Porous V2O5 ion-storage film as the counter electrode of electrochromic WO3 film: Optimization via Response Surface Methodology (RSM)
Electrochromic glass, one of the green energy-saving building materials, get more and more attention. The advancement of efficient ion storage film become a hot topic of research. The porous V 2 O 5 ion-storage film was prepared by sol-gel method using polyethylene glycol (PEG) as the pore-former. T...
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| Veröffentlicht in: | Journal of sol-gel science and technology 2023-09, Vol.107 (3), p.548-559 |
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| creator | Pan, Zixin Liang, Xiaoping Yan, Su Zeng, Jing Bai, Jinshuo Zhang, Dequan Yang, Guixiang Liu, Zhifeng |
| description | Electrochromic glass, one of the green energy-saving building materials, get more and more attention. The advancement of efficient ion storage film become a hot topic of research. The porous V
2
O
5
ion-storage film was prepared by sol-gel method using polyethylene glycol (PEG) as the pore-former. The peak current of porous V
2
O
5
films heated at 300 °C increased substantially due to the volatility temperature of PEG at 285 °C. The mutual effects of the PEG content, heat treatment temperature, and heat treatment time on the structure and electrochromic properties of porous V
2
O
5
film were investigated by the response surface method (RSM). The results show that the influence extent on ion storage is: heat treatment temperature > PEG content > heat treatment time. Under optimized process parameters of PEG content 6.2 g/100 mL sol, heat treatment time 4 h, heat treatment temperature 310 °C, the porous V
2
O
5
film exhibited excellent ion storage capacity (87.28 mC·cm
−2
). The electrochromic device (ECD) with optimized porous V
2
O
5
ion-storage film as the counter electrode of electrochromic WO
3
film has been successfully assembled, which shows fascinating performance with high optical contrast (87.8% at 550 nm) and fast response time (bleaching/coloring: 4.5/3.7 s).
Graphical Abstract
Highlights
The porous V
2
O
5
ion-storage films were prepared by sol-gel method with PEG as pore-former.
Response surface methodology (RSM) was applied to optimize the process parameter.
The sequence of the effect of the ion storage capacity is heat treatment temperature > PEG content > heat treatment time.
Electrochromic devices (ECD) was assembled with porous V
2
O
5
film as the counter electrode of WO
3
film. |
| doi_str_mv | 10.1007/s10971-023-06174-y |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2847152443</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2847152443</sourcerecordid><originalsourceid>FETCH-LOGICAL-c270t-ce762f553277336e07ce81d96f522becb59c126a80627daed8c96aa795039f573</originalsourceid><addsrcrecordid>eNp9kEtLAzEUhYMoWB9_wFXAjS6iN8lkMuNOxBcoldbHMsTMnXakndQkI9S9_9vRKu5cXQ6c71z4CNnjcMQB9HHkUGrOQEgGOdcZW66RAVdasqzI8nUygFIUDDToTbIV4wsAqIzrAfm488F3kT6KoaKNb1lMPtgJ0rqZzamNNE2ROt-1CQPFGboUfIXU17_BTYOfN44-DeU3c0KHi9TMm3eb-jn61lg6wrjwbUQ67kJtHdJbTFNf-ZmfLOnBaHx7uEM2ajuLuPtzt8nDxfn92RW7GV5en53eMCc0JOZQ56JWSgqtpcwRtMOCV2VeKyGe0T2r0nGR2wJyoSuLVeHK3FpdKpBl3dvYJvur3UXwrx3GZF58F9r-pRFFprkSWSb7lli1XPAxBqzNIjRzG5aGg_nSbVa6Ta_bfOs2yx6SKyj25XaC4W_6H-oTwBaDzg</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2847152443</pqid></control><display><type>article</type><title>Porous V2O5 ion-storage film as the counter electrode of electrochromic WO3 film: Optimization via Response Surface Methodology (RSM)</title><source>SpringerNature Journals</source><creator>Pan, Zixin ; Liang, Xiaoping ; Yan, Su ; Zeng, Jing ; Bai, Jinshuo ; Zhang, Dequan ; Yang, Guixiang ; Liu, Zhifeng</creator><creatorcontrib>Pan, Zixin ; Liang, Xiaoping ; Yan, Su ; Zeng, Jing ; Bai, Jinshuo ; Zhang, Dequan ; Yang, Guixiang ; Liu, Zhifeng</creatorcontrib><description>Electrochromic glass, one of the green energy-saving building materials, get more and more attention. The advancement of efficient ion storage film become a hot topic of research. The porous V
2
O
5
ion-storage film was prepared by sol-gel method using polyethylene glycol (PEG) as the pore-former. The peak current of porous V
2
O
5
films heated at 300 °C increased substantially due to the volatility temperature of PEG at 285 °C. The mutual effects of the PEG content, heat treatment temperature, and heat treatment time on the structure and electrochromic properties of porous V
2
O
5
film were investigated by the response surface method (RSM). The results show that the influence extent on ion storage is: heat treatment temperature > PEG content > heat treatment time. Under optimized process parameters of PEG content 6.2 g/100 mL sol, heat treatment time 4 h, heat treatment temperature 310 °C, the porous V
2
O
5
film exhibited excellent ion storage capacity (87.28 mC·cm
−2
). The electrochromic device (ECD) with optimized porous V
2
O
5
ion-storage film as the counter electrode of electrochromic WO
3
film has been successfully assembled, which shows fascinating performance with high optical contrast (87.8% at 550 nm) and fast response time (bleaching/coloring: 4.5/3.7 s).
