Nitromethylidene-containing piperazinones and morpholinone: synthesis and structure
The interactions of alkyl 3-bromo-3-nitroacrylates with 1,2-diaminoethane, 1,2-diaminopropane, 1,2-diaminocyclohexane, and 2-aminoethanol were shown to provide a convenient route for the synthesis of six-membered heterocycles – (3 Z )-3-(nitromethylidene)-piperazin-2-ones and (3 Z )-3-(nitromethylid...
Gespeichert in:
Veröffentlicht in: | Chemistry of heterocyclic compounds (New York, N.Y. 1965) N.Y. 1965), 2023-05, Vol.59 (4-5), p.322-326 |
---|---|
Hauptverfasser: | , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | 326 |
---|---|
container_issue | 4-5 |
container_start_page | 322 |
container_title | Chemistry of heterocyclic compounds (New York, N.Y. 1965) |
container_volume | 59 |
creator | Pelipko, Vasilii V. Baichurin, Ruslan I. Lyssenko, Konstantin A. Makarenko, Sergey V. |
description | The interactions of alkyl 3-bromo-3-nitroacrylates with 1,2-diaminoethane, 1,2-diaminopropane, 1,2-diaminocyclohexane, and 2-aminoethanol were shown to provide a convenient route for the synthesis of six-membered heterocycles – (3
Z
)-3-(nitromethylidene)-piperazin-2-ones and (3
Z
)-3-(nitromethylidene)morpholin-2-one. The structures of the synthesized heterocycles were characterized by a range of spectral methods and by X-ray structural analysis. |
doi_str_mv | 10.1007/s10593-023-03200-3 |
format | Article |
fullrecord | <record><control><sourceid>gale_proqu</sourceid><recordid>TN_cdi_proquest_journals_2836960279</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A757112040</galeid><sourcerecordid>A757112040</sourcerecordid><originalsourceid>FETCH-LOGICAL-c386t-f16e7a1ddfd86c1a8758db8746220014e5fa62e47e8d2fcc06056b627e92787f3</originalsourceid><addsrcrecordid>eNp9kUtLAzEQx4MoWB9fwFPB82oeu0nWWxFfUPSgnkOanbSRbrIm6aF-eqMrFEFkCENm_r885o_QGcEXBGNxmQhuWlZhWhajGFdsD01II1glWcP20QRj3FaMUHqIjlJ6K1tBZD1Bz48ux9BDXm3XrgMPlQk-a-edX04HN0DUH84HD2mqfTftQxxWYf1duZqmrc8rSG7spRw3Jm8inKADq9cJTn_yMXq9vXm5vq_mT3cP17N5ZZjkubKEg9Ck62wnuSFaikZ2CylqTssPSA2N1ZxCLUB21BqDOW74glMBLRVSWHaMzsdzhxjeN5Cyegub6MuVikrGW46paHeqpV6Dct6GHLXpXTJqJhpBCMU1LqqLP1QlOuhdGQlYV-q_ADoCJoaUIlg1RNfruFUEqy9P1OiJKp6ob08UKxAboVTEfglx9-J_qE8kDY6q</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2836960279</pqid></control><display><type>article</type><title>Nitromethylidene-containing piperazinones and morpholinone: synthesis and structure</title><source>SpringerNature Journals</source><creator>Pelipko, Vasilii V. ; Baichurin, Ruslan I. ; Lyssenko, Konstantin A. ; Makarenko, Sergey V.</creator><creatorcontrib>Pelipko, Vasilii V. ; Baichurin, Ruslan I. ; Lyssenko, Konstantin A. ; Makarenko, Sergey V.</creatorcontrib><description>The interactions of alkyl 3-bromo-3-nitroacrylates with 1,2-diaminoethane, 1,2-diaminopropane, 1,2-diaminocyclohexane, and 2-aminoethanol were shown to provide a convenient route for the synthesis of six-membered heterocycles – (3
Z
)-3-(nitromethylidene)-piperazin-2-ones and (3
Z
)-3-(nitromethylidene)morpholin-2-one. The structures of the synthesized heterocycles were characterized by a range of spectral methods and by X-ray structural analysis.</description><identifier>ISSN: 0009-3122</identifier><identifier>EISSN: 1573-8353</identifier><identifier>DOI: 10.1007/s10593-023-03200-3</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Antifungal agents ; Chemistry ; Chemistry and Materials Science ; Organic Chemistry ; Pharmacy ; Short Communications ; Spectral methods ; Structural analysis ; Synthesis</subject><ispartof>Chemistry of heterocyclic compounds (New York, N.Y. 1965), 2023-05, Vol.59 (4-5), p.322-326</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>COPYRIGHT 2023 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c386t-f16e7a1ddfd86c1a8758db8746220014e5fa62e47e8d2fcc06056b627e92787f3</citedby><cites>FETCH-LOGICAL-c386t-f16e7a1ddfd86c1a8758db8746220014e5fa62e47e8d2fcc06056b627e92787f3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10593-023-03200-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10593-023-03200-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27929,27930,41493,42562,51324</link.rule.ids></links><search><creatorcontrib>Pelipko, Vasilii V.</creatorcontrib><creatorcontrib>Baichurin, Ruslan I.</creatorcontrib><creatorcontrib>Lyssenko, Konstantin A.</creatorcontrib><creatorcontrib>Makarenko, Sergey V.</creatorcontrib><title>Nitromethylidene-containing piperazinones and morpholinone: synthesis and structure</title><title>Chemistry of heterocyclic compounds (New York, N.Y. 1965)</title><addtitle>Chem Heterocycl Comp</addtitle><description>The interactions of alkyl 3-bromo-3-nitroacrylates with 1,2-diaminoethane, 1,2-diaminopropane, 1,2-diaminocyclohexane, and 2-aminoethanol were shown to provide a convenient route for the synthesis of six-membered heterocycles – (3
