Microstructure and strain hardening behavior of the transformable 316L stainless steel processed by cryogenic pre-deformation
The dynamic formation of α′-martensite during mechanical loading is essential in achieving the desired mechanical properties of the metastable austenitic stainless steels (SS). However, the effect of α′-martensitic transformation on the mechanical behavior of 316L SS is less explored due to the over...
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description | The dynamic formation of α′-martensite during mechanical loading is essential in achieving the desired mechanical properties of the metastable austenitic stainless steels (SS). However, the effect of α′-martensitic transformation on the mechanical behavior of 316L SS is less explored due to the over stability of austenite at room temperature (RT). Here, a thermomechanical processing method of cryogenic pre-deformation is applied to tailor the deformation-induced martensitic transformation in 316L SS and the subsequent deformation behavior during mechanical testing at RT. Detailed characterizations reveal that the α′-martensite nucleated at the intersection of shear bands by cryogenic pre-deformation can continue to grow along the shear bands at RT. The cryogenically-rolled (CryoRolled) 316L SS exhibits an excellent combination of strength and ductility in comparison with the conventional cold-rolled counterparts, due to the proper activation of α′-martensitic transformation. The CryoRolled-12% sample presents a true tensile strength of 1143 MPa and a true uniform elongation of 0.17; while similar level of true tensile strength (1135 MPa) is obtained at the expense of low uniform elongation (0.024) for the RT-rolled-50% sample. A mean-field micromechanical model is applied to analyze the influence of the dynamic formation of the strengthening α′-martensite on the strain hardening behavior.
•Cryogenic Rolling enhances the martensitic transformation kinetics of 316L at RT.•The nucleation and growth of α′-martensite are characterized in details.•Cryogenic pre-deformed 316L shows a good combination of strength and ductility.•Continuous formation of α′-martensite leads to a high strain hardening capacity.•A micromechanical model is applied to analyze the strengthening contributions. |
doi_str_mv | 10.1016/j.msea.2022.144424 |
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•Cryogenic Rolling enhances the martensitic transformation kinetics of 316L at RT.•The nucleation and growth of α′-martensite are characterized in details.•Cryogenic pre-deformed 316L shows a good combination of strength and ductility.•Continuous formation of α′-martensite leads to a high strain hardening capacity.•A micromechanical model is applied to analyze the strengthening contributions.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2022.144424</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>316L stainless steel ; Austenitic stainless steels ; Cryoforming ; Cryogenic pre-deformation ; Deformation ; Deformation-induced martensitic transformation ; Edge dislocations ; Elongation ; Martensite ; Martensitic transformations ; Mechanical properties ; Mechanical tests ; Predeformation ; Room temperature ; Shear bands ; Strain hardening ; Tensile strength ; Thermomechanical treatment</subject><ispartof>Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2023-01, Vol.862, p.144424, Article 144424</ispartof><rights>2022 Elsevier B.V.</rights><rights>Copyright Elsevier BV Jan 18, 2023</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c328t-ce9a9e8b77c00fa9e18f3d0bc63705bc6b15f29552ef15ae4b77c2bfb67807d73</citedby><cites>FETCH-LOGICAL-c328t-ce9a9e8b77c00fa9e18f3d0bc63705bc6b15f29552ef15ae4b77c2bfb67807d73</cites><orcidid>0000-0001-8592-9545</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.msea.2022.144424$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,778,782,3539,27907,27908,45978</link.rule.ids></links><search><creatorcontrib>Wei, Yuntao</creatorcontrib><creatorcontrib>Lu, Qi</creatorcontrib><creatorcontrib>Kou, Zongde</creatorcontrib><creatorcontrib>Feng, Tao</creatorcontrib><creatorcontrib>Lai, Qingquan</creatorcontrib><title>Microstructure and strain hardening behavior of the transformable 316L stainless steel processed by cryogenic pre-deformation</title><title>Materials science & engineering. A, Structural materials : properties, microstructure and processing</title><description>The dynamic formation of α′-martensite during mechanical loading is essential in achieving the desired mechanical properties of the metastable austenitic stainless steels (SS). However, the effect of α′-martensitic transformation on the mechanical behavior of 316L SS is less explored due to the over stability of austenite at room temperature (RT). Here, a thermomechanical processing method of cryogenic pre-deformation is applied to tailor the deformation-induced martensitic transformation in 316L SS and the subsequent deformation behavior during mechanical testing at RT. Detailed characterizations reveal that the α′-martensite nucleated at the intersection of shear bands by cryogenic pre-deformation can continue to grow along the shear bands at RT. The cryogenically-rolled (CryoRolled) 316L SS exhibits an excellent combination of strength and ductility in comparison with the conventional cold-rolled counterparts, due to the proper activation of α′-martensitic transformation. The CryoRolled-12% sample presents a true tensile strength of 1143 MPa and a true uniform elongation of 0.17; while similar level of true tensile strength (1135 MPa) is obtained at the expense of low uniform elongation (0.024) for the RT-rolled-50% sample. A mean-field micromechanical model is applied to analyze the influence of the dynamic formation of the strengthening α′-martensite on the strain hardening behavior.
