Complexes of Ethylenediaminetetraacetic Acid with Amines. Molecular Structures of Bis(monoethanolaminium) Ethylenediaminetetraacetate and Bis[tris(hydroxymethyl)methylaminium] Ethylenediaminetetraacetate Trihydrate
Tetrabasic ethylenediaminetetraacetic acid H 4 L binds two molecules of monobasic amines to give the corresponding salts: ethylenediaminetetraacetates of bis(monoethanolaminium) H 2 L 2– ⋅2 + H 3 NCH 2 CH 2 ОН, tris(hydroxymethyl)methylaminium H 2 L 2– ⋅2 + H 3 NС(CH 2 ОН) 3 ⋅3H 2 О, diethylaminium...
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| Veröffentlicht in: | Crystallography reports 2023-04, Vol.68 (2), p.247-258 |
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| creator | Semenov, V. V. Zolotareva, N. V. Novikova, O. V. Petrov, B. I. Lazarev, N. M. Fukin, G. K. Cherkasov, A. V. Razov, E. N. |
| description | Tetrabasic ethylenediaminetetraacetic acid H
4
L
binds two molecules of monobasic amines to give the corresponding salts: ethylenediaminetetraacetates of bis(monoethanolaminium) H
2
L
2–
⋅2
+
H
3
NCH
2
CH
2
ОН, tris(hydroxymethyl)methylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
2
ОН)
3
⋅3H
2
О, diethylaminium H
2
L
2–
⋅2
+
H
2
N(C
2
H
5
)
2
⋅H
2
О,
tert
-butylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
3
)
3
⋅5H
2
О, and triethanolaminium H
2
L
2–
⋅2
+
HN(CH
2
CH
2
ОH)
3
. Dibasic hexamethylene-1,6-diamine, triethylenediamine, and tetramethylethylenediamine form the following 1 : 1 adducts: H
2
L
2–
⋅
+
NH
3
(CH
2
)
6
NH
, H
2
L
2–
⋅
+
NH
3
CH
2
CH
2
(OCH
2
CH
2
)
2
NH
, H
2
L
2–
⋅
+
HN(CH
2
CH
2
)
3
NH
+
⋅H
2
О, and H
2
L
2–
⋅
+
H(CH
3
)
2
NCH
2
CH
2
N(CH
3
)
2
H
+
. The molecular structures of bis(monoethanolaminium) ethylenediaminetetraacetate and bis[tris(hydroxymethyl)methylaminium] ethylenediaminetetraacetate trihydrate were determined. |
| doi_str_mv | 10.1134/S1063774523020141 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2841449023</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2841449023</sourcerecordid><originalsourceid>FETCH-LOGICAL-c316t-8cc1e358a5de271e5e0eb492d8c4523d6e63090539467bcb4033590cf34926e03</originalsourceid><addsrcrecordid>eNp9kV1LwzAUhosoOKc_wLuCN-6iM2nSr8s55gdMvNgEQaRk6anLaJuZpLj-UX-PCR14IfPqHHjf5wnkeN4lRmOMCb1ZYBSTJKFRSFCIMMVH3gBHcRjEafZ6bHcbBy4_9c603iCE0hTTgfc9lfW2gh1oX5b-zKy7ChooBKtFAwaMYoyDEdyfcFH4X8Ks_YmL9Nh_khXwtmLKXxjVctOqXnIr9HUtGwlmzRpZOZNo69FBOTPgs6Zw3JtRFl53hZK7rgYHjPqxt7z_a1kq4Vi7nnsnJas0XOzn0Hu5my2nD8H8-f5xOpkHnODYBCnnGEiUsqiAMMEQAYIVzcIi5e4nixhigjIUkYzGyYqvKCIkyhAviS3FgMjQu-q9WyU_W9Am38hWNfbJPEwppjRDIbEt3Le4klorKPOtEjVTXY5R7s6X_zmfZcKe0bbbfID6NR-GfgBUAaO-</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2841449023</pqid></control><display><type>article</type><title>Complexes of Ethylenediaminetetraacetic Acid with Amines. Molecular Structures of Bis(monoethanolaminium) Ethylenediaminetetraacetate and Bis[tris(hydroxymethyl)methylaminium] Ethylenediaminetetraacetate Trihydrate</title><source>SpringerLink Journals - AutoHoldings</source><creator>Semenov, V. V. ; Zolotareva, N. V. ; Novikova, O. V. ; Petrov, B. I. ; Lazarev, N. M. ; Fukin, G. K. ; Cherkasov, A. V. ; Razov, E. N.</creator><creatorcontrib>Semenov, V. V. ; Zolotareva, N. V. ; Novikova, O. V. ; Petrov, B. I. ; Lazarev, N. M. ; Fukin, G. K. ; Cherkasov, A. V. ; Razov, E. N.</creatorcontrib><description>Tetrabasic ethylenediaminetetraacetic acid H
