A starch-assisted innovative synthesis of spinel-structured and ferromagnetic behaviour of Fe3O4 nanoparticles catalytic activity evaluated in the selective oxidation
In this research work, for several temperature based on Fe 3 O 4 nanoparticles had been prepared by the sol–gel approach. The physicochemical properties of these catalysts were characterized by the X-ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), diffuse...
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| Veröffentlicht in: | SN applied sciences 2019-05, Vol.1 (5), p.472, Article 472 |
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| creator | Geetha, V. T. Puthilibai, G. Induja, S. |
| description | In this research work, for several temperature based on Fe
3
O
4
nanoparticles had been prepared by the sol–gel approach. The physicochemical properties of these catalysts were characterized by the X-ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), diffused reflectance spectra, photoluminescence spectroscopy (PL) and vibrating sample magnetometer. Fe
3
O
4
nanoparticles, TEM images and the XRD analysis designated that the chain-like Fe
3
O
4
has a crystal phase of cubic lattice by way for a mean measurement of around 25 nm. The effect of catalyst and solvent on the catalytic oxidation of benzyl alcohol using the Fe
3
O
4
catalyst prepared by sol–gel method was also investigated. |
| doi_str_mv | 10.1007/s42452-019-0450-3 |
| format | Article |
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3
O
4
nanoparticles had been prepared by the sol–gel approach. The physicochemical properties of these catalysts were characterized by the X-ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), diffused reflectance spectra, photoluminescence spectroscopy (PL) and vibrating sample magnetometer. Fe
3
O
4
nanoparticles, TEM images and the XRD analysis designated that the chain-like Fe
3
O
4
has a crystal phase of cubic lattice by way for a mean measurement of around 25 nm. The effect of catalyst and solvent on the catalytic oxidation of benzyl alcohol using the Fe
3
O
4
catalyst prepared by sol–gel method was also investigated.</description><identifier>ISSN: 2523-3963</identifier><identifier>EISSN: 2523-3971</identifier><identifier>DOI: 10.1007/s42452-019-0450-3</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>1. Chemistry (general) ; Applied and Technical Physics ; Benzyl alcohol ; Catalysts ; Catalytic activity ; Catalytic oxidation ; Chemistry/Food Science ; Crystal lattices ; Cubic lattice ; Earth Sciences ; Engineering ; Environment ; Ferromagnetism ; Iron oxides ; Materials Science ; Metal oxides ; Morphology ; Nanomaterials ; Nanoparticles ; Nanostructured materials ; Nitrates ; Oxidation ; Particle size ; Photoluminescence ; Photons ; Physicochemical properties ; Research Article ; Scanning electron microscopy ; Semiconductors ; Sol-gel processes ; Spectroscopy ; Transmission electron microscopy ; X-ray diffraction</subject><ispartof>SN applied sciences, 2019-05, Vol.1 (5), p.472, Article 472</ispartof><rights>Springer Nature Switzerland AG 2019</rights><rights>Springer Nature Switzerland AG 2019.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c359t-6f07e331bee9de9f573af599dcea5681a4257a78bdb81e20e51b0be8cb709c3b3</citedby><cites>FETCH-LOGICAL-c359t-6f07e331bee9de9f573af599dcea5681a4257a78bdb81e20e51b0be8cb709c3b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,777,781,27905,27906</link.rule.ids></links><search><creatorcontrib>Geetha, V. T.</creatorcontrib><creatorcontrib>Puthilibai, G.</creatorcontrib><creatorcontrib>Induja, S.</creatorcontrib><title>A starch-assisted innovative synthesis of spinel-structured and ferromagnetic behaviour of Fe3O4 nanoparticles catalytic activity evaluated in the selective oxidation</title><title>SN applied sciences</title><addtitle>SN Appl. Sci</addtitle><description>In this research work, for several temperature based on Fe
3
O
4
nanoparticles had been prepared by the sol–gel approach. The physicochemical properties of these catalysts were characterized by the X-ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), diffused reflectance spectra, photoluminescence spectroscopy (PL) and vibrating sample magnetometer. Fe
3
O
4
nanoparticles, TEM images and the XRD analysis designated that the chain-like Fe
3
O
4
has a crystal phase of cubic lattice by way for a mean measurement of around 25 nm. The effect of catalyst and solvent on the catalytic oxidation of benzyl alcohol using the Fe
3
O
4
