Room temperature operated hydrogen sensor using palladium coated on tapered optical fiber

•H2 sensor using tapered optical fiber coated with Palladium (Pd) NPs is proposed.•Absorbance decreases when tapered multimode fiber coated with Pd exposed to H2.•The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as NH3 and CH4. Gaseous pollutants s...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Materials science & engineering. B, Solid-state materials for advanced technology Solid-state materials for advanced technology, 2023-01, Vol.287, p.116092, Article 116092
Hauptverfasser: M. Alkhabet, Mohammed, H. Girei, Saad, K. Salih, Husam, Thabit, Rasha, Abdullah Issa, Mohammed, Paiman, Suriati, Arsad, Norhana, Thamer Alresheedi, Mohammed, A Mahdi, Mohd, H Yaacob, Mohd
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page
container_issue
container_start_page 116092
container_title Materials science & engineering. B, Solid-state materials for advanced technology
container_volume 287
creator M. Alkhabet, Mohammed
H. Girei, Saad
K. Salih, Husam
Thabit, Rasha
Abdullah Issa, Mohammed
Paiman, Suriati
Arsad, Norhana
Thamer Alresheedi, Mohammed
A Mahdi, Mohd
H Yaacob, Mohd
description •H2 sensor using tapered optical fiber coated with Palladium (Pd) NPs is proposed.•Absorbance decreases when tapered multimode fiber coated with Pd exposed to H2.•The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as NH3 and CH4. Gaseous pollutants such as hydrogen gas (H2) are present in daily human activities and have been studied extensively due to their high explosive and widespread use in many fields. A common H2 gas detector is electrically based. Although these electrical or conductometric sensors attain high sensitivity, they suffer from drawbacks, including poor selectivity, high operating temperature, and susceptibility to electromagnetic interference, which the optical-based sensor can improve. This study describes the development of a palladium-coated (Pd) optical fiber for the room temperature (H2) hydrogen application process. To improve the evanescent light field that propagates through the fiber, a multimode fiber was used to fabricate a transducing channel with cladding and core diameters of 125 μm and 62.5 μm respectively. The multimode optical fibers were tapered from 125 μm cladding diameters to 20 μm diameter, 10 mm waist-length, 5 mm to the up and down tapered region, and coated with Pd by using the drop-casting technique. Various characterization techniques have been used to characterize palladium, such as Field Emission Scanning Electron Microscopy (FESEM), X-ray energy scattering (EDX), X-ray Diffraction (XRD), and atomic force microscopy (AFM). The fabricated Pd-based sensor operates safely at room temperature with a gas concentration of 0.125 % to 2.00 % H2. The measured sensitivity, response, and recovery time were 18,645 %, 50 s, and 230 s, respectively. The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as ammonia (NH3) and methane (CH4). However, this study demonstrates reliable, efficient, and reproducible H2 detection using a simple and cost-effective method.
doi_str_mv 10.1016/j.mseb.2022.116092
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2778060658</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0921510722004809</els_id><sourcerecordid>2778060658</sourcerecordid><originalsourceid>FETCH-LOGICAL-c328t-d5dbfbfec04c26e2c456f3815545ffa7e673e1c93b6899638b92a95550fffedd3</originalsourceid><addsrcrecordid>eNp9kE1LxDAQhoMouK7-AU8Bz61J2qQteJHFL1gQRA-eQppM1pS2qUkr7L-33fXsaYbhfWaGB6FrSlJKqLht0i5CnTLCWEqpIBU7QStaFlmSV3l-ilbzhCackuIcXcTYEEIoY2yFPt-87_AI3QBBjVMA7A8dGPy1N8HvoMcR-ugDnqLrd3hQbauMmzqs_SHmezyqmVnaYXRatdi6GsIlOrOqjXD1V9fo4_HhffOcbF-fXjb320RnrBwTw01tawua5JoJYDrnwmYl5Tzn1qoCRJEB1VVWi7KqRFbWFVMV55xYa8GYbI1ujnuH4L8niKNs_BT6-aRkRVESQQQv5xQ7pnTwMQawcgiuU2EvKZGLQtnIRaFcFMqjwhm6O0Iw___jIMioHfQajAugR2m8-w__BR6Ee4c</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2778060658</pqid></control><display><type>article</type><title>Room temperature operated hydrogen sensor using palladium coated on tapered optical fiber</title><source>Elsevier ScienceDirect Journals</source><creator>M. Alkhabet, Mohammed ; H. Girei, Saad ; K. Salih, Husam ; Thabit, Rasha ; Abdullah Issa, Mohammed ; Paiman, Suriati ; Arsad, Norhana ; Thamer Alresheedi, Mohammed ; A Mahdi, Mohd ; H Yaacob, Mohd</creator><creatorcontrib>M. Alkhabet, Mohammed ; H. Girei, Saad ; K. Salih, Husam ; Thabit, Rasha ; Abdullah Issa, Mohammed ; Paiman, Suriati ; Arsad, Norhana ; Thamer Alresheedi, Mohammed ; A Mahdi, Mohd ; H Yaacob, Mohd</creatorcontrib><description>•H2 sensor using tapered optical fiber coated with Palladium (Pd) NPs is proposed.