A Study on Crystalline Structure and Li+-Ion Diffusion Coefficient of LiNixFe1−xPO4/C Cathode Material
This work focused on synthesising Ni-doped LiNi x Fe 1− x PO 4 /C ( x = 0, 0.05 and 0.1) cathode materials by hydrothermal method. The crystalline structure and morphology of the synthesised materials were investigated through x-ray diffraction, Raman scattering spectroscopy, thermal gravimetric an...
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| Veröffentlicht in: | Arabian journal for science and engineering (2011) 2023-06, Vol.48 (6), p.7713-7720 |
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| container_title | Arabian journal for science and engineering (2011) |
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| creator | Trinh, Dung V. Nguyen, Mai T. T. Huynh, Nguyen T. L. Tran, Hoang V. Huynh, Chinh D. |
| description | This work focused on synthesising Ni-doped LiNi
x
Fe
1−
x
PO
4
/C (
x
= 0, 0.05 and 0.1) cathode materials by hydrothermal method. The crystalline structure and morphology of the synthesised materials were investigated through x-ray diffraction, Raman scattering spectroscopy, thermal gravimetric analysis, and scanning electron microscopy. Their electrochemical performance was analysed by cyclic voltammetry and galvanostatic cycling test. The highest initial capacity of 170.3 mAh/g was achieved for LiNi
0.1
Fe
0.9
PO
4
/C. It also maintained 99.68% of its initial capacity for 120 cycles, with a Li
+
-ion diffusion coefficient of 1.12 × 10
−12
cm
2
/s compared with that (9.21 × 10
−13
cm
2
/s) of LiNi
0.05
Fe
0.95
PO
4
/C. |
| doi_str_mv | 10.1007/s13369-023-07799-5 |
| format | Article |
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x
Fe
1−
x
PO
4
/C (
x
= 0, 0.05 and 0.1) cathode materials by hydrothermal method. The crystalline structure and morphology of the synthesised materials were investigated through x-ray diffraction, Raman scattering spectroscopy, thermal gravimetric analysis, and scanning electron microscopy. Their electrochemical performance was analysed by cyclic voltammetry and galvanostatic cycling test. The highest initial capacity of 170.3 mAh/g was achieved for LiNi
0.1
Fe
0.9
PO
4
/C. It also maintained 99.68% of its initial capacity for 120 cycles, with a Li
+
-ion diffusion coefficient of 1.12 × 10
−12
cm
2
/s compared with that (9.21 × 10
−13
cm
2
/s) of LiNi
0.05
Fe
0.95
PO
4
/C.</description><identifier>ISSN: 2193-567X</identifier><identifier>ISSN: 1319-8025</identifier><identifier>EISSN: 2191-4281</identifier><identifier>DOI: 10.1007/s13369-023-07799-5</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Cathodes ; Crystal structure ; Crystallinity ; Diffusion coefficient ; Electrochemical analysis ; Electrode materials ; Engineering ; Humanities and Social Sciences ; Ion diffusion ; multidisciplinary ; Raman spectra ; Research Article-Chemistry ; Science</subject><ispartof>Arabian journal for science and engineering (2011), 2023-06, Vol.48 (6), p.7713-7720</ispartof><rights>King Fahd University of Petroleum & Minerals 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-f82c3250fa85220953c5c16b22ac205654af7e3a7d2d98ddd4d103b6fe271bc33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s13369-023-07799-5$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s13369-023-07799-5$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Trinh, Dung V.</creatorcontrib><creatorcontrib>Nguyen, Mai T. T.</creatorcontrib><creatorcontrib>Huynh, Nguyen T. L.</creatorcontrib><creatorcontrib>Tran, Hoang V.</creatorcontrib><creatorcontrib>Huynh, Chinh D.</creatorcontrib><title>A Study on Crystalline Structure and Li+-Ion Diffusion Coefficient of LiNixFe1−xPO4/C Cathode Material</title><title>Arabian journal for science and engineering (2011)</title><addtitle>Arab J Sci Eng</addtitle><description>This work focused on synthesising Ni-doped LiNi
x
Fe
1−
x
PO
4
/C (
x
= 0, 0.05 and 0.1) cathode materials by hydrothermal method. The crystalline structure and morphology of the synthesised materials were investigated through x-ray diffraction, Raman scattering spectroscopy, thermal gravimetric analysis, and scanning electron microscopy. Their electrochemical performance was analysed by cyclic voltammetry and galvanostatic cycling test. The highest initial capacity of 170.3 mAh/g was achieved for LiNi
0.1
Fe
0.9
PO
4
/C. It also maintained 99.68% of its initial capacity for 120 cycles, with a Li
+
-ion diffusion coefficient of 1.12 × 10
−12
cm
2
/s compared with that (9.21 × 10
−13
cm
2
/s) of LiNi
0.05
Fe
0.95
PO
4
