Extraction and characterization of lignin from waste invasive weeds with dioxane-based process
This study has put forth the concept of “control through utilization” for invasive weeds, which cause severe damage to ecosystem and biodiversity. The study comprised of extraction of lignin and pretreatment of spent biomass of four invasive weeds. Lignin was extracted from native biomass using 1,4–...
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| Veröffentlicht in: | Biomass conversion and biorefinery 2023-08, Vol.13 (12), p.11121-11130 |
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| container_title | Biomass conversion and biorefinery |
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| creator | Borah, Arup Jyoti Dikshit, Pritam Kumar Doloi, Moumita Moholkar, Vijayanand S. Poddar, Maneesh Kumar |
| description | This study has put forth the concept of “control through utilization” for invasive weeds, which cause severe damage to ecosystem and biodiversity. The study comprised of extraction of lignin and pretreatment of spent biomass of four invasive weeds. Lignin was extracted from native biomass using 1,4–dioxane as solvent. Lignin yield of all biomass varied in the range 8.61 − 11.14% w/w with the solvent recovery of 75.56–78.88% v/v. Extracted lignin was characterized using FTIR, TGA, and GPC. Lignin from
Mikania micrantha
had the highest thermal stability (T
50%
= 490 °C) and molecular weight (M
w
= 5537 g/mol). The spent biomass was subjected to dilute acid pretreatment for synthesis of total reducing sugars (TRS). TRS yields from different entities were as follows: non-extracted biomass = 94.18 − 221.81 mg/g, warm water wash = 8.74 − 15.66 mg/g, and raw biomass = 115.9 − 391.27 mg/g raw biomass. Biomass of
Saccharum spontaneum
gave the highest TRS yield.
Graphical abstract |
| doi_str_mv | 10.1007/s13399-021-01960-6 |
| format | Article |
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Mikania micrantha
had the highest thermal stability (T
50%
= 490 °C) and molecular weight (M
w
= 5537 g/mol). The spent biomass was subjected to dilute acid pretreatment for synthesis of total reducing sugars (TRS). TRS yields from different entities were as follows: non-extracted biomass = 94.18 − 221.81 mg/g, warm water wash = 8.74 − 15.66 mg/g, and raw biomass = 115.9 − 391.27 mg/g raw biomass. Biomass of
Saccharum spontaneum
gave the highest TRS yield.
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Mikania micrantha
had the highest thermal stability (T
50%
= 490 °C) and molecular weight (M
w
= 5537 g/mol). The spent biomass was subjected to dilute acid pretreatment for synthesis of total reducing sugars (TRS). TRS yields from different entities were as follows: non-extracted biomass = 94.18 − 221.81 mg/g, warm water wash = 8.74 − 15.66 mg/g, and raw biomass = 115.9 − 391.27 mg/g raw biomass. Biomass of
Saccharum spontaneum
gave the highest TRS yield.
