The Formation of Doped PZT Solid Solution and Its Structural Characterization
The main objective of this work is the synthesis, structural and morphological characterization of ceramics materials. Abbreviated PZT-PYN. Ferroelectric ceramics of general formulation Pb(ZrxTi1-x)O3 are massively used in many fields such as medicine or aeronautics because of their dielectric and e...
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| Veröffentlicht in: | Annales de chimie (Paris. 1914) 2022-10, Vol.46 (5), p.281-285 |
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| container_title | Annales de chimie (Paris. 1914) |
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| creator | Keltoum, Kribaa O. Zenkhri, Louiza Boutarfaia, Ahmed |
| description | The main objective of this work is the synthesis, structural and morphological characterization of ceramics materials. Abbreviated PZT-PYN. Ferroelectric ceramics of general formulation Pb(ZrxTi1-x)O3 are massively used in many fields such as medicine or aeronautics because of their dielectric and electromechanical properties, although the electronic properties of doped PZT are much better compared to undoped PZT. Samples selected for this study were prepared bins solid way. The thermal treatment called calcination was applied to these compositions is carried around: 450℃, 550℃, 650℃, 750℃, and 900℃ for two hours with a Vitesse of 2℃ / min., then sintered at different temperatures: 1100℃, 1150℃, 1180℃, successively to optimize the sintering temperature where the product is better physical quality. Different techniques of characterization were used such as scanning electron microscopy (SEM), x-ray diffraction (XRD) analysis, and Energy-dispersive spectrometric, which showed that the response is optimal for the compositions included in the morphotropic phase boundary, achieves excellent properties. |
| doi_str_mv | 10.18280/acsm.460507 |
| format | Article |
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Abbreviated PZT-PYN. Ferroelectric ceramics of general formulation Pb(ZrxTi1-x)O3 are massively used in many fields such as medicine or aeronautics because of their dielectric and electromechanical properties, although the electronic properties of doped PZT are much better compared to undoped PZT. Samples selected for this study were prepared bins solid way. The thermal treatment called calcination was applied to these compositions is carried around: 450℃, 550℃, 650℃, 750℃, and 900℃ for two hours with a Vitesse of 2℃ / min., then sintered at different temperatures: 1100℃, 1150℃, 1180℃, successively to optimize the sintering temperature where the product is better physical quality. Different techniques of characterization were used such as scanning electron microscopy (SEM), x-ray diffraction (XRD) analysis, and Energy-dispersive spectrometric, which showed that the response is optimal for the compositions included in the morphotropic phase boundary, achieves excellent properties.</description><identifier>ISSN: 0151-9107</identifier><identifier>EISSN: 1958-5934</identifier><identifier>DOI: 10.18280/acsm.460507</identifier><language>eng</language><publisher>Edmonton: International Information and Engineering Technology Association (IIETA)</publisher><subject>Aeronautics ; Ceramics ; Composition ; Crystal lattices ; Ferroelectricity ; Heat ; Heat treatment ; Lead zirconate titanates ; Nanocrystals ; Optimization ; Particle size ; Scanning electron microscopy ; Solid solutions ; Spectrometry ; Structural analysis ; Titanium ; Zirconium ; Zirconium oxides</subject><ispartof>Annales de chimie (Paris. 1914), 2022-10, Vol.46 (5), p.281-285</ispartof><rights>2022. 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Ferroelectric ceramics of general formulation Pb(ZrxTi1-x)O3 are massively used in many fields such as medicine or aeronautics because of their dielectric and electromechanical properties, although the electronic properties of doped PZT are much better compared to undoped PZT. Samples selected for this study were prepared bins solid way. The thermal treatment called calcination was applied to these compositions is carried around: 450℃, 550℃, 650℃, 750℃, and 900℃ for two hours with a Vitesse of 2℃ / min., then sintered at different temperatures: 1100℃, 1150℃, 1180℃, successively to optimize the sintering temperature where the product is better physical quality. 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| source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals |
| subjects | Aeronautics Ceramics Composition Crystal lattices Ferroelectricity Heat Heat treatment Lead zirconate titanates Nanocrystals Optimization Particle size Scanning electron microscopy Solid solutions Spectrometry Structural analysis Titanium Zirconium Zirconium oxides |
| title | The Formation of Doped PZT Solid Solution and Its Structural Characterization |
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