/C.</description><subject>Cathodes</subject><subject>Crystal structure</subject><subject>Crystallinity</subject><subject>Diffusion coefficient</subject><subject>Electrochemical analysis</subject><subject>Electrode materials</subject><subject>Engineering</subject><subject>Humanities and Social Sciences</subject><subject>Ion diffusion</subject><subject>multidisciplinary</subject><subject>Raman spectra</subject><subject>Research Article-Chemistry</subject><subject>Science</subject><issn>2193-567X</issn><issn>1319-8025</issn><issn>2191-4281</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kM1Kw0AURoMoWGpfwFXApYyduZPJJMsSrRaqFVRwN0zmx47EpM4k0L6Bax_RJzE1gjtX93I533fhRNEpwRcEYz4NhNI0RxgowpznOWIH0QhITlACGTn82SliKX8-jiYhuBInGc0ZIXQUrWfxQ9vpXdzUceF3oZVV5WrTH32n2s6bWNY6XrpztOiJS2dtF9yebYy1TjlTt3Fje-DObeeGfH18bu9XybSIC9muG23iW9ka72R1Eh1ZWQUz-Z3j6Gl-9VjcoOXqelHMlkgBxy2yGSgKDFuZMQCcM6qYImkJIBVglrJEWm6o5Bp0nmmtE00wLVNrgJNSUTqOzobejW_eOxNa8dp0vu5fCsiAUJ5Q2FMwUMo3IXhjxca7N-l3gmCxlyoGqaKXKn6kCtaH6BAKPVy_GP9X_U_qG0mDeco</recordid><startdate>20230601</startdate><enddate>20230601</enddate><creator>Trinh, Dung V.</creator><creator>Nguyen, Mai T. T.</creator><creator>Huynh, Nguyen T. L.</creator><creator>Tran, Hoang V.</creator><creator>Huynh, Chinh D.</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20230601</creationdate><title>A Study on Crystalline Structure and Li+-Ion Diffusion Coefficient of LiNixFe1−xPO4/C Cathode Material</title><author>Trinh, Dung V. ; Nguyen, Mai T. T. ; Huynh, Nguyen T. L. ; Tran, Hoang V. ; Huynh, Chinh D.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-f82c3250fa85220953c5c16b22ac205654af7e3a7d2d98ddd4d103b6fe271bc33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Cathodes</topic><topic>Crystal structure</topic><topic>Crystallinity</topic><topic>Diffusion coefficient</topic><topic>Electrochemical analysis</topic><topic>Electrode materials</topic><topic>Engineering</topic><topic>Humanities and Social Sciences</topic><topic>Ion diffusion</topic><topic>multidisciplinary</topic><topic>Raman spectra</topic><topic>Research Article-Chemistry</topic><topic>Science</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Trinh, Dung V.</creatorcontrib><creatorcontrib>Nguyen, Mai T. T.</creatorcontrib><creatorcontrib>Huynh, Nguyen T. L.</creatorcontrib><creatorcontrib>Tran, Hoang V.</creatorcontrib><creatorcontrib>Huynh, Chinh D.</creatorcontrib><collection>CrossRef</collection><jtitle>Arabian journal for science and engineering (2011)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Trinh, Dung V.</au><au>Nguyen, Mai T. T.</au><au>Huynh, Nguyen T. L.</au><au>Tran, Hoang V.</au><au>Huynh, Chinh D.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A Study on Crystalline Structure and Li+-Ion Diffusion Coefficient of LiNixFe1−xPO4/C Cathode Material</atitle><jtitle>Arabian journal for science and engineering (2011)</jtitle><stitle>Arab J Sci Eng</stitle><date>2023-06-01</date><risdate>2023</risdate><volume>48</volume><issue>6</issue><spage>7713</spage><epage>7720</epage><pages>7713-7720</pages><issn>2193-567X</issn><issn>1319-8025</issn><eissn>2191-4281</eissn><abstract>This work focused on synthesising Ni-doped LiNi
x
Fe
1−
x
PO
4
/C (
x
= 0, 0.05 and 0.1) cathode materials by hydrothermal method. The crystalline structure and morphology of the synthesised materials were investigated through x-ray diffraction, Raman scattering spectroscopy, thermal gravimetric analysis, and scanning electron microscopy. Their electrochemical performance was analysed by cyclic voltammetry and galvanostatic cycling test. The highest initial capacity of 170.3 mAh/g was achieved for LiNi
0.1
Fe
0.9
PO
4
/C. It also maintained 99.68% of its initial capacity for 120 cycles, with a Li
+
-ion diffusion coefficient of 1.12 × 10
−12
cm
2
/s compared with that (9.21 × 10
−13
cm
2
/s) of LiNi
0.05
Fe
0.95
PO
4
/C.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s13369-023-07799-5</doi><tpages>8</tpages></addata></record> |
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| issn | 2193-567X 1319-8025 2191-4281 |
| language | eng |
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| subjects | Cathodes Crystal structure Crystallinity Diffusion coefficient Electrochemical analysis Electrode materials Engineering Humanities and Social Sciences Ion diffusion multidisciplinary Raman spectra Research Article-Chemistry Science |
| title | A Study on Crystalline Structure and Li+-Ion Diffusion Coefficient of LiNixFe1−xPO4/C Cathode Material |
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