Identification of a pseudo-ternary intermetallic compound in the stirred zone of friction-stir-welded 5083 aluminum alloy with 316L steel
Macrostructure, microstructure, and distribution of phases through the interface were analyzed for friction-stir-welded joints 5083 aluminum alloy and 316L steel. Several analytical techniques, including light microscopy, transmission and scanning electron microscopy, elemental analysis using X-ray...
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| Veröffentlicht in: | Journal of materials science 2023-03, Vol.58 (12), p.5516-5529 |
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| creator | Celis, Mayerling Martinez Harcuba, Petr Veselý, Jozef Moisy, Florent Picot, Florent Retoux, Richard Domenges, Bernadette Hug, Eric |
| description | Macrostructure, microstructure, and distribution of phases through the interface were analyzed for friction-stir-welded joints 5083 aluminum alloy and 316L steel. Several analytical techniques, including light microscopy, transmission and scanning electron microscopy, elemental analysis using X-ray spectroscopy, and electron diffraction, were used to thoroughly analyze the weld interface. The interface is characterized by a significant reduction in grain size for both aluminum alloy and stainless steel. New compounds, not corresponding to thermodynamically stable phases in the binary Al–Fe phase diagram, were found in the stirred zone (SZ) as dispersed particles. On the steel side of the welding, thin slabs of new compounds were found, as well, being interlaced with the stainless steel. The observations support that the grain refinement of stainless steel is likely due to a continuous dynamic recrystallization. The intermetallic compounds present as a layer at the interface, exhibiting nanometric grain size, were identified by electron diffraction as Al
13
Fe
4
and Al
5
Fe
2
phases. Concerning the intermetallic compound formed in SZ, the elemental analysis showed a compound containing principally Al and Fe, with admixture of Si and Mn. It was concluded that it is a pseudo-ternary compound with body-centered cubic structure,
Im
-3 space group, which is for the first time reported in this kind of dissimilar assembly, and is known as α-Al(Fe,Mn)Si. |
| doi_str_mv | 10.1007/s10853-023-08312-x |
| format | Article |
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13
Fe
4
and Al
5
Fe
2
phases. Concerning the intermetallic compound formed in SZ, the elemental analysis showed a compound containing principally Al and Fe, with admixture of Si and Mn. It was concluded that it is a pseudo-ternary compound with body-centered cubic structure,
Im
-3 space group, which is for the first time reported in this kind of dissimilar assembly, and is known as α-Al(Fe,Mn)Si.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-023-08312-x</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Alloys ; Aluminum ; Aluminum alloys ; Aluminum base alloys ; Analysis ; Austenitic stainless steels ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Classical Mechanics ; Crystallography and Scattering Methods ; Dynamic recrystallization ; Electron diffraction ; Friction stir welding ; Grain refinement ; Grain size ; Intermetallic compounds ; Iron ; Macrostructure ; Manganese ; Materials Science ; Metals & Corrosion ; Microscopy ; Optical microscopy ; Phase diagrams ; Phases ; Polymer Sciences ; Silicon ; Solid Mechanics ; Stainless steel ; Welded joints ; Welding</subject><ispartof>Journal of materials science, 2023-03, Vol.58 (12), p.5516-5529</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>COPYRIGHT 2023 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c392t-9dd655d989cbbb544a23094992f852a10164cdc9e1f1a30d9e1733c012cd88b93</citedby><cites>FETCH-LOGICAL-c392t-9dd655d989cbbb544a23094992f852a10164cdc9e1f1a30d9e1733c012cd88b93</cites><orcidid>0000-0002-7407-5545</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10853-023-08312-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10853-023-08312-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41466,42535,51296</link.rule.ids></links><search><creatorcontrib>Celis, Mayerling Martinez</creatorcontrib><creatorcontrib>Harcuba, Petr</creatorcontrib><creatorcontrib>Veselý, Jozef</creatorcontrib><creatorcontrib>Moisy, Florent</creatorcontrib><creatorcontrib>Picot, Florent</creatorcontrib><creatorcontrib>Retoux, Richard</creatorcontrib><creatorcontrib>Domenges, Bernadette</creatorcontrib><creatorcontrib>Hug, Eric</creatorcontrib><title>Identification