Structural and luminescence characterization of β-Ga2O3 nanopowders obtained via high-energy ball milling
β-Ga 2 O 3 nanocrystals have been successfully obtained by the high-energy ball milling method. The obtained nanocrystalline powders have been characterized using X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray spectroscopy, and luminescent spectroscopy. X-ray diffractio...
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| Veröffentlicht in: | Applied nanoscience 2023-07, Vol.13 (7), p.5149-5155 |
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| creator | Luchechko, A. Vasyltsiv, V. Kushlyk, M. Slobodzyan, D. Baláž, M. Cebulski, J. Szmuc, K. Szlęzak, J. Shpotyuk, Y. |
| description | β-Ga
2
O
3
nanocrystals have been successfully obtained by the high-energy ball milling method. The obtained nanocrystalline powders have been characterized using X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray spectroscopy, and luminescent spectroscopy. X-ray diffraction patterns show a single gallium oxide structure formed in the milling process with a small amount of α-Ga
2
O
3
phase. The grains of irregular shape were identified with the TEM technique. HRTEM images confirmed the formation of the β-Ga
2
O
3
nanocrystals with a size distribution of 50–80 nm. Three luminescence bands peaked at about 2.52, 2.91, and 3.26 eV were observed in photoluminescence spectra. The gradual blue shift of the emission maxima at the excitation in the fundamental absorption edge under the different milling conditions was detected. |
| doi_str_mv | 10.1007/s13204-022-02717-x |
| format | Article |
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2
O
3
nanocrystals have been successfully obtained by the high-energy ball milling method. The obtained nanocrystalline powders have been characterized using X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray spectroscopy, and luminescent spectroscopy. X-ray diffraction patterns show a single gallium oxide structure formed in the milling process with a small amount of α-Ga
2
O
3
phase. The grains of irregular shape were identified with the TEM technique. HRTEM images confirmed the formation of the β-Ga
2
O
3
nanocrystals with a size distribution of 50–80 nm. Three luminescence bands peaked at about 2.52, 2.91, and 3.26 eV were observed in photoluminescence spectra. The gradual blue shift of the emission maxima at the excitation in the fundamental absorption edge under the different milling conditions was detected.</description><identifier>ISSN: 2190-5509</identifier><identifier>EISSN: 2190-5517</identifier><identifier>DOI: 10.1007/s13204-022-02717-x</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Ball milling ; Blue shift ; Chemistry and Materials Science ; Diffraction patterns ; Gallium oxides ; Luminescence ; Materials Science ; Membrane Biology ; Nanochemistry ; Nanocrystals ; Nanotechnology ; Nanotechnology and Microengineering ; Original Article ; Photoluminescence ; Size distribution ; Spectroscopy ; Structural analysis ; X-ray diffraction</subject><ispartof>Applied nanoscience, 2023-07, Vol.13 (7), p.5149-5155</ispartof><rights>The Author(s) 2022</rights><rights>The Author(s) 2022. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c363t-14cb062abb3b0d056a83472e786743e89482050d9fbd2887279d0cdf60aa69c3</citedby><cites>FETCH-LOGICAL-c363t-14cb062abb3b0d056a83472e786743e89482050d9fbd2887279d0cdf60aa69c3</cites><orcidid>0000-0001-6710-7839</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s13204-022-02717-x$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s13204-022-02717-x$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Luchechko, A.</creatorcontrib><creatorcontrib>Vasyltsiv, V.</creatorcontrib><creatorcontrib>Kushlyk, M.</creatorcontrib><creatorcontrib>Slobodzyan, D.</creatorcontrib><creatorcontrib>Baláž, M.</creatorcontrib><creatorcontrib>Cebulski, J.</creatorcontrib><creatorcontrib>Szmuc, K.</creatorcontrib><creatorcontrib>Szlęzak, J.</creatorcontrib><creatorcontrib>Shpotyuk, Y.</creatorcontrib><title>Structural and luminescence characterization of β-Ga2O3 nanopowders obtained via high-energy ball milling</title><title>Applied nanoscience</title><addtitle>Appl Nanosci</addtitle><description>β-Ga
2
O
3
nanocrystals have been successfully obtained by the high-energy ball milling method. The obtained nanocrystalline powders have been characterized using X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray spectroscopy, and luminescent spectroscopy. X-ray diffraction patterns show a single gallium oxide structure formed in the milling process with a small amount of α-Ga
2
O
3
phase. The grains of irregular shape were identified with the TEM technique. HRTEM images confirmed the formation of the β-Ga
2
O
3