4
L
binds two molecules of monobasic amines to give the corresponding salts: ethylenediaminetetraacetates of bis(monoethanolaminium) H
2
L
2–
⋅2
+
H
3
NCH
2
CH
2
ОН, tris(hydroxymethyl)methylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
2
ОН)
3
⋅3H
2
О, diethylaminium H
2
L
2–
⋅2
+
H
2
N(C
2
H
5
)
2
⋅H
2
О,
tert
-butylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
3
)
3
⋅5H
2
О, and triethanolaminium H
2
L
2–
⋅2
+
HN(CH
2
CH
2
ОH)
3
. Dibasic hexamethylene-1,6-diamine, triethylenediamine, and tetramethylethylenediamine form the following 1 : 1 adducts: H
2
L
2–
⋅
+
NH
3
(CH
2
)
6
NH
, H
2
L
2–
⋅
+
NH
3
CH
2
CH
2
(OCH
2
CH
2
)
2
NH
, H
2
L
2–
⋅
+
HN(CH
2
CH
2
)
3
NH
+
⋅H
2
О, and H
2
L
2–
⋅
+
H(CH
3
)
2
NCH
2
CH
2
N(CH
3
)
2
H
+
. The molecular structures of bis(monoethanolaminium) ethylenediaminetetraacetate and bis[tris(hydroxymethyl)methylaminium] ethylenediaminetetraacetate trihydrate were determined.</description><identifier>ISSN: 1063-7745</identifier><identifier>EISSN: 1562-689X</identifier><identifier>DOI: 10.1134/S1063774523020141</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Adducts ; Amines ; Ammonia ; Crystallography and Scattering Methods ; Diamines ; Molecular structure ; Physics ; Physics and Astronomy ; Structure of Organic Compounds</subject><ispartof>Crystallography reports, 2023-04, Vol.68 (2), p.247-258</ispartof><rights>Pleiades Publishing, Inc. 2023. ISSN 1063-7745, Crystallography Reports, 2023, Vol. 68, No. 2, pp. 247–258. © Pleiades Publishing, Inc., 2023. Russian Text © The Author(s), 2023, published in Kristallografiya, 2023, Vol. 68, No. 2, pp. 234–245.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-8cc1e358a5de271e5e0eb492d8c4523d6e63090539467bcb4033590cf34926e03</citedby><cites>FETCH-LOGICAL-c316t-8cc1e358a5de271e5e0eb492d8c4523d6e63090539467bcb4033590cf34926e03</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1063774523020141$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1063774523020141$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Semenov, V. V.</creatorcontrib><creatorcontrib>Zolotareva, N. V.</creatorcontrib><creatorcontrib>Novikova, O. V.</creatorcontrib><creatorcontrib>Petrov, B. I.</creatorcontrib><creatorcontrib>Lazarev, N. M.</creatorcontrib><creatorcontrib>Fukin, G. K.</creatorcontrib><creatorcontrib>Cherkasov, A. V.</creatorcontrib><creatorcontrib>Razov, E. N.</creatorcontrib><title>Complexes of Ethylenediaminetetraacetic Acid with Amines. Molecular Structures of Bis(monoethanolaminium) Ethylenediaminetetraacetate and Bis[tris(hydroxymethyl)methylaminium] Ethylenediaminetetraacetate Trihydrate</title><title>Crystallography reports</title><addtitle>Crystallogr. Rep</addtitle><description>Tetrabasic ethylenediaminetetraacetic acid H