•Cryogenic Rolling enhances the martensitic transformation kinetics of 316L at RT.•The nucleation and growth of α′-martensite are characterized in details.•Cryogenic pre-deformed 316L shows a good combination of strength and ductility.•Continuous formation of α′-martensite leads to a high strain hardening capacity.•A micromechanical model is applied to analyze the strengthening contributions.</description><subject>316L stainless steel</subject><subject>Austenitic stainless steels</subject><subject>Cryoforming</subject><subject>Cryogenic pre-deformation</subject><subject>Deformation</subject><subject>Deformation-induced martensitic transformation</subject><subject>Edge dislocations</subject><subject>Elongation</subject><subject>Martensite</subject><subject>Martensitic transformations</subject><subject>Mechanical properties</subject><subject>Mechanical tests</subject><subject>Predeformation</subject><subject>Room temperature</subject><subject>Shear bands</subject><subject>Strain hardening</subject><subject>Tensile strength</subject><subject>Thermomechanical treatment</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kMtOwzAQRS0EEqXwA6wssU7wI4kTiQ2qeElFbGBtOfa4dZTGxU6QuuDfcShrVvO6Z2Z0EbqmJKeEVrddvougckYYy2lRFKw4QQtaC54VDa9O0YI0jGYlafg5uoixI4TQgpQL9P3qdPBxDJMepwBYDQanSrkBb1UwMLhhg1vYqi_nA_YWj1vAaT5E68NOtT1gTqt1YhLSQ4wpA-jxPnidKjC4PWAdDn6TVunUhszALzo6P1yiM6v6CFd_cYk-Hh_eV8_Z-u3pZXW_zjRn9ZhpaFQDdSuEJsSmlNaWG9LqigtSptDS0rKmLBlYWiooZiVrbVuJmggj-BLdHPemtz4niKPs_BSGdFIyUVPBaUNZUrGjanYkBrByH9xOhYOkRM42y07ONsvZZnm0OUF3RwjS_18OgozawaDBuAB6lMa7__AfHC2I0w</recordid><startdate>20230118</startdate><enddate>20230118</enddate><creator>Wei, Yuntao</creator><creator>Lu, Qi</creator><creator>Kou, Zongde</creator><creator>Feng, Tao</creator><creator>Lai, Qingquan</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0001-8592-9545</orcidid></search><sort><creationdate>20230118</creationdate><title>Microstructure and strain hardening behavior of the transformable 316L stainless steel processed by cryogenic pre-deformation</title><author>Wei, Yuntao ; Lu, Qi ; Kou, Zongde ; Feng, Tao ; Lai, Qingquan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c328t-ce9a9e8b77c00fa9e18f3d0bc63705bc6b15f29552ef15ae4b77c2bfb67807d73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>316L stainless steel</topic><topic>Austenitic stainless steels</topic><topic>Cryoforming</topic><topic>Cryogenic pre-deformation</topic><topic>Deformation</topic><topic>Deformation-induced martensitic transformation</topic><topic>Edge dislocations</topic><topic>Elongation</topic><topic>Martensite</topic><topic>Martensitic transformations</topic><topic>Mechanical properties</topic><topic>Mechanical tests</topic><topic>Predeformation</topic><topic>Room temperature</topic><topic>Shear bands</topic><topic>Strain hardening</topic><topic>Tensile strength</topic><topic>Thermomechanical treatment</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wei, Yuntao</creatorcontrib><creatorcontrib>Lu, Qi</creatorcontrib><creatorcontrib>Kou, Zongde</creatorcontrib><creatorcontrib>Feng, Tao</creatorcontrib><creatorcontrib>Lai, Qingquan</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wei, Yuntao</au><au>Lu, Qi</au><au>Kou, Zongde</au><au>Feng, Tao</au><au>Lai, Qingquan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microstructure and strain hardening behavior of the transformable 316L stainless steel processed by cryogenic pre-deformation</atitle><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2023-01-18</date><risdate>2023</risdate><volume>862</volume><spage>144424</spage><pages>144424-</pages><artnum>144424</artnum><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>The dynamic formation of α′-martensite during mechanical loading is essential in achieving the desired mechanical properties of the metastable austenitic stainless steels (SS). However, the effect of α′-martensitic transformation on the mechanical behavior of 316L SS is less explored due to the over stability of austenite at room temperature (RT). Here, a thermomechanical processing method of cryogenic pre-deformation is applied to tailor the deformation-induced martensitic transformation in 316L SS and the subsequent deformation behavior during mechanical testing at RT. Detailed characterizations reveal that the α′-martensite nucleated at the intersection of shear bands by cryogenic pre-deformation can continue to grow along the shear bands at RT. The cryogenically-rolled (CryoRolled) 316L SS exhibits an excellent combination of strength and ductility in comparison with the conventional cold-rolled counterparts, due to the proper activation of α′-martensitic transformation. The CryoRolled-12% sample presents a true tensile strength of 1143 MPa and a true uniform elongation of 0.17; while similar level of true tensile strength (1135 MPa) is obtained at the expense of low uniform elongation (0.024) for the RT-rolled-50% sample. A mean-field micromechanical model is applied to analyze the influence of the dynamic formation of the strengthening α′-martensite on the strain hardening behavior.
•Cryogenic Rolling enhances the martensitic transformation kinetics of 316L at RT.•The nucleation and growth of α′-martensite are characterized in details.•Cryogenic pre-deformed 316L shows a good combination of strength and ductility.•Continuous formation of α′-martensite leads to a high strain hardening capacity.•A micromechanical model is applied to analyze the strengthening contributions.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2022.144424</doi><orcidid>https://orcid.org/0000-0001-8592-9545</orcidid></addata></record> |
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subjects | 316L stainless steel Austenitic stainless steels Cryoforming Cryogenic pre-deformation Deformation Deformation-induced martensitic transformation Edge dislocations Elongation Martensite Martensitic transformations Mechanical properties Mechanical tests Predeformation Room temperature Shear bands Strain hardening Tensile strength Thermomechanical treatment |
title | Microstructure and strain hardening behavior of the transformable 316L stainless steel processed by cryogenic pre-deformation |
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