of a pseudo-ternary intermetallic compound in the stirred zone of friction-stir-welded 5083 aluminum alloy with 316L steel</title><title>Journal of materials science</title><addtitle>J Mater Sci</addtitle><description>Macrostructure, microstructure, and distribution of phases through the interface were analyzed for friction-stir-welded joints 5083 aluminum alloy and 316L steel. Several analytical techniques, including light microscopy, transmission and scanning electron microscopy, elemental analysis using X-ray spectroscopy, and electron diffraction, were used to thoroughly analyze the weld interface. The interface is characterized by a significant reduction in grain size for both aluminum alloy and stainless steel. New compounds, not corresponding to thermodynamically stable phases in the binary Al–Fe phase diagram, were found in the stirred zone (SZ) as dispersed particles. On the steel side of the welding, thin slabs of new compounds were found, as well, being interlaced with the stainless steel. The observations support that the grain refinement of stainless steel is likely due to a continuous dynamic recrystallization. The intermetallic compounds present as a layer at the interface, exhibiting nanometric grain size, were identified by electron diffraction as Al
13
Fe
4
and Al
5
Fe
2
phases. Concerning the intermetallic compound formed in SZ, the elemental analysis showed a compound containing principally Al and Fe, with admixture of Si and Mn. It was concluded that it is a pseudo-ternary compound with body-centered cubic structure,
Im
-3 space group, which is for the first time reported in this kind of dissimilar assembly, and is known as α-Al(Fe,Mn)Si.</description><subject>Alloys</subject><subject>Aluminum</subject><subject>Aluminum alloys</subject><subject>Aluminum base alloys</subject><subject>Analysis</subject><subject>Austenitic stainless steels</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Crystallography and Scattering Methods</subject><subject>Dynamic recrystallization</subject><subject>Electron diffraction</subject><subject>Friction stir welding</subject><subject>Grain refinement</subject><subject>Grain size</subject><subject>Intermetallic compounds</subject><subject>Iron</subject><subject>Macrostructure</subject><subject>Manganese</subject><subject>Materials Science</subject><subject>Metals & Corrosion</subject><subject>Microscopy</subject><subject>Optical microscopy</subject><subject>Phase diagrams</subject><subject>Phases</subject><subject>Polymer Sciences</subject><subject>Silicon</subject><subject>Solid Mechanics</subject><subject>Stainless steel</subject><subject>Welded joints</subject><subject>Welding</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9UV1rFDEUHUTBtfYP-BTwyYe0-ZjMJI-lqF1YKKh9Dtl8bFMyyZpk6NZ_4L820xGkLxJCDveec7g3p-s-YHSBERovC0acUYhIu5xiAk-vug1mI4U9R_R1t0GIEEj6Ab_t3pXygBBiI8Gb7vfW2Fi981pVnyJIDihwLHY2CVabo8pPwMeGJltVCF4DnaZjmqNpZVDvLSjV52wN-JWiXeQue71YwaUBH20wrcnaVECFefJxnhoI6Qk8-noPKB52zcLa8L5741Qo9vzve9bdffn84_oG7m6_bq-vdlBTQSoUxgyMGcGF3u_3rO8VoUj0QhDHGVEY4aHXRguLHVYUmQZGSjXCRBvO94KedR9X32NOP2dbqnxIc1s0FElGLjhn_YAa62JlHVSw0keXala6HWMnr9uqzrf61dgTzjBHi-DTC0HjVHuqBzWXIrffv73kkpWrcyolWyeP2U_tqyVGcslTrnnKlqd8zlOemoiuotLI8WDzv7n_o_oD_tOjSg</recordid><startdate>20230301</startdate><enddate>20230301</enddate><creator>Celis, Mayerling Martinez</creator><creator>Harcuba, Petr</creator><creator>Veselý, Jozef</creator><creator>Moisy, Florent</creator><creator>Picot, Florent</creator><creator>Retoux, Richard</creator><creator>Domenges, Bernadette</creator><creator>Hug, Eric</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0002-7407-5545</orcidid></search><sort><creationdate>20230301</creationdate><title>Identification of a pseudo-ternary intermetallic compound in the stirred zone of friction-stir-welded 5083 aluminum alloy with 316L steel</title><author>Celis, Mayerling Martinez ; Harcuba, Petr ; Veselý, Jozef ; Moisy, Florent ; Picot, Florent ; Retoux, Richard ; Domenges, Bernadette ; Hug, Eric</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c392t-9dd655d989cbbb544a23094992f852a10164cdc9e1f1a30d9e1733c012cd88b93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Alloys</topic><topic>Aluminum</topic><topic>Aluminum