Photocatalytic Degradation of Toxic Dyes and Antimicrobial Activities by Cadmium Doped Magnesium Ferrites Synthesized by Combustion Method
The structural properties of nanocrystalline spinel ferrites with chemical formula Mg 0.8−x Cd x Fe 2 O 4 (x = 0.2, 0.4 and 0.6) prepared by combustion method and characterized by XRD, FTIR, SEM, EDX, TEM and UV studies. The X-ray diffraction (XRD) measurements confirmed the formation of a cubic spi...
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| Veröffentlicht in: | Journal of inorganic and organometallic polymers and materials 2023-10, Vol.33 (10), p.3087-3104 |
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| container_title | Journal of inorganic and organometallic polymers and materials |
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| creator | Bessy, T. C. Gatasheh, Mansour K. Hatamleh, Ashraf Atef Arokiyaraj, Selvaraj Johnson, J. Bindhu, M. R. |
| description | The structural properties of nanocrystalline spinel ferrites with chemical formula Mg
0.8−x
Cd
x
Fe
2
O
4
(x = 0.2, 0.4 and 0.6) prepared by combustion method and characterized by XRD, FTIR, SEM, EDX, TEM and UV studies. The X-ray diffraction (XRD) measurements confirmed the formation of a cubic spinel structure with space group Fd3m. Fourier transform infrared (FTIR) spectroscopy confirmed the existence of metal oxygen (M–O) bonding in the prepared samples. Absorption bands observed in FTIR spectra around 590 cm
−1
and 434 cm
−1
corresponds to vibrations of tetrahedral and octahedral complexes respectively. Scanning electron microscopic (SEM) analysis of surface morphology revealed irregular agglomeration of ferrite particles. The elemental compositions of the prepared NPs were analysed by EDX. TEM studies reveal the formation of spherical nanoparticles with agglomeration. The UV–visible study showed the optical band gaps decreased from 4.4 to 3.6 eV with increasing Cd
2+
doping. The photocatalytic reduction of Methylene Blue (MB) and Congo Red (CR) was also investigated using the prepared nanocatalysts. CR was more effectively degraded as compared to MB. Antibacterial results showed the activity against
Pseudomonas aeruginosa, Staphylococcus aureus, Candida albicans
and
Aspergillus Flaves.
All ferrite nanoparticles showed antimicrobial activity toward all pathogens selected. Of these, the most powerful was Cd
0.2
Mg
0.6
Fe
2
O
4
, showing zone of inhibition of 32 mm against
P. aeruginosa
. |
| doi_str_mv | 10.1007/s10904-023-02716-7 |
| format | Article |
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0.8−x
Cd
x
Fe
2
O
4
(x = 0.2, 0.4 and 0.6) prepared by combustion method and characterized by XRD, FTIR, SEM, EDX, TEM and UV studies. The X-ray diffraction (XRD) measurements confirmed the formation of a cubic spinel structure with space group Fd3m. Fourier transform infrared (FTIR) spectroscopy confirmed the existence of metal oxygen (M–O) bonding in the prepared samples. Absorption bands observed in FTIR spectra around 590 cm
−1
and 434 cm
−1
corresponds to vibrations of tetrahedral and octahedral complexes respectively. Scanning electron microscopic (SEM) analysis of surface morphology revealed irregular agglomeration of ferrite particles. The elemental compositions of the prepared NPs were analysed by EDX. TEM studies reveal the formation of spherical nanoparticles with agglomeration. The UV–visible study showed the optical band gaps decreased from 4.4 to 3.6 eV with increasing Cd
2+
doping. The photocatalytic reduction of Methylene Blue (MB) and Congo Red (CR) was also investigated using the prepared nanocatalysts. CR was more effectively degraded as compared to MB. Antibacterial results showed the activity against
Pseudomonas aeruginosa, Staphylococcus aureus, Candida albicans
and
Aspergillus Flaves.