•Absorbance decreases when tapered multimode fiber coated with Pd exposed to H2.•The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as NH3 and CH4. Gaseous pollutants such as hydrogen gas (H2) are present in daily human activities and have been studied extensively due to their high explosive and widespread use in many fields. A common H2 gas detector is electrically based. Although these electrical or conductometric sensors attain high sensitivity, they suffer from drawbacks, including poor selectivity, high operating temperature, and susceptibility to electromagnetic interference, which the optical-based sensor can improve. This study describes the development of a palladium-coated (Pd) optical fiber for the room temperature (H2) hydrogen application process. To improve the evanescent light field that propagates through the fiber, a multimode fiber was used to fabricate a transducing channel with cladding and core diameters of 125 μm and 62.5 μm respectively. The multimode optical fibers were tapered from 125 μm cladding diameters to 20 μm diameter, 10 mm waist-length, 5 mm to the up and down tapered region, and coated with Pd by using the drop-casting technique. Various characterization techniques have been used to characterize palladium, such as Field Emission Scanning Electron Microscopy (FESEM), X-ray energy scattering (EDX), X-ray Diffraction (XRD), and atomic force microscopy (AFM). The fabricated Pd-based sensor operates safely at room temperature with a gas concentration of 0.125 % to 2.00 % H2. The measured sensitivity, response, and recovery time were 18,645 %, 50 s, and 230 s, respectively. The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as ammonia (NH3) and methane (CH4). However, this study demonstrates reliable, efficient, and reproducible H2 detection using a simple and cost-effective method.</description><identifier>ISSN: 0921-5107</identifier><identifier>EISSN: 1873-4944</identifier><identifier>DOI: 10.1016/j.mseb.2022.116092</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Ammonia ; Chemical sensors ; Cladding ; Diameters ; Drop-casting ; Electromagnetic interference ; Explosives detection ; Field emission microscopy ; Gas detectors ; Gases ; H2 gas ; Hydrogen ; Methane ; Microscopy ; Operating temperature ; Optical fibers ; Optical measuring instruments ; Palladium ; Palladium (Pd) ; Recovery time ; Room temperature ; Selectivity ; Sensitivity ; Tapered optical fiber</subject><ispartof>Materials science &amp; engineering. B, Solid-state materials for advanced technology, 2023-01, Vol.287, p.116092, Article 116092</ispartof><rights>2022 Elsevier B.V.</rights><rights>Copyright Elsevier BV Jan 2023</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c328t-d5dbfbfec04c26e2c456f3815545ffa7e673e1c93b6899638b92a95550fffedd3</citedby><cites>FETCH-LOGICAL-c328t-d5dbfbfec04c26e2c456f3815545ffa7e673e1c93b6899638b92a95550fffedd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.mseb.2022.116092$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,777,781,3537,27905,27906,45976</link.rule.ids></links><search><creatorcontrib>M. Alkhabet, Mohammed</creatorcontrib><creatorcontrib>H. Girei, Saad</creatorcontrib><creatorcontrib>K. Salih, Husam</creatorcontrib><creatorcontrib>Thabit, Rasha</creatorcontrib><creatorcontrib>Abdullah Issa, Mohammed</creatorcontrib><creatorcontrib>Paiman, Suriati</creatorcontrib><creatorcontrib>Arsad, Norhana</creatorcontrib><creatorcontrib>Thamer Alresheedi, Mohammed</creatorcontrib><creatorcontrib>A Mahdi, Mohd</creatorcontrib><creatorcontrib>H Yaacob, Mohd</creatorcontrib><title>Room temperature operated hydrogen sensor using palladium coated on tapered optical fiber</title><title>Materials science &amp; engineering. B, Solid-state materials for advanced technology</title><description>•H2 sensor using tapered optical fiber coated with Palladium (Pd) NPs is proposed.•Absorbance decreases when tapered multimode fiber coated with Pd exposed to H2.