alloys</topic><topic>Aluminum base alloys</topic><topic>Analysis</topic><topic>Austenitic stainless steels</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Classical Mechanics</topic><topic>Crystallography and Scattering Methods</topic><topic>Dynamic recrystallization</topic><topic>Electron diffraction</topic><topic>Friction stir welding</topic><topic>Grain refinement</topic><topic>Grain size</topic><topic>Intermetallic compounds</topic><topic>Iron</topic><topic>Macrostructure</topic><topic>Manganese</topic><topic>Materials Science</topic><topic>Metals & Corrosion</topic><topic>Microscopy</topic><topic>Optical microscopy</topic><topic>Phase diagrams</topic><topic>Phases</topic><topic>Polymer Sciences</topic><topic>Silicon</topic><topic>Solid Mechanics</topic><topic>Stainless steel</topic><topic>Welded joints</topic><topic>Welding</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Celis, Mayerling Martinez</creatorcontrib><creatorcontrib>Harcuba, Petr</creatorcontrib><creatorcontrib>Veselý, Jozef</creatorcontrib><creatorcontrib>Moisy, Florent</creatorcontrib><creatorcontrib>Picot, Florent</creatorcontrib><creatorcontrib>Retoux, Richard</creatorcontrib><creatorcontrib>Domenges, Bernadette</creatorcontrib><creatorcontrib>Hug, Eric</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Celis, Mayerling Martinez</au><au>Harcuba, Petr</au><au>Veselý, Jozef</au><au>Moisy, Florent</au><au>Picot, Florent</au><au>Retoux, Richard</au><au>Domenges, Bernadette</au><au>Hug, Eric</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Identification of a pseudo-ternary intermetallic compound in the stirred zone of friction-stir-welded 5083 aluminum alloy with 316L steel</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><date>2023-03-01</date><risdate>2023</risdate><volume>58</volume><issue>12</issue><spage>5516</spage><epage>5529</epage><pages>5516-5529</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>Macrostructure, microstructure, and distribution of phases through the interface were analyzed for friction-stir-welded joints 5083 aluminum alloy and 316L steel. Several analytical techniques, including light microscopy, transmission and scanning electron microscopy, elemental analysis using X-ray spectroscopy, and electron diffraction, were used to thoroughly analyze the weld interface. The interface is characterized by a significant reduction in grain size for both aluminum alloy and stainless steel. New compounds, not corresponding to thermodynamically stable phases in the binary Al–Fe phase diagram, were found in the stirred zone (SZ) as dispersed particles. On the steel side of the welding, thin slabs of new compounds were found, as well, being interlaced with the stainless steel. The observations support that the grain refinement of stainless steel is likely due to a continuous dynamic recrystallization. The intermetallic compounds present as a layer at the interface, exhibiting nanometric grain size, were identified by electron diffraction as Al
13
Fe
4
and Al
5
Fe
2
phases. Concerning the intermetallic compound formed in SZ, the elemental analysis showed a compound containing principally Al and Fe, with admixture of Si and Mn. It was concluded that it is a pseudo-ternary compound with body-centered cubic structure,
Im
-3 space group, which is for the first time reported in this kind of dissimilar assembly, and is known as α-Al(Fe,Mn)Si.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-023-08312-x</doi><tpages>14</tpages><orcidid>https://orcid.org/0000-0002-7407-5545</orcidid></addata></record> |
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| subjects | Alloys Aluminum Aluminum alloys Aluminum base alloys Analysis Austenitic stainless steels Characterization and Evaluation of Materials Chemistry and Materials Science Classical Mechanics Crystallography and Scattering Methods Dynamic recrystallization Electron diffraction Friction stir welding Grain refinement Grain size Intermetallic compounds Iron Macrostructure Manganese Materials Science Metals & Corrosion Microscopy Optical microscopy Phase diagrams Phases Polymer Sciences Silicon Solid Mechanics Stainless steel Welded joints Welding |
| title | Identification of a pseudo-ternary intermetallic compound in the stirred zone of friction-stir-welded 5083 aluminum alloy with 316L steel |
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