All ferrite nanoparticles showed antimicrobial activity toward all pathogens selected. Of these, the most powerful was Cd
0.2
Mg
0.6
Fe
2
O
4
, showing zone of inhibition of 32 mm against
P. aeruginosa
.</description><identifier>ISSN: 1574-1443</identifier><identifier>EISSN: 1574-1451</identifier><identifier>DOI: 10.1007/s10904-023-02716-7</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Absorption spectra ; Agglomeration ; Antimicrobial agents ; Chemistry ; Chemistry and Materials Science ; Combustion ; Fourier transforms ; Infrared spectroscopy ; Inorganic Chemistry ; Magnesium ferrites ; Methylene blue ; Nanoparticles ; Organic Chemistry ; Photocatalysis ; Photodegradation ; Polymer Sciences ; Pseudomonas aeruginosa ; Scanning electron microscopy ; Spectrum analysis ; Spinel ; X-ray diffraction</subject><ispartof>Journal of inorganic and organometallic polymers and materials, 2023-10, Vol.33 (10), p.3087-3104</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-a69346ae8f3b44cdc4832b4b5c88ee508ed5b61b809e53f1395d79df184518073</citedby><cites>FETCH-LOGICAL-c319t-a69346ae8f3b44cdc4832b4b5c88ee508ed5b61b809e53f1395d79df184518073</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10904-023-02716-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10904-023-02716-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Bessy, T. C.</creatorcontrib><creatorcontrib>Gatasheh, Mansour K.</creatorcontrib><creatorcontrib>Hatamleh, Ashraf Atef</creatorcontrib><creatorcontrib>Arokiyaraj, Selvaraj</creatorcontrib><creatorcontrib>Johnson, J.</creatorcontrib><creatorcontrib>Bindhu, M. R.</creatorcontrib><title>Photocatalytic Degradation of Toxic Dyes and Antimicrobial Activities by Cadmium Doped Magnesium Ferrites Synthesized by Combustion Method</title><title>Journal of inorganic and organometallic polymers and materials</title><addtitle>J Inorg Organomet Polym</addtitle><description>The structural properties of nanocrystalline spinel ferrites with chemical formula Mg
0.8−x
Cd
x
Fe
2
O
4
(x = 0.2, 0.4 and 0.6) prepared by combustion method and characterized by XRD, FTIR, SEM, EDX, TEM and UV studies. The X-ray diffraction (XRD) measurements confirmed the formation of a cubic spinel structure with space group Fd3m. Fourier transform infrared (FTIR) spectroscopy confirmed the existence of metal oxygen (M–O) bonding in the prepared samples. Absorption bands observed in FTIR spectra around 590 cm
−1
and 434 cm
−1
corresponds to vibrations of tetrahedral and octahedral complexes respectively. Scanning electron microscopic (SEM) analysis of surface morphology revealed irregular agglomeration of ferrite particles. The elemental compositions of the prepared NPs were analysed by EDX. TEM studies reveal the formation of spherical nanoparticles with agglomeration. The UV–visible study showed the optical band gaps decreased from 4.4 to 3.6 eV with increasing Cd
2+
doping. The photocatalytic reduction of Methylene Blue (MB) and Congo Red (CR) was also investigated using the prepared nanocatalysts. CR was more effectively degraded as compared to MB. Antibacterial results showed the activity against
Pseudomonas aeruginosa, Staphylococcus aureus, Candida albicans
and
Aspergillus Flaves.
All ferrite nanoparticles showed antimicrobial activity toward all pathogens selected. Of these, the most powerful was Cd
0.2
Mg
0.6
Fe
2
O
4
, showing zone of inhibition of 32 mm against
P. aeruginosa
.</description><subject>Absorption spectra</subject><subject>Agglomeration</subject><subject>Antimicrobial agents</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Combustion</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Inorganic Chemistry</subject><subject>Magnesium ferrites</subject><subject>Methylene blue</subject><subject>Nanoparticles</subject><subject>Organic Chemistry</subject><subject>Photocatalysis</subject><subject>Photodegradation</subject><subject>Polymer Sciences</subject><subject>Pseudomonas aeruginosa</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Spinel</subject><subject>X-ray diffraction</subject><issn>1574-1443</issn><issn>1574-1451</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kF1PwyAUhonRxDn9A16ReF2FAi29XDa_ki2aOK8JLXRjWcsEZqw_wV8tXY3eeXHC-XjOe8ILwCVG1xih_MZjVCCaoJTEyHGW5EdghFlOE0wZPv7NKTkFZ95vECIcMTwCX89rG2wlg9x2wVRwpldOKhmMbaGt4dJ-9M1OeyhbBSdtMI2pnC2N3MJJFcy7CSYOyw5OpWrMvoEzu9MKLuSq1b6v77RzJkTmpWvDOvY-47jnbVPu_eHQQoe1VefgpJZbry9-3jF4vbtdTh-S-dP943QyTyqCi5DIrCA0k5rXpKS0UhXlJC1pySrOtWaIa8XKDJccFZqRGpOCqbxQNebRCY5yMgZXg-7O2be99kFs7N618aRIeZ4xhHjKI5UOVPyt907XYudMI10nMBK952LwXETPxcFz0UuTYclHuF1p9yf9z9Y3MJiGYQ</recordid><startdate>20231001</startdate><enddate>20231001</enddate><creator>Bessy, T. C.