Analysis of Small-Mass Biological Samples by ICP MS Using Microwave Acid Digestion of Several Samples in the Common Atmosphere of a Standard Autoclave
To expand the available tools for the analysis of samples of biological and plant origin of small mass (10–20 mg) using ICP MS, we developed a construction made of three compact teflon reaction minivessels (inserts) of an internal volume of 3 mL, placed in a standard autoclave (EasyPrep) of a volume...
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| Veröffentlicht in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2023-03, Vol.78 (3), p.324-329 |
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| container_title | Journal of analytical chemistry (New York, N.Y.) |
| container_volume | 78 |
| creator | Kolotov, V. P. Dogadkin, D. N. Zaichik, V. E. Shirokova, V. I. Dogadkin, N. N. |
| description | To expand the available tools for the analysis of samples of biological and plant origin of small mass (10–20 mg) using ICP MS, we developed a construction made of three compact teflon reaction minivessels (inserts) of an internal volume of 3 mL, placed in a standard autoclave (EasyPrep) of a volume of 100 cm
3
of a MARS-5 microwave system (CEM). The acid digestion of samples in reaction minivessels requires no more than 1.5 mL of highly pure acids. The digestion of samples proceeds in the common gas atmosphere of a standard autoclave filled with a needed volume of acids of pure for analysis grade. The method was tested on reference materials of plants and biological sample. The results obtained are in agreement with the certified values. The developed method ensures the decrease of the detection limits and obtaining new data on the concentrations of B, Ga, Y, Nb, Tl, Bi, and a number of rare-earth elements in the reference materials. |
| doi_str_mv | 10.1134/S1061934823030061 |
| format | Article |
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3
of a MARS-5 microwave system (CEM). The acid digestion of samples in reaction minivessels requires no more than 1.5 mL of highly pure acids. The digestion of samples proceeds in the common gas atmosphere of a standard autoclave filled with a needed volume of acids of pure for analysis grade. The method was tested on reference materials of plants and biological sample. The results obtained are in agreement with the certified values. The developed method ensures the decrease of the detection limits and obtaining new data on the concentrations of B, Ga, Y, Nb, Tl, Bi, and a number of rare-earth elements in the reference materials.</description><identifier>ISSN: 1061-9348</identifier><identifier>EISSN: 1608-3199</identifier><identifier>DOI: 10.1134/S1061934823030061</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Acid digestion ; Analysis ; Analytical Chemistry ; Autoclaves ; Biological effects ; Biological products ; Biological properties ; Chemistry ; Chemistry and Materials Science ; Inductively coupled plasma mass spectrometry ; Inserts ; Methods ; Polytetrafluoroethylene ; Rare earth elements ; Reference materials</subject><ispartof>Journal of analytical chemistry (New York, N.Y.), 2023-03, Vol.78 (3), p.324-329</ispartof><rights>Pleiades Publishing, Ltd. 2023. ISSN 1061-9348, Journal of Analytical Chemistry, 2023, Vol. 78, No. 3, pp. 324–329. © Pleiades Publishing, Ltd., 2023. Russian Text © The Author(s), 2023, published in Zhurnal Analiticheskoi Khimii, 2023, Vol. 78, No. 3, pp. 216–222.</rights><rights>COPYRIGHT 2023 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c455t-603d50e44b8139713e684900df8c0b5335a3c679ca5cf59ea9cec398fa1ea6df3</citedby><cites>FETCH-LOGICAL-c455t-603d50e44b8139713e684900df8c0b5335a3c679ca5cf59ea9cec398fa1ea6df3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1061934823030061$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1061934823030061$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,777,781,27905,27906,41469,42538,51300</link.rule.ids></links><search><creatorcontrib>Kolotov, V. P.</creatorcontrib><creatorcontrib>Dogadkin, D. N.</creatorcontrib><creatorcontrib>Zaichik, V. E.</creatorcontrib><creatorcontrib>Shirokova, V. I.</creatorcontrib><creatorcontrib>Dogadkin, N. N.</creatorcontrib><title>Analysis of Small-Mass Biological Samples by ICP MS Using Microwave Acid Digestion of Several Samples in the Common Atmosphere of a Standard Autoclave</title><title>Journal of analytical chemistry (New York, N.Y.)</title><addtitle>J Anal Chem</addtitle><description>To expand the available tools for the analysis of samples of biological and plant origin of small mass (10–20 mg) using ICP MS, we developed a construction made of three compact teflon reaction minivessels (inserts) of an internal volume of 3 mL, placed in a standard autoclave (EasyPrep) of a volume of 100 cm
3
