Catalytic Application of Electrochemically Prepared Nickel Oxide Nanoparticles to Synthesize 2, 5–Disubstituted-1, 3, 4–Oxadiazoles

The present work aims to synthesize 2,5–disubstituted-1,3,4–oxadiazoles using electrochemically prepared nanoparticles of nickel oxide as catalyst. The nanoparticles thus prepared using electrochemical syntheses are in appreciable yield. The tetrabutyl phosphonium bromide has been used for capping f...

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Veröffentlicht in:Oriental journal of chemistry 2020-04, Vol.36 (2), p.300-308
Hauptverfasser: R. Sawant, Manisha, Gaikwad, Suresh T., Dare, Sushama B., Rajbhoj, Anjali S.
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container_end_page 308
container_issue 2
container_start_page 300
container_title Oriental journal of chemistry
container_volume 36
creator R. Sawant, Manisha
Gaikwad, Suresh T.
Dare, Sushama B.
Rajbhoj, Anjali S.
description The present work aims to synthesize 2,5–disubstituted-1,3,4–oxadiazoles using electrochemically prepared nanoparticles of nickel oxide as catalyst. The nanoparticles thus prepared using electrochemical syntheses are in appreciable yield. The tetrabutyl phosphonium bromide has been used for capping followed by UV, FTIR, XRD, SEM EDS and TEM SAED studies for the characterization. The 2,5-disubstituted-1,3,4-oxadiazoles were synthesized from substituted benzoic acids and their hydrazides in microwave synthesis system using prepared nanoparticles as a catalyst.
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subjects Benzoic acid
Catalysts
Drug delivery systems
Electrolytes
Fourier transforms
Hydrazides
Ligands
Morphology
Nanoparticles
Nickel
Nickel oxides
Oxadiazoles
Particle size
Scanning electron microscopy
title Catalytic Application of Electrochemically Prepared Nickel Oxide Nanoparticles to Synthesize 2, 5–Disubstituted-1, 3, 4–Oxadiazoles
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