Catalytic Application of Electrochemically Prepared Nickel Oxide Nanoparticles to Synthesize 2, 5–Disubstituted-1, 3, 4–Oxadiazoles
The present work aims to synthesize 2,5–disubstituted-1,3,4–oxadiazoles using electrochemically prepared nanoparticles of nickel oxide as catalyst. The nanoparticles thus prepared using electrochemical syntheses are in appreciable yield. The tetrabutyl phosphonium bromide has been used for capping f...
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Veröffentlicht in: | Oriental journal of chemistry 2020-04, Vol.36 (2), p.300-308 |
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creator | R. Sawant, Manisha Gaikwad, Suresh T. Dare, Sushama B. Rajbhoj, Anjali S. |
description | The present work aims to synthesize 2,5–disubstituted-1,3,4–oxadiazoles using electrochemically prepared nanoparticles of nickel oxide as catalyst. The nanoparticles thus prepared using electrochemical syntheses are in appreciable yield. The tetrabutyl phosphonium bromide has been used for capping followed by UV, FTIR, XRD, SEM EDS and TEM SAED studies for the characterization. The 2,5-disubstituted-1,3,4-oxadiazoles were synthesized from substituted benzoic acids and their hydrazides in microwave synthesis system using prepared nanoparticles as a catalyst. |
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subjects | Benzoic acid Catalysts Drug delivery systems Electrolytes Fourier transforms Hydrazides Ligands Morphology Nanoparticles Nickel Nickel oxides Oxadiazoles Particle size Scanning electron microscopy |
title | Catalytic Application of Electrochemically Prepared Nickel Oxide Nanoparticles to Synthesize 2, 5–Disubstituted-1, 3, 4–Oxadiazoles |
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