•The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as NH3 and CH4. Gaseous pollutants such as hydrogen gas (H2) are present in daily human activities and have been studied extensively due to their high explosive and widespread use in many fields. A common H2 gas detector is electrically based. Although these electrical or conductometric sensors attain high sensitivity, they suffer from drawbacks, including poor selectivity, high operating temperature, and susceptibility to electromagnetic interference, which the optical-based sensor can improve. This study describes the development of a palladium-coated (Pd) optical fiber for the room temperature (H2) hydrogen application process. To improve the evanescent light field that propagates through the fiber, a multimode fiber was used to fabricate a transducing channel with cladding and core diameters of 125 μm and 62.5 μm respectively. The multimode optical fibers were tapered from 125 μm cladding diameters to 20 μm diameter, 10 mm waist-length, 5 mm to the up and down tapered region, and coated with Pd by using the drop-casting technique. Various characterization techniques have been used to characterize palladium, such as Field Emission Scanning Electron Microscopy (FESEM), X-ray energy scattering (EDX), X-ray Diffraction (XRD), and atomic force microscopy (AFM). The fabricated Pd-based sensor operates safely at room temperature with a gas concentration of 0.125 % to 2.00 % H2. The measured sensitivity, response, and recovery time were 18,645 %, 50 s, and 230 s, respectively. The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as ammonia (NH3) and methane (CH4). However, this study demonstrates reliable, efficient, and reproducible H2 detection using a simple and cost-effective method.</description><subject>Ammonia</subject><subject>Chemical sensors</subject><subject>Cladding</subject><subject>Diameters</subject><subject>Drop-casting</subject><subject>Electromagnetic interference</subject><subject>Explosives detection</subject><subject>Field emission microscopy</subject><subject>Gas detectors</subject><subject>Gases</subject><subject>H2 gas</subject><subject>Hydrogen</subject><subject>Methane</subject><subject>Microscopy</subject><subject>Operating temperature</subject><subject>Optical fibers</subject><subject>Optical measuring instruments</subject><subject>Palladium</subject><subject>Palladium (Pd)</subject><subject>Recovery time</subject><subject>Room temperature</subject><subject>Selectivity</subject><subject>Sensitivity</subject><subject>Tapered optical fiber</subject><issn>0921-5107</issn><issn>1873-4944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LxDAQhoMouK7-AU8Bz61J2qQteJHFL1gQRA-eQppM1pS2qUkr7L-33fXsaYbhfWaGB6FrSlJKqLht0i5CnTLCWEqpIBU7QStaFlmSV3l-ilbzhCackuIcXcTYEEIoY2yFPt-87_AI3QBBjVMA7A8dGPy1N8HvoMcR-ugDnqLrd3hQbauMmzqs_SHmezyqmVnaYXRatdi6GsIlOrOqjXD1V9fo4_HhffOcbF-fXjb320RnrBwTw01tawua5JoJYDrnwmYl5Tzn1qoCRJEB1VVWi7KqRFbWFVMV55xYa8GYbI1ujnuH4L8niKNs_BT6-aRkRVESQQQv5xQ7pnTwMQawcgiuU2EvKZGLQtnIRaFcFMqjwhm6O0Iw___jIMioHfQajAugR2m8-w__BR6Ee4c</recordid><startdate>202301</startdate><enddate>202301</enddate><creator>M. Alkhabet, Mohammed</creator><creator>H. Girei, Saad</creator><creator>K. Salih, Husam</creator><creator>Thabit, Rasha</creator><creator>Abdullah Issa, Mohammed</creator><creator>Paiman, Suriati</creator><creator>Arsad, Norhana</creator><creator>Thamer Alresheedi, Mohammed</creator><creator>A Mahdi, Mohd</creator><creator>H Yaacob, Mohd</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>202301</creationdate><title>Room temperature operated hydrogen sensor using palladium coated on tapered optical fiber</title><author>M. Alkhabet, Mohammed ; H. Girei, Saad ; K. Salih, Husam ; Thabit, Rasha ; Abdullah Issa, Mohammed ; Paiman, Suriati ; Arsad, Norhana ; Thamer Alresheedi, Mohammed ; A Mahdi, Mohd ; H Yaacob, Mohd</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c328t-d5dbfbfec04c26e2c456f3815545ffa7e673e1c93b6899638b92a95550fffedd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Ammonia</topic><topic>Chemical sensors</topic><topic>Cladding</topic><topic>Diameters</topic><topic>Drop-casting</topic><topic>Electromagnetic interference</topic><topic>Explosives detection</topic><topic>Field emission microscopy</topic><topic>Gas detectors</topic><topic>Gases</topic><topic>H2 gas</topic><topic>Hydrogen</topic><topic>Methane</topic><topic>Microscopy</topic><topic>Operating temperature</topic><topic>Optical fibers</topic><topic>Optical measuring instruments</topic><topic>Palladium</topic><topic>Palladium (Pd)</topic><topic>Recovery time</topic><topic>Room temperature</topic><topic>Selectivity</topic><topic>Sensitivity</topic><topic>Tapered optical fiber</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>M. Alkhabet, Mohammed</creatorcontrib><creatorcontrib>H. Girei, Saad</creatorcontrib><creatorcontrib>K. Salih, Husam</creatorcontrib><creatorcontrib>Thabit, Rasha</creatorcontrib><creatorcontrib>Abdullah