Synchrotron X-ray measurements of cellulose in the cell wall of aged wood under uniaxial loading

The purpose of this study is to examine the effect of wood aging on the mechanical behavior at the cell-wall level. Synchrotron X-ray diffraction (XRD) measurements were performed to investigate the mechanical behavior of cellulose in the S layer of aged wood from a 250-year-old attic cabin beam. XR...

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Veröffentlicht in:Holzforschung 2023-04, Vol.77 (4), p.260-269
Hauptverfasser: Kojima, Erina, Yamasaki, Mariko, Lee, Chang-Goo, Sasaki, Yasutoshi
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Yamasaki, Mariko
Lee, Chang-Goo
Sasaki, Yasutoshi
description The purpose of this study is to examine the effect of wood aging on the mechanical behavior at the cell-wall level. Synchrotron X-ray diffraction (XRD) measurements were performed to investigate the mechanical behavior of cellulose in the S layer of aged wood from a 250-year-old attic cabin beam. XRD measurements under uniaxial loading were performed on the cellulose (004) plane; the results were compared with those of recent wood. The cellulose in aged wood exhibited a delayed response to both tensile and compressive loading compared with recent wood. Under compressive loading, cellulose showed an increase in maximum strain and a significant increase in the variation of cellulose orientation angle, indicating that it may exhibit buckling-like meandering behavior. These results could be explained based on the decrease in hemicellulose content in the cell wall due to wood aging. In other words, the results suggested that an amorphous material in the cell wall affected the mechanical behavior of wood at the cell-wall level.
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Synchrotron X-ray diffraction (XRD) measurements were performed to investigate the mechanical behavior of cellulose in the S layer of aged wood from a 250-year-old attic cabin beam. XRD measurements under uniaxial loading were performed on the cellulose (004) plane; the results were compared with those of recent wood. The cellulose in aged wood exhibited a delayed response to both tensile and compressive loading compared with recent wood. Under compressive loading, cellulose showed an increase in maximum strain and a significant increase in the variation of cellulose orientation angle, indicating that it may exhibit buckling-like meandering behavior. These results could be explained based on the decrease in hemicellulose content in the cell wall due to wood aging. 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source De Gruyter journals
subjects aged wood
Aging
Amorphous materials
Buckling
Cell walls
Cellulose
Delayed response
Hemicellulose
mechanical behavior
Mechanical properties
Synchrotron radiation
Synchrotrons
wood cell wall
X-ray diffraction
title Synchrotron X-ray measurements of cellulose in the cell wall of aged wood under uniaxial loading
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