</creator><creator>Gatasheh, Mansour K.</creator><creator>Hatamleh, Ashraf Atef</creator><creator>Arokiyaraj, Selvaraj</creator><creator>Johnson, J.</creator><creator>Bindhu, M. R.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20231001</creationdate><title>Photocatalytic Degradation of Toxic Dyes and Antimicrobial Activities by Cadmium Doped Magnesium Ferrites Synthesized by Combustion Method</title><author>Bessy, T. C. ; Gatasheh, Mansour K. ; Hatamleh, Ashraf Atef ; Arokiyaraj, Selvaraj ; Johnson, J. ; Bindhu, M. R.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-a69346ae8f3b44cdc4832b4b5c88ee508ed5b61b809e53f1395d79df184518073</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Absorption spectra</topic><topic>Agglomeration</topic><topic>Antimicrobial agents</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Combustion</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Inorganic Chemistry</topic><topic>Magnesium ferrites</topic><topic>Methylene blue</topic><topic>Nanoparticles</topic><topic>Organic Chemistry</topic><topic>Photocatalysis</topic><topic>Photodegradation</topic><topic>Polymer Sciences</topic><topic>Pseudomonas aeruginosa</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Spinel</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bessy, T. C.</creatorcontrib><creatorcontrib>Gatasheh, Mansour K.</creatorcontrib><creatorcontrib>Hatamleh, Ashraf Atef</creatorcontrib><creatorcontrib>Arokiyaraj, Selvaraj</creatorcontrib><creatorcontrib>Johnson, J.</creatorcontrib><creatorcontrib>Bindhu, M. R.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of inorganic and organometallic polymers and materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bessy, T. C.</au><au>Gatasheh, Mansour K.</au><au>Hatamleh, Ashraf Atef</au><au>Arokiyaraj, Selvaraj</au><au>Johnson, J.</au><au>Bindhu, M. R.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Photocatalytic Degradation of Toxic Dyes and Antimicrobial Activities by Cadmium Doped Magnesium Ferrites Synthesized by Combustion Method</atitle><jtitle>Journal of inorganic and organometallic polymers and materials</jtitle><stitle>J Inorg Organomet Polym</stitle><date>2023-10-01</date><risdate>2023</risdate><volume>33</volume><issue>10</issue><spage>3087</spage><epage>3104</epage><pages>3087-3104</pages><issn>1574-1443</issn><eissn>1574-1451</eissn><abstract>The structural properties of nanocrystalline spinel ferrites with chemical formula Mg
0.8−x
Cd
x
Fe
2
O
4
(x = 0.2, 0.4 and 0.6) prepared by combustion method and characterized by XRD, FTIR, SEM, EDX, TEM and UV studies. The X-ray diffraction (XRD) measurements confirmed the formation of a cubic spinel structure with space group Fd3m. Fourier transform infrared (FTIR) spectroscopy confirmed the existence of metal oxygen (M–O) bonding in the prepared samples. Absorption bands observed in FTIR spectra around 590 cm
−1
and 434 cm
−1
corresponds to vibrations of tetrahedral and octahedral complexes respectively. Scanning electron microscopic (SEM) analysis of surface morphology revealed irregular agglomeration of ferrite particles. The elemental compositions of the prepared NPs were analysed by EDX. TEM studies reveal the formation of spherical nanoparticles with agglomeration. The UV–visible study showed the optical band gaps decreased from 4.4 to 3.6 eV with increasing Cd
2+
doping. The photocatalytic reduction of Methylene Blue (MB) and Congo Red (CR) was also investigated using the prepared nanocatalysts. CR was more effectively degraded as compared to MB. Antibacterial results showed the activity against
Pseudomonas aeruginosa, Staphylococcus aureus, Candida albicans
and
Aspergillus Flaves.
All ferrite nanoparticles showed antimicrobial activity toward all pathogens selected. Of these, the most powerful was Cd
0.2
Mg
0.6
Fe
2
O
4
, showing zone of inhibition of 32 mm against
P. aeruginosa
.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10904-023-02716-7</doi><tpages>18</tpages></addata></record> |
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| subjects | Absorption spectra Agglomeration Antimicrobial agents Chemistry Chemistry and Materials Science Combustion Fourier transforms Infrared spectroscopy Inorganic Chemistry Magnesium ferrites Methylene blue Nanoparticles Organic Chemistry Photocatalysis Photodegradation Polymer Sciences Pseudomonas aeruginosa Scanning electron microscopy Spectrum analysis Spinel X-ray diffraction |
| title | Photocatalytic Degradation of Toxic Dyes and Antimicrobial Activities by Cadmium Doped Magnesium Ferrites Synthesized by Combustion Method |
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