Hydrothermally synthesized NiFe2O4/rGO composites: structure, morphology and electrical conductivity
The effect of thermal treatment on the structural arrangement and pore size distribution in NiFe 2 O 4 /reduced graphene oxide composite materials has been studied using X-ray diffraction, Mössbauer spectroscopy, and nitrogen adsorption/desorption technique. Composite materials have been successfull...
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| Veröffentlicht in: | Applied nanoscience 2023-07, Vol.13 (7), p.5199-5209 |
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| creator | Hodlevska, Myroslava Kotsyubynsky, Volodymyr Boychuk, Volodymyra Budzulyak, Ivan Rachiy, Bogdan Zapukhlyak, Ruslan Hodlevsky, Mykola Turovska, Liliia |
| description | The effect of thermal treatment on the structural arrangement and pore size distribution in NiFe
2
O
4
/reduced graphene oxide composite materials has been studied using X-ray diffraction, Mössbauer spectroscopy, and nitrogen adsorption/desorption technique. Composite materials have been successfully synthesized by the joint hydrothermal method using graphene oxide colloidal solution obtained by the modified Tour method. The electrical properties of the composite materials, as well as the pure component, have been studied in the frequency range from 0.1 Hz to 1 MHz, in the temperature range from 25 to 175 °C using impedance spectroscopy. A synergetic increase in the electrical conductivity of composite materials compared to pure components has been observed. The activation energies of interparticle hopping of charge carriers have been calculated using Arrhenius-type conductivity plots. |
| doi_str_mv | 10.1007/s13204-022-02741-x |
| format | Article |
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2
O
4
/reduced graphene oxide composite materials has been studied using X-ray diffraction, Mössbauer spectroscopy, and nitrogen adsorption/desorption technique. Composite materials have been successfully synthesized by the joint hydrothermal method using graphene oxide colloidal solution obtained by the modified Tour method. The electrical properties of the composite materials, as well as the pure component, have been studied in the frequency range from 0.1 Hz to 1 MHz, in the temperature range from 25 to 175 °C using impedance spectroscopy. A synergetic increase in the electrical conductivity of composite materials compared to pure components has been observed. The activation energies of interparticle hopping of charge carriers have been calculated using Arrhenius-type conductivity plots.</description><identifier>ISSN: 2190-5509</identifier><identifier>EISSN: 2190-5517</identifier><identifier>DOI: 10.1007/s13204-022-02741-x</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Chemistry and Materials Science ; Composite materials ; Current carriers ; Electrical properties ; Electrical resistivity ; Frequency ranges ; Graphene ; Heat treatment ; Materials Science ; Membrane Biology ; Mossbauer spectroscopy ; Nanochemistry ; Nanotechnology ; Nanotechnology and Microengineering ; Nickel ferrites ; Original Article ; Pore size distribution ; Synthesis</subject><ispartof>Applied nanoscience, 2023-07, Vol.13 (7), p.5199-5209</ispartof><rights>Springer Nature Switzerland AG 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-b65f366e975a5d3953a77104fca6064e68b24c4298580dc79b5f5ac9c4ed76253</citedby><cites>FETCH-LOGICAL-c319t-b65f366e975a5d3953a77104fca6064e68b24c4298580dc79b5f5ac9c4ed76253</cites><orcidid>0000-0001-6461-937X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s13204-022-02741-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s13204-022-02741-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27923,27924,41487,42556,51318</link.rule.ids></links><search><creatorcontrib>Hodlevska, Myroslava</creatorcontrib><creatorcontrib>Kotsyubynsky, Volodymyr</creatorcontrib><creatorcontrib>Boychuk, Volodymyra</creatorcontrib><creatorcontrib>Budzulyak, Ivan</creatorcontrib><creatorcontrib>Rachiy, Bogdan</creatorcontrib><creatorcontrib>Zapukhlyak, Ruslan</creatorcontrib><creatorcontrib>Hodlevsky, Mykola</creatorcontrib><creatorcontrib>Turovska, Liliia</creatorcontrib><title>Hydrothermally synthesized NiFe2O4/rGO composites: structure, morphology and electrical conductivity</title><title>Applied nanoscience</title><addtitle>Appl Nanosci</addtitle><description>The effect of thermal treatment on the structural arrangement and pore size distribution in NiFe
2
O
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/reduced graphene oxide composite materials has been studied using X-ray diffraction, Mössbauer spectroscopy, and nitrogen adsorption/desorption technique. Composite materials have been successfully synthesized by the joint hydrothermal method using graphene oxide colloidal solution obtained by the modified Tour method. The electrical properties of the composite materials, as well as the pure component, have been studied in the frequency range from 0.1 Hz to 1 MHz, in the temperature range from 25 to 175 °C using impedance spectroscopy. A synergetic increase in the electrical conductivity of composite materials compared to pure components has been observed. 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2
O
4
/reduced graphene oxide composite materials has been studied using X-ray diffraction, Mössbauer spectroscopy, and nitrogen adsorption/desorption technique. Composite materials have been successfully synthesized by the joint hydrothermal method using graphene oxide colloidal solution obtained by the modified Tour method. The electrical properties of the composite materials, as well as the pure component, have been studied in the frequency range from 0.1 Hz to 1 MHz, in the temperature range from 25 to 175 °C using impedance spectroscopy. A synergetic increase in the electrical conductivity of composite materials compared to pure components has been observed. The activation energies of interparticle hopping of charge carriers have been calculated using Arrhenius-type conductivity plots.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s13204-022-02741-x</doi><tpages>11</tpages><orcidid>https://orcid.org/0000-0001-6461-937X</orcidid></addata></record> |
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| subjects | Chemistry and Materials Science Composite materials Current carriers Electrical properties Electrical resistivity Frequency ranges Graphene Heat treatment Materials Science Membrane Biology Mossbauer spectroscopy Nanochemistry Nanotechnology Nanotechnology and Microengineering Nickel ferrites Original Article Pore size distribution Synthesis |
| title | Hydrothermally synthesized NiFe2O4/rGO composites: structure, morphology and electrical conductivity |
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