Thermal hazard assessment by TGA, DSC, and ARC experimental and simulated thermokinetic approaches for trinitrophloroglucinol
Hazardous chemicals often have the characteristics of high-energy and high-risk, and environmental factors have a significant impact on them. Trinitrophloroglucinol, as an essential energetic intermediate, is widely used in the modern military, aerospace, and energy fields. It is the representative...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2023-06, Vol.148 (11), p.5039-5049 |
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| container_title | Journal of thermal analysis and calorimetry |
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| creator | Liu, Ye-Cheng Zhou, Hai-Lin Tang, Yan Li, You Zhai, Juan Jiang, Jun-Cheng Xing, Zhi-Xiang Huang, An-Chi |
| description | Hazardous chemicals often have the characteristics of high-energy and high-risk, and environmental factors have a significant impact on them. Trinitrophloroglucinol, as an essential energetic intermediate, is widely used in the modern military, aerospace, and energy fields. It is the representative substance of aromatic nitro compounds. Due to the unique properties of nitro, it has both an electron absorption conjugation effect and an electron absorption induction effect. These two effects lead to nitro becoming an electron absorption group, giving it high energy. For such dangerous substances containing nitro, it is of far-reaching significance to study the impact of environmental changes on their safety status. To determine the thermal safety performance of these substances in different external environments, different calorimetric devices, including thermogravimetry, differential scanning calorimetry, and accelerating rate calorimeter, are used to simulate different storage environments. Combined with calorimetric data, thermokinetic models suitable for trinitrophloroglucinol were established for thermal safety analysis. The results provide some quantitative guidance for the use and storage of aromatic nitro compounds. |
| doi_str_mv | 10.1007/s10973-022-11649-1 |
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Trinitrophloroglucinol, as an essential energetic intermediate, is widely used in the modern military, aerospace, and energy fields. It is the representative substance of aromatic nitro compounds. Due to the unique properties of nitro, it has both an electron absorption conjugation effect and an electron absorption induction effect. These two effects lead to nitro becoming an electron absorption group, giving it high energy. For such dangerous substances containing nitro, it is of far-reaching significance to study the impact of environmental changes on their safety status. To determine the thermal safety performance of these substances in different external environments, different calorimetric devices, including thermogravimetry, differential scanning calorimetry, and accelerating rate calorimeter, are used to simulate different storage environments. Combined with calorimetric data, thermokinetic models suitable for trinitrophloroglucinol were established for thermal safety analysis. The results provide some quantitative guidance for the use and storage of aromatic nitro compounds.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>DOI: 10.1007/s10973-022-11649-1</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Absorption ; Analytical Chemistry ; Aromatic compounds ; Chemistry ; Chemistry and Materials Science ; Conjugation ; Hazard assessment ; Heat measurement ; Information storage and retrieval ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Nitro compounds ; Physical Chemistry ; Polymer Sciences ; Safety ; Thermogravimetry</subject><ispartof>Journal of thermal analysis and calorimetry, 2023-06, Vol.148 (11), p.5039-5049</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2022. 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Trinitrophloroglucinol, as an essential energetic intermediate, is widely used in the modern military, aerospace, and energy fields. It is the representative substance of aromatic nitro compounds. Due to the unique properties of nitro, it has both an electron absorption conjugation effect and an electron absorption induction effect. These two effects lead to nitro becoming an electron absorption group, giving it high energy. For such dangerous substances containing nitro, it is of far-reaching significance to study the impact of environmental changes on their safety status. To determine the thermal safety performance of these substances in different external environments, different calorimetric devices, including thermogravimetry, differential scanning calorimetry, and accelerating rate calorimeter, are used to simulate different storage environments. Combined with calorimetric data, thermokinetic models suitable for trinitrophloroglucinol were established for thermal safety analysis. The results provide some quantitative guidance for the use and storage of aromatic nitro compounds.