of a MARS-5 microwave system (CEM). The acid digestion of samples in reaction minivessels requires no more than 1.5 mL of highly pure acids. The digestion of samples proceeds in the common gas atmosphere of a standard autoclave filled with a needed volume of acids of pure for analysis grade. The method was tested on reference materials of plants and biological sample. The results obtained are in agreement with the certified values. The developed method ensures the decrease of the detection limits and obtaining new data on the concentrations of B, Ga, Y, Nb, Tl, Bi, and a number of rare-earth elements in the reference materials.</description><subject>Acid digestion</subject><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Autoclaves</subject><subject>Biological effects</subject><subject>Biological products</subject><subject>Biological properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Inductively coupled plasma mass spectrometry</subject><subject>Inserts</subject><subject>Methods</subject><subject>Polytetrafluoroethylene</subject><subject>Rare earth elements</subject><subject>Reference materials</subject><issn>1061-9348</issn><issn>1608-3199</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp1ksFu1DAQhiNEJUrLA3CzxIlDir1OsvYxLKWs1BWI0HM064xTV4m92N7SfZE-bx0WqaxY5INH4-__Nfo9WfaW0QvGePGhYbRikhdiximnqX6RnbKKipwzKV-mOrXy6f1V9jqEO0qpFKw6zR5rC8MumECcJs0Iw5CvIATy0bjB9UbBQBoYNwMGst6R5eIbWTXkJhjbk5VR3v2CeyS1Mh35ZHoM0Tj72wnv0f-lNZbEWyQLN44JqOPowuYWPU4skCaC7cB3pN5Gp4ZkeZ6daBgCvvlzn2U3ny9_LL7k11-vlov6OldFWca8orwrKRbFWjAu54xjJQpJaaeFouuS8xK4quZSQal0KRGkQsWl0MAQqk7zs-zd3nfj3c9tmr-9c1ufIgntTDDKhJjN6TPVw4CtsdpFD2o0QbX1PEUuhKgmKj9C9WinJJxFbVL7gL84wqfT4WjUUcH7A0FiIj7EHrYhtMvm-yHL9mz6oxA86nbjzQh-1zLaThvT_rMxSTPba0JibY_-OYz_i54AASe_xQ</recordid><startdate>20230301</startdate><enddate>20230301</enddate><creator>Kolotov, V. P.</creator><creator>Dogadkin, D. N.</creator><creator>Zaichik, V. E.</creator><creator>Shirokova, V. I.</creator><creator>Dogadkin, N. N.</creator><general>Pleiades Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>20230301</creationdate><title>Analysis of Small-Mass Biological Samples by ICP MS Using Microwave Acid Digestion of Several Samples in the Common Atmosphere of a Standard Autoclave</title><author>Kolotov, V. P. ; Dogadkin, D. N. ; Zaichik, V. E. ; Shirokova, V. I. ; Dogadkin, N. N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c455t-603d50e44b8139713e684900df8c0b5335a3c679ca5cf59ea9cec398fa1ea6df3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Acid digestion</topic><topic>Analysis</topic><topic>Analytical Chemistry</topic><topic>Autoclaves</topic><topic>Biological effects</topic><topic>Biological products</topic><topic>Biological properties</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Inductively coupled plasma mass spectrometry</topic><topic>Inserts</topic><topic>Methods</topic><topic>Polytetrafluoroethylene</topic><topic>Rare earth elements</topic><topic>Reference materials</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kolotov, V. P.</creatorcontrib><creatorcontrib>Dogadkin, D. N.</creatorcontrib><creatorcontrib>Zaichik, V. E.</creatorcontrib><creatorcontrib>Shirokova, V. I.</creatorcontrib><creatorcontrib>Dogadkin, N. N.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kolotov, V. P.</au><au>Dogadkin, D. N.</au><au>Zaichik, V. E.</au><au>Shirokova, V. I.</au><au>Dogadkin, N. N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Analysis of Small-Mass Biological Samples by ICP MS Using Microwave Acid Digestion of Several Samples in the Common Atmosphere of a Standard Autoclave</atitle><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle><stitle>J Anal Chem</stitle><date>2023-03-01</date><risdate>2023</risdate><volume>78</volume><issue>3</issue><spage>324</spage><epage>329</epage><pages>324-329</pages><issn>1061-9348</issn><eissn>1608-3199</eissn><abstract>To expand the available tools for the analysis of samples of biological and plant origin of small mass (10–20 mg) using ICP MS, we developed a construction made of three compact teflon reaction minivessels (inserts) of an internal volume of 3 mL, placed in a standard autoclave (EasyPrep) of a volume of 100 cm
3
of a MARS-5 microwave system (CEM). The acid digestion of samples in reaction minivessels requires no more than 1.5 mL of highly pure acids. The digestion of samples proceeds in the common gas atmosphere of a standard autoclave filled with a needed volume of acids of pure for analysis grade. The method was tested on reference materials of plants and biological sample. The results obtained are in agreement with the certified values. The developed method ensures the decrease of the detection limits and obtaining new data on the concentrations of B, Ga, Y, Nb, Tl, Bi, and a number of rare-earth elements in the reference materials.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1061934823030061</doi><tpages>6</tpages></addata></record> |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Acid digestion Analysis Analytical Chemistry Autoclaves Biological effects Biological products Biological properties Chemistry Chemistry and Materials Science Inductively coupled plasma mass spectrometry Inserts Methods Polytetrafluoroethylene Rare earth elements Reference materials |
| title | Analysis of Small-Mass Biological Samples by ICP MS Using Microwave Acid Digestion of Several Samples in the Common Atmosphere of a Standard Autoclave |
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