Increasing Thermal Stability of the Surface of Submicrocrystalline Nickel under High-Fluence Ion Irradiation

— The results of an experimental study of the effect of high-fluence ion irradiation on the thermal stability of the microstructure and surface relief of submicrocrystalline nickel are presented and discussed. The submicron structure of nickel is obtained during severe plastic deformation by torsion...

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Veröffentlicht in:Surface investigation, x-ray, synchrotron and neutron techniques x-ray, synchrotron and neutron techniques, 2023-02, Vol.17 (1), p.54-58
Hauptverfasser: Borisov, A. M., Mashkova, E. S., Ovchinnikov, M. A., Khisamov, R. K., Musabirov, I. I., Shayakhmetov, R. U., Mulyukov, R. R.
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container_title Surface investigation, x-ray, synchrotron and neutron techniques
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creator Borisov, A. M.
Mashkova, E. S.
Ovchinnikov, M. A.
Khisamov, R. K.
Musabirov, I. I.
Shayakhmetov, R. U.
Mulyukov, R. R.
description — The results of an experimental study of the effect of high-fluence ion irradiation on the thermal stability of the microstructure and surface relief of submicrocrystalline nickel are presented and discussed. The submicron structure of nickel is obtained during severe plastic deformation by torsion under a high pressure of 6 GPa. Irradiation with 30-keV argon ions with a dose of 3 × 10 18 cm –2 is carried out. The ion irradiation of submicrocrystalline nickel is shown to lead to the formation of a cone-shaped surface morphology. This morphology is thermally stable up to a temperature of at least 500°C. Using etching with a focused 30‑keV gallium-ion beam, a surface layer 10-µm thick of irradiated submicrocrystalline nickel annealed at 500°С is studied. It is found that the ion-induced cone-shaped morphology of the surface could be preserved during annealing and block grain growth in the surface layer.
doi_str_mv 10.1134/S102745102301007X
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M. ; Mashkova, E. S. ; Ovchinnikov, M. A. ; Khisamov, R. K. ; Musabirov, I. I. ; Shayakhmetov, R. U. ; Mulyukov, R. R.</creator><creatorcontrib>Borisov, A. M. ; Mashkova, E. S. ; Ovchinnikov, M. A. ; Khisamov, R. K. ; Musabirov, I. I. ; Shayakhmetov, R. U. ; Mulyukov, R. R.</creatorcontrib><description>— The results of an experimental study of the effect of high-fluence ion irradiation on the thermal stability of the microstructure and surface relief of submicrocrystalline nickel are presented and discussed. The submicron structure of nickel is obtained during severe plastic deformation by torsion under a high pressure of 6 GPa. Irradiation with 30-keV argon ions with a dose of 3 × 10 18 cm –2 is carried out. The ion irradiation of submicrocrystalline nickel is shown to lead to the formation of a cone-shaped surface morphology. This morphology is thermally stable up to a temperature of at least 500°C. Using etching with a focused 30‑keV gallium-ion beam, a surface layer 10-µm thick of irradiated submicrocrystalline nickel annealed at 500°С is studied. It is found that the ion-induced cone-shaped morphology of the surface could be preserved during annealing and block grain growth in the surface layer.</description><identifier>ISSN: 1027-4510</identifier><identifier>EISSN: 1819-7094</identifier><identifier>DOI: 10.1134/S102745102301007X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Annealing ; Argon ions ; Chemistry and Materials Science ; Fluence ; Gallium ; Grain growth ; Ion beams ; Ion irradiation ; Materials Science ; Morphology ; Nickel ; Plastic deformation ; Surface layers ; Surface stability ; Surfaces and Interfaces ; Thermal stability ; Thin Films</subject><ispartof>Surface investigation, x-ray, synchrotron and neutron techniques, 2023-02, Vol.17 (1), p.54-58</ispartof><rights>Pleiades Publishing, Ltd. 2023. 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subjects Annealing
Argon ions
Chemistry and Materials Science
Fluence
Gallium
Grain growth
Ion beams
Ion irradiation
Materials Science
Morphology
Nickel
Plastic deformation
Surface layers
Surface stability
Surfaces and Interfaces
Thermal stability
Thin Films
title Increasing Thermal Stability of the Surface of Submicrocrystalline Nickel under High-Fluence Ion Irradiation
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