catalyst prepared by sol–gel method was also investigated.</description><subject>1. Chemistry (general)</subject><subject>Applied and Technical Physics</subject><subject>Benzyl alcohol</subject><subject>Catalysts</subject><subject>Catalytic activity</subject><subject>Catalytic oxidation</subject><subject>Chemistry/Food Science</subject><subject>Crystal lattices</subject><subject>Cubic lattice</subject><subject>Earth Sciences</subject><subject>Engineering</subject><subject>Environment</subject><subject>Ferromagnetism</subject><subject>Iron oxides</subject><subject>Materials Science</subject><subject>Metal oxides</subject><subject>Morphology</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Nanostructured materials</subject><subject>Nitrates</subject><subject>Oxidation</subject><subject>Particle size</subject><subject>Photoluminescence</subject><subject>Photons</subject><subject>Physicochemical properties</subject><subject>Research Article</subject><subject>Scanning electron microscopy</subject><subject>Semiconductors</subject><subject>Sol-gel processes</subject><subject>Spectroscopy</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><issn>2523-3963</issn><issn>2523-3971</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp1kc1O3DAURiPUSkXAA3RnibVb_8RxvESoFKSR2NC1dePcMEbBHmxn1HmhPicegsqKlS37fPfY-prmO2c_OGP6Z25FqwRl3FDWKkblSXMqlJBUGs2__N938ltzkfMTY0xoI9tenjb_rkgukNyWQs4-FxyJDyHuofg9knwIZYv1nMSJ5J0PONNc0uLKkioJYSQTphSf4TFg8Y4MuIW9j0s6Bm5Q3rckQIg7SPV2xkwcFJgPRxRcVfhyILiHeYHVTKqOZJzRvfnjXz_Wl8Rw3nydYM548b6eNX9ufj1c39LN_e-766sNdVKZQruJaZSSD4hmRDMpLWFSxowOQXU9h1YoDbofxqHnKBgqPrABezdoZpwc5Flzuc7dpfiyYC72qX4mVKUVuu9bKTveVYqvlEsx54ST3SX_DOlgObPHRuzaiK2N2GMjVtaMWDO5suER08fkz0OvKhWTUw</recordid><startdate>20190501</startdate><enddate>20190501</enddate><creator>Geetha, V. T.</creator><creator>Puthilibai, G.</creator><creator>Induja, S.</creator><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20190501</creationdate><title>A starch-assisted innovative synthesis of spinel-structured and ferromagnetic behaviour of Fe3O4 nanoparticles catalytic activity evaluated in the selective oxidation</title><author>Geetha, V. T. ; Puthilibai, G. ; Induja, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c359t-6f07e331bee9de9f573af599dcea5681a4257a78bdb81e20e51b0be8cb709c3b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>1. Chemistry (general)</topic><topic>Applied and Technical Physics</topic><topic>Benzyl alcohol</topic><topic>Catalysts</topic><topic>Catalytic activity</topic><topic>Catalytic oxidation</topic><topic>Chemistry/Food Science</topic><topic>Crystal lattices</topic><topic>Cubic lattice</topic><topic>Earth Sciences</topic><topic>Engineering</topic><topic>Environment</topic><topic>Ferromagnetism</topic><topic>Iron oxides</topic><topic>Materials Science</topic><topic>Metal oxides</topic><topic>Morphology</topic><topic>Nanomaterials</topic><topic>Nanoparticles</topic><topic>Nanostructured materials</topic><topic>Nitrates</topic><topic>Oxidation</topic><topic>Particle size</topic><topic>Photoluminescence</topic><topic>Photons</topic><topic>Physicochemical properties</topic><topic>Research Article</topic><topic>Scanning electron microscopy</topic><topic>Semiconductors</topic><topic>Sol-gel processes</topic><topic>Spectroscopy</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Geetha, V. T.</creatorcontrib><creatorcontrib>Puthilibai, G.</creatorcontrib><creatorcontrib>Induja, S.</creatorcontrib><collection>CrossRef</collection><jtitle>SN applied sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Geetha, V. T.</au><au>Puthilibai, G.</au><au>Induja, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A starch-assisted innovative synthesis of spinel-structured and ferromagnetic behaviour of Fe3O4 nanoparticles catalytic activity evaluated in the selective oxidation</atitle><jtitle>SN applied sciences</jtitle><stitle>SN Appl. Sci</stitle><date>2019-05-01</date><risdate>2019</risdate><volume>1</volume><issue>5</issue><spage>472</spage><pages>472-</pages><artnum>472</artnum><issn>2523-3963</issn><eissn>2523-3971</eissn><abstract>In this research work, for several temperature based on Fe
3
O
4
nanoparticles had been prepared by the sol–gel approach. The physicochemical properties of these catalysts were characterized by the X-ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), diffused reflectance spectra, photoluminescence spectroscopy (PL) and vibrating sample magnetometer. Fe
3
O
4
nanoparticles, TEM images and the XRD analysis designated that the chain-like Fe
3
O
4
has a crystal phase of cubic lattice by way for a mean measurement of around 25 nm. The effect of catalyst and solvent on the catalytic oxidation of benzyl alcohol using the Fe
3
O
4
catalyst prepared by sol–gel method was also investigated.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s42452-019-0450-3</doi><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
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| ispartof | SN applied sciences, 2019-05, Vol.1 (5), p.472, Article 472 |
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| language | eng |
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| source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals |
| subjects | 1. Chemistry (general) Applied and Technical Physics Benzyl alcohol Catalysts Catalytic activity Catalytic oxidation Chemistry/Food Science Crystal lattices Cubic lattice Earth Sciences Engineering Environment Ferromagnetism Iron oxides Materials Science Metal oxides Morphology Nanomaterials Nanoparticles Nanostructured materials Nitrates Oxidation Particle size Photoluminescence Photons Physicochemical properties Research Article Scanning electron microscopy Semiconductors Sol-gel processes Spectroscopy Transmission electron microscopy X-ray diffraction |
| title | A starch-assisted innovative synthesis of spinel-structured and ferromagnetic behaviour of Fe3O4 nanoparticles catalytic activity evaluated in the selective oxidation |
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