nanocrystals with a size distribution of 50–80 nm. Three luminescence bands peaked at about 2.52, 2.91, and 3.26 eV were observed in photoluminescence spectra. The gradual blue shift of the emission maxima at the excitation in the fundamental absorption edge under the different milling conditions was detected.</description><subject>Ball milling</subject><subject>Blue shift</subject><subject>Chemistry and Materials Science</subject><subject>Diffraction patterns</subject><subject>Gallium oxides</subject><subject>Luminescence</subject><subject>Materials Science</subject><subject>Membrane Biology</subject><subject>Nanochemistry</subject><subject>Nanocrystals</subject><subject>Nanotechnology</subject><subject>Nanotechnology and Microengineering</subject><subject>Original Article</subject><subject>Photoluminescence</subject><subject>Size distribution</subject><subject>Spectroscopy</subject><subject>Structural analysis</subject><subject>X-ray diffraction</subject><issn>2190-5509</issn><issn>2190-5517</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><recordid>eNp9kM9KAzEQh4MoWGpfwFPA82r-7Wb3KEWrUOjB3kM2yW5TtklNdrX1sXwQn8noit4cGGYOv28GPgAuMbrGCPGbiClBLEOEpOaYZ4cTMCG4QlmeY376u6PqHMxi3KJUOeMFzSdg-9SHQfVDkB2UTsNu2FlnojJOGag2MkjVm2DfZG-9g76BH-_ZQpIVhU46v_ev2oQIfd3LhGn4YiXc2HaTGWdCe4S17Dq4s11nXXsBzhrZRTP7mVOwvr9bzx-y5WrxOL9dZooWtM8wUzUqiKxrWiON8kKWlHFieFlwRk1ZsZKgHOmqqTUpS054pZHSTYGkLCpFp-BqPLsP_nkwsRdbPwSXPgpSEsYqTjFLKTKmVPAxBtOIfbA7GY4CI_FlVYxWRbIqvq2KQ4LoCMUUdq0Jf6f_oT4B6h579g</recordid><startdate>20230701</startdate><enddate>20230701</enddate><creator>Luchechko, A.</creator><creator>Vasyltsiv, V.</creator><creator>Kushlyk, M.</creator><creator>Slobodzyan, D.</creator><creator>Baláž, M.</creator><creator>Cebulski, J.</creator><creator>Szmuc, K.</creator><creator>Szlęzak, J.</creator><creator>Shpotyuk, Y.</creator><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>C6C</scope><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0001-6710-7839</orcidid></search><sort><creationdate>20230701</creationdate><title>Structural and luminescence characterization of β-Ga2O3 nanopowders obtained via high-energy ball milling</title><author>Luchechko, A. ; Vasyltsiv, V. ; Kushlyk, M. ; Slobodzyan, D. ; Baláž, M. ; Cebulski, J. ; Szmuc, K. ; Szlęzak, J. ; Shpotyuk, Y.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c363t-14cb062abb3b0d056a83472e786743e89482050d9fbd2887279d0cdf60aa69c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Ball milling</topic><topic>Blue shift</topic><topic>Chemistry and Materials Science</topic><topic>Diffraction patterns</topic><topic>Gallium oxides</topic><topic>Luminescence</topic><topic>Materials Science</topic><topic>Membrane Biology</topic><topic>Nanochemistry</topic><topic>Nanocrystals</topic><topic>Nanotechnology</topic><topic>Nanotechnology and Microengineering</topic><topic>Original Article</topic><topic>Photoluminescence</topic><topic>Size distribution</topic><topic>Spectroscopy</topic><topic>Structural analysis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Luchechko, A.</creatorcontrib><creatorcontrib>Vasyltsiv, V.</creatorcontrib><creatorcontrib>Kushlyk, M.</creatorcontrib><creatorcontrib>Slobodzyan, D.</creatorcontrib><creatorcontrib>Baláž, M.</creatorcontrib><creatorcontrib>Cebulski, J.</creatorcontrib><creatorcontrib>Szmuc, K.</creatorcontrib><creatorcontrib>Szlęzak, J.</creatorcontrib><creatorcontrib>Shpotyuk, Y.</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>CrossRef</collection><jtitle>Applied nanoscience</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Luchechko, A.</au><au>Vasyltsiv, V.</au><au>Kushlyk, M.</au><au>Slobodzyan, D.</au><au>Baláž, M.</au><au>Cebulski, J.</au><au>Szmuc, K.</au><au>Szlęzak, J.</au><au>Shpotyuk, Y.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structural and luminescence characterization of β-Ga2O3 nanopowders obtained via high-energy ball milling</atitle><jtitle>Applied nanoscience</jtitle><stitle>Appl Nanosci</stitle><date>2023-07-01</date><risdate>2023</risdate><volume>13</volume><issue>7</issue><spage>5149</spage><epage>5155</epage><pages>5149-5155</pages><issn>2190-5509</issn><eissn>2190-5517</eissn><abstract>β-Ga
2
O
3
nanocrystals have been successfully obtained by the high-energy ball milling method. The obtained nanocrystalline powders have been characterized using X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray spectroscopy, and luminescent spectroscopy. X-ray diffraction patterns show a single gallium oxide structure formed in the milling process with a small amount of α-Ga
2
O
3
phase. The grains of irregular shape were identified with the TEM technique. HRTEM images confirmed the formation of the β-Ga
2
O
3
nanocrystals with a size distribution of 50–80 nm. Three luminescence bands peaked at about 2.52, 2.91, and 3.26 eV were observed in photoluminescence spectra. The gradual blue shift of the emission maxima at the excitation in the fundamental absorption edge under the different milling conditions was detected.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s13204-022-02717-x</doi><tpages>7</tpages><orcidid>https://orcid.org/0000-0001-6710-7839</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Ball milling Blue shift Chemistry and Materials Science Diffraction patterns Gallium oxides Luminescence Materials Science Membrane Biology Nanochemistry Nanocrystals Nanotechnology Nanotechnology and Microengineering Original Article Photoluminescence Size distribution Spectroscopy Structural analysis X-ray diffraction |
| title | Structural and luminescence characterization of β-Ga2O3 nanopowders obtained via high-energy ball milling |
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