals LLC.</rights><rights>2024 The American Ceramic Society and Wiley Periodicals LLC.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><orcidid>0000-0002-5231-4605 ; 0000-0002-1131-8650</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Fijag.16644$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Fijag.16644$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids></links><search><creatorcontrib>Kajihara, Takato</creatorcontrib><creatorcontrib>Hijiya, Hiroyuki</creatorcontrib><creatorcontrib>Yoshida, Satoshi</creatorcontrib><creatorcontrib>Ninomiya, Kakeru</creatorcontrib><creatorcontrib>Nishibori, Maiko</creatorcontrib><creatorcontrib>Saito, Hikaru</creatorcontrib><creatorcontrib>Fujino, Shigeru</creatorcontrib><creatorcontrib>Hata, Satoshi</creatorcontrib><title>Effect of ZrSnO4 solid solution on the crystallization behavior of Li2O–Al2O3–SiO2 glasses</title><title>International journal of applied glass science</title><description>Herein, the crystallization behavior of a Li2O–Al2O3–SiO2 (LAS) glass system with the addition of ZrO2 and SnO2 as nucleating agents was investigated using X‐ray diffraction, differential scanning calorimetry, four‐dimensional scanning transmission electron microscopy, and X‐ray absorption fine‐structure measurements. At lower heat‐treatment temperatures, the addition of ZrO2 and SnO2 afforded a ZrSnO4 solid solution (SS), whereas at higher heat‐treatment temperatures, the ZrSnO4 SS decomposed, affording tetragonal ZrO2 and tetragonal SnO2. LAS‐based crystalline phases, such as β‐quartz and β‐spodumene phases SS, were formed after the formation of the ZrSnO4 SS. ZrSnO4 SS particles a few nanometers in size were present in contact with the β‐quartz SS particles a few dozen nanometers in size. This suggests that the ZrSnO4 SS served as a crystal nucleus for the β‐quartz SS, promoting its growth.</description><subject>4D‐STEM</subject><subject>Aluminum oxide</subject><subject>Crystallization</subject><subject>DSC</subject><subject>Heat treatment</subject><subject>Li2O–Al2O3–SiO2 glass ceramics</subject><subject>Lithium oxides</subject><subject>Quartz</subject><subject>Reagents</subject><subject>Scanning transmission electron microscopy</subject><subject>Silicon dioxide</subject><subject>Solid solutions</subject><subject>Spodumene</subject><subject>Tin dioxide</subject><subject>XAFS</subject><subject>XRD</subject><subject>Zirconium dioxide</subject><subject>ZrSnO4</subject><issn>2041-1286</issn><issn>2041-1294</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNo9UE1PAjEQbYwmEuTiL9jE82K_dtseCUHEkOwBvXiwKbSFkspiu2jWk__Bf-gvsQvGyWTey8ybmeQBcI3gEKW4dVu1HqKypPQM9DCkKEdY0PN_zstLMIhxC1MQzkvBe-BlYq1ZNVlts-ew2FU0i7V3uquHxtW7LGWzMdkqtLFR3rtPdWwvzUa9uzp0i3OHq5-v75HHFUm4cBXO1l7FaOIVuLDKRzP4wz54ups8ju_zeTWdjUfzfI9xQXMrRME0pKoslIBca1VYpCg3jBBrNUOMWYhX2EDNOElTREoBWUn1EhG6NKQPbk5396F-O5jYyG19CLv0UmIuCs4EJTip0En14bxp5T64VxVaiaDs_JOdf_Lon5w9jKZHRn4BPs5lyg</recordid><startdate>202401</startdate><enddate>202401</enddate><creator>Kajihara, Takato</creator><creator>Hijiya, Hiroyuki</creator><creator>Yoshida, Satoshi</creator><creator>Ninomiya, Kakeru</creator><creator>Nishibori, Maiko</creator><creator>Saito, Hikaru</creator><creator>Fujino, Shigeru</creator><creator>Hata, Satoshi</creator><general>Wiley Subscription Services, Inc</general><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0002-5231-4605</orcidid><orcidid>https://orcid.org/0000-0002-1131-8650</orcidid></search><sort><creationdate>202401</creationdate><title>Effect of ZrSnO4 solid solution on the crystallization behavior of Li2O–Al2O3–SiO2 