Lattice strain visualization inside a 400 nm single grain of BaTiO3 in polycrystalline ceramics by Bragg coherent X-ray diffraction imaging
The degree of anisotropy and the domain arrangement of crystal structures in ferroelectrics are affected by the grain boundaries and by the shape and size of the grains. To understand the grain boundary effects that occur in ferroelectric ceramics, we introduce a technique for nondestructively obser...
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| Veröffentlicht in: | Japanese Journal of Applied Physics 2023-11, Vol.62 (SM), p.SM1022 |
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| container_title | Japanese Journal of Applied Physics |
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| creator | Oshime, Norihiro Ohwada, Kenji Machida, Akihiko Fukushima, Nagise Shirakawa, Kosuke Ueno, Shintaro Fujii, Ichiro Wada, Satoshi Sugawara, Kento Shimada, Ayumu Ueno, Tetsuro Watanuki, Tetsu Ishii, Kenji Toyokawa, Hidenori Momma, Koichi Kim, Sangwook Tsukada, Shinya Kuroiwa, Yoshihiro |
| description | The degree of anisotropy and the domain arrangement of crystal structures in ferroelectrics are affected by the grain boundaries and by the shape and size of the grains. To understand the grain boundary effects that occur in ferroelectric ceramics, we introduce a technique for nondestructively observing the internal lattice strain distribution of a submicrometer-sized ferroelectric grain in polycrystalline materials. The ferroelectric phase transition of a single grain in the polycrystalline materials was evaluated by tracking the changes in the Bragg coherent X-ray diffraction (CXD) patterns. The internal lattice strain distribution of the grains in the paraelectric phase was visualized via Bragg CXD imaging. A pair of 90° domains in the ferroelectric phase were also imaged in three dimensions, and showed a domain boundary correlated with the internal lattice strain caused by the stresses from the adjacent grains. |
| doi_str_mv | 10.35848/1347-4065/ace832 |
| format | Article |
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To understand the grain boundary effects that occur in ferroelectric ceramics, we introduce a technique for nondestructively observing the internal lattice strain distribution of a submicrometer-sized ferroelectric grain in polycrystalline materials. The ferroelectric phase transition of a single grain in the polycrystalline materials was evaluated by tracking the changes in the Bragg coherent X-ray diffraction (CXD) patterns. The internal lattice strain distribution of the grains in the paraelectric phase was visualized via Bragg CXD imaging. 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J. Appl. Phys</addtitle><description>The degree of anisotropy and the domain arrangement of crystal structures in ferroelectrics are affected by the grain boundaries and by the shape and size of the grains. To understand the grain boundary effects that occur in ferroelectric ceramics, we introduce a technique for nondestructively observing the internal lattice strain distribution of a submicrometer-sized ferroelectric grain in polycrystalline materials. The ferroelectric phase transition of a single grain in the polycrystalline materials was evaluated by tracking the changes in the Bragg coherent X-ray diffraction (CXD) patterns. The internal lattice strain distribution of the grains in the paraelectric phase was visualized via Bragg CXD imaging. 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| ispartof | Japanese Journal of Applied Physics, 2023-11, Vol.62 (SM), p.SM1022 |
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| source | IOP Publishing Journals; Institute of Physics (IOP) Journals - HEAL-Link |
| subjects | Anisotropy Barium titanates Ceramics coherent X-ray diffraction Diffraction patterns Ferroelectric materials Ferroelectricity ferroelectrics Grain boundaries grain boundary imaging Lattice strain Phase transitions Polycrystals Strain distribution X ray imagery X-ray diffraction |
| title | Lattice strain visualization inside a 400 nm single grain of BaTiO3 in polycrystalline ceramics by Bragg coherent X-ray diffraction imaging |
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