Pure graphite as a reference material for the determination of trace elements: An interlaboratory collaborative study
Seven synthetic graphite powders of different grade of purity were analyzed by means of INAA, WDXRF, EDXRF, DC-OES directly and using ICP-MS, ICP-OES, ETAAS and FAAS in combination with various sample preparation techniques. On the basis of a statistical evaluation of the results obtained, for the t...
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Veröffentlicht in: | Analytical and bioanalytical chemistry 1997-02, Vol.357 (3), p.266-273 |
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container_title | Analytical and bioanalytical chemistry |
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creator | BÖGERSHAUSEN, W CICCIARELLI, R GERCKEN, B KÖNIG, E KRIVAN, V MÜLLER-KÄFER, R PAVEL, J SELTNER, H SCHELCHER, J |
description | Seven synthetic graphite powders of different grade of purity were analyzed by means of INAA, WDXRF, EDXRF, DC-OES directly and using ICP-MS, ICP-OES, ETAAS and FAAS in combination with various sample preparation techniques. On the basis of a statistical evaluation of the results obtained, for the trace elements Al, Ca, Cr, Cu, Fe, Mn and Ni, reference values were established and, for the elements As, Co, Mg, Mo, Pb, Sb, Si, Sr, Ti, V, Zn and Zr, informative values are given. The analyzed reference materials are commercially available. |
doi_str_mv | 10.1007/s002160050151 |
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On the basis of a statistical evaluation of the results obtained, for the trace elements Al, Ca, Cr, Cu, Fe, Mn and Ni, reference values were established and, for the elements As, Co, Mg, Mo, Pb, Sb, Si, Sr, Ti, V, Zn and Zr, informative values are given. 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powders of different grade of purity were analyzed by means of INAA, WDXRF, EDXRF, DC-OES directly and using ICP-MS, ICP-OES, ETAAS and FAAS in combination with various sample preparation techniques. 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subjects | Aluminum Analytical chemistry Chemistry Chromium Copper Exact sciences and technology Graphite Iron Manganese Molybdenum Reference materials Sample preparation Spectrometric and optical methods Titanium Trace elements Zirconium |
title | Pure graphite as a reference material for the determination of trace elements: An interlaboratory collaborative study |
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