Lamb–Mössbauer factor of powders determined by Mössbauer spectroscopy with resonant detector
The Lamb–Mössbauer factor is a crucial material parameter for the proper quantitative analysis of Mössbauer experiments. We report on a method for determining the Lamb–Mössbauer factor of powdered samples. It utilizes a resonant Mössbauer spectrometer together with a customized sample preparation, w...
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| Veröffentlicht in: | Chemical papers 2023-12, Vol.77 (12), p.7283-7288 |
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| creator | Novák, Petr Schlattauerová, Tereza Procházka, Vít Kopp, Josef Vrba, Vlastimil |
| description | The Lamb–Mössbauer factor is a crucial material parameter for the proper quantitative analysis of Mössbauer experiments. We report on a method for determining the Lamb–Mössbauer factor of powdered samples. It utilizes a resonant Mössbauer spectrometer together with a customized sample preparation, which ensures a homogeneous thickness of the powdered absorbers. Compared with other methods of Lamb‒Mössbauer factor determination, the presented approach is direct and requires only a single Mössbauer measurement. To demonstrate this method, the Lamb–Mössbauer factor of iron(II) oxalate dihydrate samples with varying thickness was measured. The resulting value of the Lamb–Mössbauer factor was 0.38 ± 0.03. The presented approach can be used for a large variety of powdered materials. |
| doi_str_mv | 10.1007/s11696-023-02844-x |
| format | Article |
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| source | SpringerNature Journals |
| subjects | Biochemistry Biotechnology Chemistry Chemistry and Materials Science Chemistry/Food Science Industrial Chemistry/Chemical Engineering Materials Science Medicinal Chemistry Mossbauer spectroscopy Original Paper Thickness measurement |
| title | Lamb–Mössbauer factor of powders determined by Mössbauer spectroscopy with resonant detector |
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