</description><subject>Absorption</subject><subject>Analytical Chemistry</subject><subject>Aromatic compounds</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Conjugation</subject><subject>Hazard assessment</subject><subject>Heat measurement</subject><subject>Information storage and retrieval</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Nitro compounds</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Safety</subject><subject>Thermogravimetry</subject><issn>1388-6150</issn><issn>1588-2926</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kU1r3DAQhk1poWmSP5CToKdCnOrDluTjsm3TQCCQbM9iVh7tKvVariRDUuh_r7YulFyKDhKj5xkNeqvqgtErRqn6mBjtlKgp5zVjsulq9qo6Ya3WNe-4fF3Oopwla-nb6l1Kj5TSrqPspPq12WM8wED28BNiTyAlTOmAYybbZ7K5Xl2STw_rSwJjT1b3a4JPE0Z_vC_OsZj8YR4gY0_ysVP47kfM3hKYphjA7jERFyLJ0Y8-xzDthxDDbpitH8NwVr1xMCQ8_7ufVt--fN6sv9a3d9c369VtbUXHc817zYRrLAdhpXKcuR6sA-RSNrLTAFspWqa3FDVsnepV06iuby1oRxtnqTit3i99y0w_ZkzZPIY5juVJwzVTkgutmkJdLdQOBjR-dCFHsGX1ePA2jOh8qa9US7kWUskifHghFCbjU97BnJK5ebh_yfKFtTGkFNGZqfwjxGfDqDlmaJYMTcnQ_MnQsCKJRUoFHncY_839H-s3cyGgHA</recordid><startdate>20230601</startdate><enddate>20230601</enddate><creator>Liu, Ye-Cheng</creator><creator>Zhou, Hai-Lin</creator><creator>Tang, Yan</creator><creator>Li, You</creator><creator>Zhai, Juan</creator><creator>Jiang, Jun-Cheng</creator><creator>Xing, Zhi-Xiang</creator><creator>Huang, An-Chi</creator><general>Springer International Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><orcidid>https://orcid.org/0000-0002-7682-5434</orcidid></search><sort><creationdate>20230601</creationdate><title>Thermal hazard assessment by TGA, DSC, and ARC experimental and simulated thermokinetic approaches for trinitrophloroglucinol</title><author>Liu, Ye-Cheng ; Zhou, Hai-Lin ; Tang, Yan ; Li, You ; Zhai, Juan ; Jiang, Jun-Cheng ; Xing, Zhi-Xiang ; Huang, An-Chi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c392t-2d813f4c2a3c67f21fdacfae2664698aab63518b0e8abf7d74479d5ca8f04fc03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Absorption</topic><topic>Analytical Chemistry</topic><topic>Aromatic compounds</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Conjugation</topic><topic>Hazard assessment</topic><topic>Heat measurement</topic><topic>Information storage and retrieval</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Nitro compounds</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Safety</topic><topic>Thermogravimetry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Ye-Cheng</creatorcontrib><creatorcontrib>Zhou, Hai-Lin</creatorcontrib><creatorcontrib>Tang, Yan</creatorcontrib><creatorcontrib>Li, You</creatorcontrib><creatorcontrib>Zhai, Juan</creatorcontrib><creatorcontrib>Jiang, Jun-Cheng</creatorcontrib><creatorcontrib>Xing, Zhi-Xiang</creatorcontrib><creatorcontrib>Huang, An-Chi</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Ye-Cheng</au><au>Zhou, Hai-Lin</au><au>Tang, Yan</au><au>Li, You</au><au>Zhai, Juan</au><au>Jiang, Jun-Cheng</au><au>Xing, Zhi-Xiang</au><au>Huang, An-Chi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Thermal hazard assessment by TGA, DSC, and ARC experimental and simulated thermokinetic approaches for trinitrophloroglucinol</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2023-06-01</date><risdate>2023</risdate><volume>148</volume><issue>11</issue><spage>5039</spage><epage>5049</epage><pages>5039-5049</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><abstract>Hazardous chemicals often have the characteristics of high-energy and high-risk, and environmental factors have a significant impact on them. Trinitrophloroglucinol, as an essential energetic intermediate, is widely used in the modern military, aerospace, and energy fields. It is the representative substance of aromatic nitro compounds. Due to the unique properties of nitro, it has both an electron absorption conjugation effect and an electron absorption induction effect. These two effects lead to nitro becoming an electron absorption group, giving it high energy. For such dangerous substances containing nitro, it is of far-reaching significance to study the impact of environmental changes on their safety status. To determine the thermal safety performance of these substances in different external environments, different calorimetric devices, including thermogravimetry, differential scanning calorimetry, and accelerating rate calorimeter, are used to simulate different storage environments. Combined with calorimetric data, thermokinetic models suitable for trinitrophloroglucinol were established for thermal safety analysis. 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| subjects | Absorption Analytical Chemistry Aromatic compounds Chemistry Chemistry and Materials Science Conjugation Hazard assessment Heat measurement Information storage and retrieval Inorganic Chemistry Measurement Science and Instrumentation Nitro compounds Physical Chemistry Polymer Sciences Safety Thermogravimetry |
| title | Thermal hazard assessment by TGA, DSC, and ARC experimental and simulated thermokinetic approaches for trinitrophloroglucinol |
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