Pure graphite as a reference material for the determination of trace elements: An interlaboratory collaborative study

Seven synthetic graphite powders of different grade of purity were analyzed by means of INAA, WDXRF, EDXRF, DC-OES directly and using ICP-MS, ICP-OES, ETAAS and FAAS in combination with various sample preparation techniques. On the basis of a statistical evaluation of the results obtained, for the t...

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Veröffentlicht in:Analytical and bioanalytical chemistry 1997-02, Vol.357 (3), p.266-273
Hauptverfasser: BÖGERSHAUSEN, W, CICCIARELLI, R, GERCKEN, B, KÖNIG, E, KRIVAN, V, MÜLLER-KÄFER, R, PAVEL, J, SELTNER, H, SCHELCHER, J
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container_end_page 273
container_issue 3
container_start_page 266
container_title Analytical and bioanalytical chemistry
container_volume 357
creator BÖGERSHAUSEN, W
CICCIARELLI, R
GERCKEN, B
KÖNIG, E
KRIVAN, V
MÜLLER-KÄFER, R
PAVEL, J
SELTNER, H
SCHELCHER, J
description Seven synthetic graphite powders of different grade of purity were analyzed by means of INAA, WDXRF, EDXRF, DC-OES directly and using ICP-MS, ICP-OES, ETAAS and FAAS in combination with various sample preparation techniques. On the basis of a statistical evaluation of the results obtained, for the trace elements Al, Ca, Cr, Cu, Fe, Mn and Ni, reference values were established and, for the elements As, Co, Mg, Mo, Pb, Sb, Si, Sr, Ti, V, Zn and Zr, informative values are given. The analyzed reference materials are commercially available.
doi_str_mv 10.1007/s002160050151
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identifier ISSN: 0937-0633
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subjects Aluminum
Analytical chemistry
Chemistry
Chromium
Copper
Exact sciences and technology
Graphite
Iron
Manganese
Molybdenum
Reference materials
Sample preparation
Spectrometric and optical methods
Titanium
Trace elements
Zirconium
title Pure graphite as a reference material for the determination of trace elements: An interlaboratory collaborative study
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