Graphical abstract</description><subject>Biodiversity</subject><subject>Biomass</subject><subject>Biotechnology</subject><subject>Energy</subject><subject>Lignin</subject><subject>Original Article</subject><subject>Pretreatment</subject><subject>Renewable and Green Energy</subject><subject>Solvents</subject><subject>Thermal stability</subject><subject>Warm water</subject><subject>Weeds</subject><issn>2190-6815</issn><issn>2190-6823</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kEtPwzAQhC0EElXpH-BkiXNgbedhH1FVHlIlLnDFcpJ166p1ip02hV9P2iC4cdrZ1cyO9BFyzeCWARR3kQmhVAKcJcBUDkl-RkacqV5ILs5_NcsuySTGFQBwUQgpYETeZ4c2mKp1jafG17RamuOKwX2Z07GxdO0W3nlqQ7OhnYktUuf3Jro90g6xjrRz7ZLWrjkYj0lpItZ0G5oKY7wiF9asI05-5pi8Pcxep0_J_OXxeXo_TyrBVJvICgwAKywqm9U5rwqRZrJUuUVhhaiNAuRlyW0qIU9rzHgpeCllatKUoWJiTG6Gv33vxw5jq1fNLvi-UnOZSiWZKKB38cFVhSbGgFZvg9uY8KkZ6CNKPaDUPUp9QqnzPiSGUOzNfoHh7_U_qW9VFXdX</recordid><startdate>20230801</startdate><enddate>20230801</enddate><creator>Borah, Arup Jyoti</creator><creator>Dikshit, Pritam Kumar</creator><creator>Doloi, Moumita</creator><creator>Moholkar, Vijayanand S.</creator><creator>Poddar, Maneesh Kumar</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20230801</creationdate><title>Extraction and characterization of lignin from waste invasive weeds with dioxane-based process</title><author>Borah, Arup Jyoti ; Dikshit, Pritam Kumar ; Doloi, Moumita ; Moholkar, Vijayanand S. ; Poddar, Maneesh Kumar</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-8c0a0017fe9f5d62c73458b96fe3f33da90e2bb2f48064de52b32b884a441e913</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Biodiversity</topic><topic>Biomass</topic><topic>Biotechnology</topic><topic>Energy</topic><topic>Lignin</topic><topic>Original Article</topic><topic>Pretreatment</topic><topic>Renewable and Green Energy</topic><topic>Solvents</topic><topic>Thermal stability</topic><topic>Warm water</topic><topic>Weeds</topic><toplevel>online_resources</toplevel><creatorcontrib>Borah, Arup Jyoti</creatorcontrib><creatorcontrib>Dikshit, Pritam Kumar</creatorcontrib><creatorcontrib>Doloi, Moumita</creatorcontrib><creatorcontrib>Moholkar, Vijayanand S.</creatorcontrib><creatorcontrib>Poddar, Maneesh Kumar</creatorcontrib><collection>CrossRef</collection><jtitle>Biomass conversion and biorefinery</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Borah, Arup Jyoti</au><au>Dikshit, Pritam Kumar</au><au>Doloi, Moumita</au><au>Moholkar, Vijayanand S.</au><au>Poddar, Maneesh Kumar</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Extraction and characterization of lignin from waste invasive weeds with dioxane-based process</atitle><jtitle>Biomass conversion and biorefinery</jtitle><stitle>Biomass Conv. Bioref</stitle><date>2023-08-01</date><risdate>2023</risdate><volume>13</volume><issue>12</issue><spage>11121</spage><epage>11130</epage><pages>11121-11130</pages><issn>2190-6815</issn><eissn>2190-6823</eissn><abstract>This study has put forth the concept of “control through utilization” for invasive weeds, which cause severe damage to ecosystem and biodiversity. The study comprised of extraction of lignin and pretreatment of spent biomass of four invasive weeds. Lignin was extracted from native biomass using 1,4–dioxane as solvent. Lignin yield of all biomass varied in the range 8.61 − 11.14% w/w with the solvent recovery of 75.56–78.88% v/v. Extracted lignin was characterized using FTIR, TGA, and GPC. Lignin from
Mikania micrantha
had the highest thermal stability (T
50%
= 490 °C) and molecular weight (M
w
= 5537 g/mol). The spent biomass was subjected to dilute acid pretreatment for synthesis of total reducing sugars (TRS). TRS yields from different entities were as follows: non-extracted biomass = 94.18 − 221.81 mg/g, warm water wash = 8.74 − 15.66 mg/g, and raw biomass = 115.9 − 391.27 mg/g raw biomass. Biomass of
Saccharum spontaneum
gave the highest TRS yield.
Graphical abstract</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s13399-021-01960-6</doi><tpages>10</tpages></addata></record> |
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| subjects | Biodiversity Biomass Biotechnology Energy Lignin Original Article Pretreatment Renewable and Green Energy Solvents Thermal stability Warm water Weeds |
| title | Extraction and characterization of lignin from waste invasive weeds with dioxane-based process |
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