Z
)-3-(nitromethylidene)-piperazin-2-ones and (3
Z
)-3-(nitromethylidene)morpholin-2-one. The structures of the synthesized heterocycles were characterized by a range of spectral methods and by X-ray structural analysis.</description><subject>Antifungal agents</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Organic Chemistry</subject><subject>Pharmacy</subject><subject>Short Communications</subject><subject>Spectral methods</subject><subject>Structural analysis</subject><subject>Synthesis</subject><issn>0009-3122</issn><issn>1573-8353</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kUtLAzEQx4MoWB9fwFPB82oeu0nWWxFfUPSgnkOanbSRbrIm6aF-eqMrFEFkCENm_r885o_QGcEXBGNxmQhuWlZhWhajGFdsD01II1glWcP20QRj3FaMUHqIjlJ6K1tBZD1Bz48ux9BDXm3XrgMPlQk-a-edX04HN0DUH84HD2mqfTftQxxWYf1duZqmrc8rSG7spRw3Jm8inKADq9cJTn_yMXq9vXm5vq_mT3cP17N5ZZjkubKEg9Ck62wnuSFaikZ2CylqTssPSA2N1ZxCLUB21BqDOW74glMBLRVSWHaMzsdzhxjeN5Cyegub6MuVikrGW46paHeqpV6Dct6GHLXpXTJqJhpBCMU1LqqLP1QlOuhdGQlYV-q_ADoCJoaUIlg1RNfruFUEqy9P1OiJKp6ob08UKxAboVTEfglx9-J_qE8kDY6q</recordid><startdate>20230501</startdate><enddate>20230501</enddate><creator>Pelipko, Vasilii V.</creator><creator>Baichurin, Ruslan I.</creator><creator>Lyssenko, Konstantin A.</creator><creator>Makarenko, Sergey V.</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20230501</creationdate><title>Nitromethylidene-containing piperazinones and morpholinone: synthesis and structure</title><author>Pelipko, Vasilii V. ; Baichurin, Ruslan I. ; Lyssenko, Konstantin A. ; Makarenko, Sergey V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c386t-f16e7a1ddfd86c1a8758db8746220014e5fa62e47e8d2fcc06056b627e92787f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Antifungal agents</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Organic Chemistry</topic><topic>Pharmacy</topic><topic>Short Communications</topic><topic>Spectral methods</topic><topic>Structural analysis</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Pelipko, Vasilii V.</creatorcontrib><creatorcontrib>Baichurin, Ruslan I.</creatorcontrib><creatorcontrib>Lyssenko, Konstantin A.</creatorcontrib><creatorcontrib>Makarenko, Sergey V.</creatorcontrib><collection>CrossRef</collection><jtitle>Chemistry of heterocyclic compounds (New York, N.Y. 1965)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Pelipko, Vasilii V.</au><au>Baichurin, Ruslan I.</au><au>Lyssenko, Konstantin A.</au><au>Makarenko, Sergey V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Nitromethylidene-containing piperazinones and morpholinone: synthesis and structure</atitle><jtitle>Chemistry of heterocyclic compounds (New York, N.Y. 1965)</jtitle><stitle>Chem Heterocycl Comp</stitle><date>2023-05-01</date><risdate>2023</risdate><volume>59</volume><issue>4-5</issue><spage>322</spage><epage>326</epage><pages>322-326</pages><issn>0009-3122</issn><eissn>1573-8353</eissn><abstract>The interactions of alkyl 3-bromo-3-nitroacrylates with 1,2-diaminoethane, 1,2-diaminopropane, 1,2-diaminocyclohexane, and 2-aminoethanol were shown to provide a convenient route for the synthesis of six-membered heterocycles – (3
Z
)-3-(nitromethylidene)-piperazin-2-ones and (3
Z
)-3-(nitromethylidene)morpholin-2-one. The structures of the synthesized heterocycles were characterized by a range of spectral methods and by X-ray structural analysis.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10593-023-03200-3</doi><tpages>5</tpages></addata></record> |
fulltext | fulltext |
identifier | ISSN: 0009-3122 |
ispartof | Chemistry of heterocyclic compounds (New York, N.Y. 1965), 2023-05, Vol.59 (4-5), p.322-326 |
issn | 0009-3122 1573-8353 |
language | eng |
recordid | cdi_proquest_journals_2836960279 |
source | SpringerNature Journals |
subjects | Antifungal agents Chemistry Chemistry and Materials Science Organic Chemistry Pharmacy Short Communications Spectral methods Structural analysis Synthesis |
title | Nitromethylidene-containing piperazinones and morpholinone: synthesis and structure |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-14T03%3A25%3A31IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_proqu&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Nitromethylidene-containing%20piperazinones%20and%20morpholinone:%20synthesis%20and%20structure&rft.jtitle=Chemistry%20of%20heterocyclic%20compounds%20(New%20York,%20N.Y.%201965)&rft.au=Pelipko,%20Vasilii%20V.&rft.date=2023-05-01&rft.volume=59&rft.issue=4-5&rft.spage=322&rft.epage=326&rft.pages=322-326&rft.issn=0009-3122&rft.eissn=1573-8353&rft_id=info:doi/10.1007/s10593-023-03200-3&rft_dat=%3Cgale_proqu%3EA757112040%3C/gale_proqu%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2836960279&rft_id=info:pmid/&rft_galeid=A757112040&rfr_iscdi=true |