4
L
binds two molecules of monobasic amines to give the corresponding salts: ethylenediaminetetraacetates of bis(monoethanolaminium) H
2
L
2–
⋅2
+
H
3
NCH
2
CH
2
ОН, tris(hydroxymethyl)methylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
2
ОН)
3
⋅3H
2
О, diethylaminium H
2
L
2–
⋅2
+
H
2
N(C
2
H
5
)
2
⋅H
2
О,
tert
-butylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
3
)
3
⋅5H
2
О, and triethanolaminium H
2
L
2–
⋅2
+
HN(CH
2
CH
2
ОH)
3
. Dibasic hexamethylene-1,6-diamine, triethylenediamine, and tetramethylethylenediamine form the following 1 : 1 adducts: H
2
L
2–
⋅
+
NH
3
(CH
2
)
6
NH
, H
2
L
2–
⋅
+
NH
3
CH
2
CH
2
(OCH
2
CH
2
)
2
NH
, H
2
L
2–
⋅
+
HN(CH
2
CH
2
)
3
NH
+
⋅H
2
О, and H
2
L
2–
⋅
+
H(CH
3
)
2
NCH
2
CH
2
N(CH
3
)
2
H
+
. The molecular structures of bis(monoethanolaminium) ethylenediaminetetraacetate and bis[tris(hydroxymethyl)methylaminium] ethylenediaminetetraacetate trihydrate were determined.</description><subject>Adducts</subject><subject>Amines</subject><subject>Ammonia</subject><subject>Crystallography and Scattering Methods</subject><subject>Diamines</subject><subject>Molecular structure</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Structure of Organic Compounds</subject><issn>1063-7745</issn><issn>1562-689X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kV1LwzAUhosoOKc_wLuCN-6iM2nSr8s55gdMvNgEQaRk6anLaJuZpLj-UX-PCR14IfPqHHjf5wnkeN4lRmOMCb1ZYBSTJKFRSFCIMMVH3gBHcRjEafZ6bHcbBy4_9c603iCE0hTTgfc9lfW2gh1oX5b-zKy7ChooBKtFAwaMYoyDEdyfcFH4X8Ks_YmL9Nh_khXwtmLKXxjVctOqXnIr9HUtGwlmzRpZOZNo69FBOTPgs6Zw3JtRFl53hZK7rgYHjPqxt7z_a1kq4Vi7nnsnJas0XOzn0Hu5my2nD8H8-f5xOpkHnODYBCnnGEiUsqiAMMEQAYIVzcIi5e4nixhigjIUkYzGyYqvKCIkyhAviS3FgMjQu-q9WyU_W9Am38hWNfbJPEwppjRDIbEt3Le4klorKPOtEjVTXY5R7s6X_zmfZcKe0bbbfID6NR-GfgBUAaO-</recordid><startdate>20230401</startdate><enddate>20230401</enddate><creator>Semenov, V. V.</creator><creator>Zolotareva, N. V.</creator><creator>Novikova, O. V.</creator><creator>Petrov, B. I.</creator><creator>Lazarev, N. M.</creator><creator>Fukin, G. K.</creator><creator>Cherkasov, A. V.</creator><creator>Razov, E. N.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20230401</creationdate><title>Complexes of Ethylenediaminetetraacetic Acid with Amines. Molecular Structures of Bis(monoethanolaminium) Ethylenediaminetetraacetate and Bis[tris(hydroxymethyl)methylaminium] Ethylenediaminetetraacetate Trihydrate</title><author>Semenov, V. V. ; Zolotareva, N. V. ; Novikova, O. V. ; Petrov, B. I. ; Lazarev, N. M. ; Fukin, G. K. ; Cherkasov, A. V. ; Razov, E. N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-8cc1e358a5de271e5e0eb492d8c4523d6e63090539467bcb4033590cf34926e03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Adducts</topic><topic>Amines</topic><topic>Ammonia</topic><topic>Crystallography and Scattering Methods</topic><topic>Diamines</topic><topic>Molecular structure</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Structure of Organic Compounds</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Semenov, V. V.