Graphical Abstract
Highlights
The porous V
2
O
5
ion-storage films were prepared by sol-gel method with PEG as pore-former.
Response surface methodology (RSM) was applied to optimize the process parameter.
The sequence of the effect of the ion storage capacity is heat treatment temperature > PEG content > heat treatment time.
Electrochromic devices (ECD) was assembled with porous V
2
O
5
film as the counter electrode of WO
3
film.</description><identifier>ISSN: 0928-0707</identifier><identifier>EISSN: 1573-4846</identifier><identifier>DOI: 10.1007/s10971-023-06174-y</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Bleaching ; Building materials ; Ceramics ; Chemistry and Materials Science ; Clean energy ; Composites ; Construction materials ; Electrochromic cells ; Electrochromism ; Electrodes ; Glass ; Green buildings ; Heat treating ; Heat treatment ; Inorganic Chemistry ; Ion storage ; Materials Science ; Nanotechnology ; Natural Materials ; Optical and Electronic Materials ; Optimization ; Original Paper: Devices based on sol-gel or hybrid materials ; Polyethylene glycol ; Process parameters ; Response surface methodology ; Sol-gel processes ; Storage capacity ; Vanadium pentoxide</subject><ispartof>Journal of sol-gel science and technology, 2023-09, Vol.107 (3), p.548-559</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-ce762f553277336e07ce81d96f522becb59c126a80627daed8c96aa795039f573</cites><orcidid>0000-0003-0292-9465</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10971-023-06174-y$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10971-023-06174-y$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Pan, Zixin</creatorcontrib><creatorcontrib>Liang, Xiaoping</creatorcontrib><creatorcontrib>Yan, Su</creatorcontrib><creatorcontrib>Zeng, Jing</creatorcontrib><creatorcontrib>Bai, Jinshuo</creatorcontrib><creatorcontrib>Zhang, Dequan</creatorcontrib><creatorcontrib>Yang, Guixiang</creatorcontrib><creatorcontrib>Liu, Zhifeng</creatorcontrib><title>Porous V2O5 ion-storage film as the counter electrode of electrochromic WO3 film: Optimization via Response Surface Methodology (RSM)</title><title>Journal of sol-gel science and technology</title><addtitle>J Sol-Gel Sci Technol</addtitle><description>Electrochromic glass, one of the green energy-saving building materials, get more and more attention. The advancement of efficient ion storage film become a hot topic of research. The porous V
2
O
5
ion-storage film was prepared by sol-gel method using polyethylene glycol (PEG) as the pore-former. The peak current of porous V
2
O
5
films heated at 300 °C increased substantially due to the volatility temperature of PEG at 285 °C. The mutual effects of the PEG content, heat treatment temperature, and heat treatment time on the structure and electrochromic properties of porous V
2
O
5
film were investigated by the response surface method (RSM). The results show that the influence extent on ion storage is: heat treatment temperature > PEG content > heat treatment time. Under optimized process parameters of PEG content 6.2 g/100 mL sol, heat treatment time 4 h, heat treatment temperature 310 °C, the porous V
2
O
5
film exhibited excellent ion storage capacity (87.28 mC·cm
−2
). The electrochromic device (ECD) with optimized porous V
2
O
5
ion-storage film as the counter electrode of electrochromic WO
3
film has been successfully assembled, which shows fascinating performance with high optical contrast (87.8% at 550 nm) and fast response time (bleaching/coloring: 4.5/3.7 s).