glasses</title><author>Kajihara, Takato ; Hijiya, Hiroyuki ; Yoshida, Satoshi ; Ninomiya, Kakeru ; Nishibori, Maiko ; Saito, Hikaru ; Fujino, Shigeru ; Hata, Satoshi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p2254-f9957d04a65a908dda5f1a48e733ffd7177f02c2e0d783da513690764db134be3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>4D‐STEM</topic><topic>Aluminum oxide</topic><topic>Crystallization</topic><topic>DSC</topic><topic>Heat treatment</topic><topic>Li2O–Al2O3–SiO2 glass ceramics</topic><topic>Lithium oxides</topic><topic>Quartz</topic><topic>Reagents</topic><topic>Scanning transmission electron microscopy</topic><topic>Silicon dioxide</topic><topic>Solid solutions</topic><topic>Spodumene</topic><topic>Tin dioxide</topic><topic>XAFS</topic><topic>XRD</topic><topic>Zirconium dioxide</topic><topic>ZrSnO4</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kajihara, Takato</creatorcontrib><creatorcontrib>Hijiya, Hiroyuki</creatorcontrib><creatorcontrib>Yoshida, Satoshi</creatorcontrib><creatorcontrib>Ninomiya, Kakeru</creatorcontrib><creatorcontrib>Nishibori, Maiko</creatorcontrib><creatorcontrib>Saito, Hikaru</creatorcontrib><creatorcontrib>Fujino, Shigeru</creatorcontrib><creatorcontrib>Hata, Satoshi</creatorcontrib><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>International journal of applied glass science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kajihara, Takato</au><au>Hijiya, Hiroyuki</au><au>Yoshida, Satoshi</au><au>Ninomiya, Kakeru</au><au>Nishibori, Maiko</au><au>Saito, Hikaru</au><au>Fujino, Shigeru</au><au>Hata, Satoshi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of ZrSnO4 solid solution on the crystallization behavior of Li2O–Al2O3–SiO2 glasses</atitle><jtitle>International journal of applied glass science</jtitle><date>2024-01</date><risdate>2024</risdate><volume>15</volume><issue>1</issue><spage>31</spage><epage>43</epage><pages>31-43</pages><issn>2041-1286</issn><eissn>2041-1294</eissn><abstract>Herein, the crystallization behavior of a Li2O–Al2O3–SiO2 (LAS) glass system with the addition of ZrO2 and SnO2 as nucleating agents was investigated using X‐ray diffraction, differential scanning calorimetry, four‐dimensional scanning transmission electron microscopy, and X‐ray absorption fine‐structure measurements. At lower heat‐treatment temperatures, the addition of ZrO2 and SnO2 afforded a ZrSnO4 solid solution (SS), whereas at higher heat‐treatment temperatures, the ZrSnO4 SS decomposed, affording tetragonal ZrO2 and tetragonal SnO2. LAS‐based crystalline phases, such as β‐quartz and β‐spodumene phases SS, were formed after the formation of the ZrSnO4 SS. ZrSnO4 SS particles a few nanometers in size were present in contact with the β‐quartz SS particles a few dozen nanometers in size. This suggests that the ZrSnO4 SS served as a crystal nucleus for the β‐quartz SS, promoting its growth.</abstract><cop>Westerville</cop><pub>Wiley Subscription Services, Inc</pub><doi>10.1111/ijag.16644</doi><tpages>13</tpages><orcidid>https://orcid.org/0000-0002-5231-4605</orcidid><orcidid>https://orcid.org/0000-0002-1131-8650</orcidid></addata></record> |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | 4D‐STEM Aluminum oxide Crystallization DSC Heat treatment Li2O–Al2O3–SiO2 glass ceramics Lithium oxides Quartz Reagents Scanning transmission electron microscopy Silicon dioxide Solid solutions Spodumene Tin dioxide XAFS XRD Zirconium dioxide ZrSnO4 |
| title | Effect of ZrSnO4 solid solution on the crystallization behavior of Li2O–Al2O3–SiO2 glasses |
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