</creatorcontrib><creatorcontrib>Zolotareva, N. V.</creatorcontrib><creatorcontrib>Novikova, O. V.</creatorcontrib><creatorcontrib>Petrov, B. I.</creatorcontrib><creatorcontrib>Lazarev, N. M.</creatorcontrib><creatorcontrib>Fukin, G. K.</creatorcontrib><creatorcontrib>Cherkasov, A. V.</creatorcontrib><creatorcontrib>Razov, E. N.</creatorcontrib><collection>CrossRef</collection><jtitle>Crystallography reports</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Semenov, V. V.</au><au>Zolotareva, N. V.</au><au>Novikova, O. V.</au><au>Petrov, B. I.</au><au>Lazarev, N. M.</au><au>Fukin, G. K.</au><au>Cherkasov, A. V.</au><au>Razov, E. N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Complexes of Ethylenediaminetetraacetic Acid with Amines. Molecular Structures of Bis(monoethanolaminium) Ethylenediaminetetraacetate and Bis[tris(hydroxymethyl)methylaminium] Ethylenediaminetetraacetate Trihydrate</atitle><jtitle>Crystallography reports</jtitle><stitle>Crystallogr. Rep</stitle><date>2023-04-01</date><risdate>2023</risdate><volume>68</volume><issue>2</issue><spage>247</spage><epage>258</epage><pages>247-258</pages><issn>1063-7745</issn><eissn>1562-689X</eissn><abstract>Tetrabasic ethylenediaminetetraacetic acid H
4
L
binds two molecules of monobasic amines to give the corresponding salts: ethylenediaminetetraacetates of bis(monoethanolaminium) H
2
L
2–
⋅2
+
H
3
NCH
2
CH
2
ОН, tris(hydroxymethyl)methylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
2
ОН)
3
⋅3H
2
О, diethylaminium H
2
L
2–
⋅2
+
H
2
N(C
2
H
5
)
2
⋅H
2
О,
tert
-butylaminium H
2
L
2–
⋅2
+
H
3
NС(CH
3
)
3
⋅5H
2
О, and triethanolaminium H
2
L
2–
⋅2
+
HN(CH
2
CH
2
ОH)
3
. Dibasic hexamethylene-1,6-diamine, triethylenediamine, and tetramethylethylenediamine form the following 1 : 1 adducts: H
2
L
2–
⋅
+
NH
3
(CH
2
)
6
NH
, H
2
L
2–
⋅
+
NH
3
CH
2
CH
2
(OCH
2
CH
2
)
2
NH
, H
2
L
2–
⋅
+
HN(CH
2
CH
2
)
3
NH
+
⋅H
2
О, and H
2
L
2–
⋅
+
H(CH
3
)
2
NCH
2
CH
2
N(CH
3
)
2
H
+
. The molecular structures of bis(monoethanolaminium) ethylenediaminetetraacetate and bis[tris(hydroxymethyl)methylaminium] ethylenediaminetetraacetate trihydrate were determined.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1063774523020141</doi><tpages>12</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1063-7745 |
| ispartof | Crystallography reports, 2023-04, Vol.68 (2), p.247-258 |
| issn | 1063-7745 1562-689X |
| language | eng |
| recordid | cdi_proquest_journals_2841449023 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Adducts Amines Ammonia Crystallography and Scattering Methods Diamines Molecular structure Physics Physics and Astronomy Structure of Organic Compounds |
| title | Complexes of Ethylenediaminetetraacetic Acid with Amines. Molecular Structures of Bis(monoethanolaminium) Ethylenediaminetetraacetate and Bis[tris(hydroxymethyl)methylaminium] Ethylenediaminetetraacetate Trihydrate |
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