Graphical Abstract
Highlights
The porous V
2
O
5
ion-storage films were prepared by sol-gel method with PEG as pore-former.
Response surface methodology (RSM) was applied to optimize the process parameter.
The sequence of the effect of the ion storage capacity is heat treatment temperature > PEG content > heat treatment time.
Electrochromic devices (ECD) was assembled with porous V
2
O
5
film as the counter electrode of WO
3
film.</description><subject>Bleaching</subject><subject>Building materials</subject><subject>Ceramics</subject><subject>Chemistry and Materials Science</subject><subject>Clean energy</subject><subject>Composites</subject><subject>Construction materials</subject><subject>Electrochromic cells</subject><subject>Electrochromism</subject><subject>Electrodes</subject><subject>Glass</subject><subject>Green buildings</subject><subject>Heat treating</subject><subject>Heat treatment</subject><subject>Inorganic Chemistry</subject><subject>Ion storage</subject><subject>Materials Science</subject><subject>Nanotechnology</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Optimization</subject><subject>Original Paper: Devices based on sol-gel or hybrid materials</subject><subject>Polyethylene glycol</subject><subject>Process parameters</subject><subject>Response surface methodology</subject><subject>Sol-gel processes</subject><subject>Storage capacity</subject><subject>Vanadium pentoxide</subject><issn>0928-0707</issn><issn>1573-4846</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kEtLAzEUhYMoWB9_wFXAjS6iN8lkMuNOxBcoldbHMsTMnXakndQkI9S9_9vRKu5cXQ6c71z4CNnjcMQB9HHkUGrOQEgGOdcZW66RAVdasqzI8nUygFIUDDToTbIV4wsAqIzrAfm488F3kT6KoaKNb1lMPtgJ0rqZzamNNE2ROt-1CQPFGboUfIXU17_BTYOfN44-DeU3c0KHi9TMm3eb-jn61lg6wrjwbUQ67kJtHdJbTFNf-ZmfLOnBaHx7uEM2ajuLuPtzt8nDxfn92RW7GV5en53eMCc0JOZQ56JWSgqtpcwRtMOCV2VeKyGe0T2r0nGR2wJyoSuLVeHK3FpdKpBl3dvYJvur3UXwrx3GZF58F9r-pRFFprkSWSb7lli1XPAxBqzNIjRzG5aGg_nSbVa6Ta_bfOs2yx6SKyj25XaC4W_6H-oTwBaDzg</recordid><startdate>20230901</startdate><enddate>20230901</enddate><creator>Pan, Zixin</creator><creator>Liang, Xiaoping</creator><creator>Yan, Su</creator><creator>Zeng, Jing</creator><creator>Bai, Jinshuo</creator><creator>Zhang, Dequan</creator><creator>Yang, Guixiang</creator><creator>Liu, Zhifeng</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0003-0292-9465</orcidid></search><sort><creationdate>20230901</creationdate><title>Porous V2O5 ion-storage film as the counter electrode of electrochromic WO3 film: Optimization via Response Surface Methodology (RSM)</title><author>Pan, Zixin ; Liang, Xiaoping ; Yan, Su ; Zeng, Jing ; Bai, Jinshuo ; Zhang, Dequan ; Yang, Guixiang ; Liu, Zhifeng</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-ce762f553277336e07ce81d96f522becb59c126a80627daed8c96aa795039f573</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Bleaching</topic><topic>Building materials</topic><topic>Ceramics</topic><topic>Chemistry and Materials Science</topic><topic>Clean energy</topic><topic>Composites</topic><topic>Construction materials</topic><topic>Electrochromic cells</topic><topic>Electrochromism</topic><topic>Electrodes</topic><topic>Glass</topic><topic>Green buildings</topic><topic>Heat treating</topic><topic>Heat treatment</topic><topic>Inorganic Chemistry</topic><topic>Ion storage</topic><topic>Materials Science</topic><topic>Nanotechnology</topic><topic>Natural Materials</topic><topic>Optical and Electronic Materials</topic><topic>Optimization</topic><topic>Original Paper: Devices based on sol-gel or hybrid materials</topic><topic>Polyethylene glycol</topic><topic>Process parameters</topic><topic>Response surface methodology</topic><topic>Sol-gel processes</topic><topic>Storage capacity</topic><topic>Vanadium pentoxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Pan, Zixin</creatorcontrib><creatorcontrib>Liang, Xiaoping</creatorcontrib><creatorcontrib>Yan, Su</creatorcontrib><creatorcontrib>Zeng, Jing</creatorcontrib><creatorcontrib>Bai, Jinshuo</creatorcontrib><creatorcontrib>Zhang, Dequan</creatorcontrib><creatorcontrib>Yang, Guixiang</creatorcontrib><creatorcontrib>Liu, Zhifeng</creatorcontrib><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><jtitle>Journal of sol-gel science and technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Pan, Zixin</au><au>Liang, Xiaoping</au><au>Yan, Su</au><au>Zeng, Jing</au><au>Bai, Jinshuo</au><au>Zhang, Dequan</au><au>Yang, Guixiang</au><au>Liu, Zhifeng</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Porous V2O5 ion-storage film as the counter electrode of electrochromic WO3 film: Optimization via Response Surface Methodology (RSM)</atitle><jtitle>Journal of sol-gel science and technology</jtitle><stitle>J Sol-Gel Sci Technol</stitle><date>2023-09-01</date><risdate>2023</risdate><volume>107</volume><issue>3</issue><spage>548</spage><epage>559</epage><pages>548-559</pages><issn>0928-0707</issn><eissn>1573-4846</eissn><abstract>Electrochromic glass, one of the green energy-saving building materials, get more and more attention. The advancement of efficient ion storage film become a hot topic of research. The porous V
2
O
5
ion-storage film was prepared by sol-gel method using polyethylene glycol (PEG) as the pore-former. The peak current of porous V
2
O
5
films heated at 300 °C increased substantially due to the volatility temperature of PEG at 285 °C. The mutual effects of the PEG content, heat treatment temperature, and heat treatment time on the structure and electrochromic properties of porous V
2
O
5
film were investigated by the response surface method (RSM). The results show that the influence extent on ion storage is: heat treatment temperature > PEG content > heat treatment time. Under optimized process parameters of PEG content 6.2 g/100 mL sol, heat treatment time 4 h, heat treatment temperature 310 °C, the porous V
2
O
5
film exhibited excellent ion storage capacity (87.28 mC·cm
−2
). The electrochromic device (ECD) with optimized porous V
2
O
5
ion-storage film as the counter electrode of electrochromic WO
3
film has been successfully assembled, which shows fascinating performance with high optical contrast (87.8% at 550 nm) and fast response time (bleaching/coloring: 4.5/3.7 s).
Graphical Abstract
Highlights
The porous V
2
O
5
ion-storage films were prepared by sol-gel method with PEG as pore-former.
Response surface methodology (RSM) was applied to optimize the process parameter.
The sequence of the effect of the ion storage capacity is heat treatment temperature > PEG content > heat treatment time.
Electrochromic devices (ECD) was assembled with porous V
2
O
5
film as the counter electrode of WO
3
film.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10971-023-06174-y</doi><tpages>12</tpages><orcidid>https://orcid.org/0000-0003-0292-9465</orcidid></addata></record> |
| fulltext | fulltext |
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| ispartof | Journal of sol-gel science and technology, 2023-09, Vol.107 (3), p.548-559 |
| issn | 0928-0707 1573-4846 |
| language | eng |
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| source | SpringerNature Journals |
| subjects | Bleaching Building materials Ceramics Chemistry and Materials Science Clean energy Composites Construction materials Electrochromic cells Electrochromism Electrodes Glass Green buildings Heat treating Heat treatment Inorganic Chemistry Ion storage Materials Science Nanotechnology Natural Materials Optical and Electronic Materials Optimization Original Paper: Devices based on sol-gel or hybrid materials Polyethylene glycol Process parameters Response surface methodology Sol-gel processes Storage capacity Vanadium pentoxide |
| title | Porous V2O5 ion-storage film as the counter electrode of electrochromic WO3 film: Optimization via Response Surface Methodology (RSM) |
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