Issa, Mohammed</creatorcontrib><creatorcontrib>Paiman, Suriati</creatorcontrib><creatorcontrib>Arsad, Norhana</creatorcontrib><creatorcontrib>Thamer Alresheedi, Mohammed</creatorcontrib><creatorcontrib>A Mahdi, Mohd</creatorcontrib><creatorcontrib>H Yaacob, Mohd</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Materials science &amp; engineering. B, Solid-state materials for advanced technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>M. Alkhabet, Mohammed</au><au>H. Girei, Saad</au><au>K. Salih, Husam</au><au>Thabit, Rasha</au><au>Abdullah Issa, Mohammed</au><au>Paiman, Suriati</au><au>Arsad, Norhana</au><au>Thamer Alresheedi, Mohammed</au><au>A Mahdi, Mohd</au><au>H Yaacob, Mohd</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Room temperature operated hydrogen sensor using palladium coated on tapered optical fiber</atitle><jtitle>Materials science &amp; engineering. B, Solid-state materials for advanced technology</jtitle><date>2023-01</date><risdate>2023</risdate><volume>287</volume><spage>116092</spage><pages>116092-</pages><artnum>116092</artnum><issn>0921-5107</issn><eissn>1873-4944</eissn><abstract>•H2 sensor using tapered optical fiber coated with Palladium (Pd) NPs is proposed.•Absorbance decreases when tapered multimode fiber coated with Pd exposed to H2.•The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as NH3 and CH4. Gaseous pollutants such as hydrogen gas (H2) are present in daily human activities and have been studied extensively due to their high explosive and widespread use in many fields. A common H2 gas detector is electrically based. Although these electrical or conductometric sensors attain high sensitivity, they suffer from drawbacks, including poor selectivity, high operating temperature, and susceptibility to electromagnetic interference, which the optical-based sensor can improve. This study describes the development of a palladium-coated (Pd) optical fiber for the room temperature (H2) hydrogen application process. To improve the evanescent light field that propagates through the fiber, a multimode fiber was used to fabricate a transducing channel with cladding and core diameters of 125 μm and 62.5 μm respectively. The multimode optical fibers were tapered from 125 μm cladding diameters to 20 μm diameter, 10 mm waist-length, 5 mm to the up and down tapered region, and coated with Pd by using the drop-casting technique. Various characterization techniques have been used to characterize palladium, such as Field Emission Scanning Electron Microscopy (FESEM), X-ray energy scattering (EDX), X-ray Diffraction (XRD), and atomic force microscopy (AFM). The fabricated Pd-based sensor operates safely at room temperature with a gas concentration of 0.125 % to 2.00 % H2. The measured sensitivity, response, and recovery time were 18,645 %, 50 s, and 230 s, respectively. The selectivity of the fabricated sensor toward H2 was affirmed with no response to other gases such as ammonia (NH3) and methane (CH4). However, this study demonstrates reliable, efficient, and reproducible H2 detection using a simple and cost-effective method.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.mseb.2022.116092</doi></addata></record>
fulltext fulltext
identifier ISSN: 0921-5107
ispartof Materials science & engineering. B, Solid-state materials for advanced technology, 2023-01, Vol.287, p.116092, Article 116092
issn 0921-5107
1873-4944
language eng
recordid cdi_proquest_journals_2778060658
source Elsevier ScienceDirect Journals
subjects Ammonia
Chemical sensors
Cladding
Diameters
Drop-casting
Electromagnetic interference
Explosives detection
Field emission microscopy
Gas detectors
Gases
H2 gas
Hydrogen
Methane
Microscopy
Operating temperature
Optical fibers
Optical measuring instruments
Palladium
Palladium (Pd)
Recovery time
Room temperature
Selectivity
Sensitivity
Tapered optical fiber
title Room temperature operated hydrogen sensor using palladium coated on tapered optical fiber
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-19T05%3A54%3A47IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Room%20temperature%20operated%20hydrogen%20sensor%20using%20palladium%20coated%20on%20tapered%20optical%20fiber&rft.jtitle=Materials%20science%20&%20engineering.%20B,%20Solid-state%20materials%20for%20advanced%20technology&rft.au=M.%20Alkhabet,%20Mohammed&rft.date=2023-01&rft.volume=287&rft.spage=116092&rft.pages=116092-&rft.artnum=116092&rft.issn=0921-5107&rft.eissn=1873-4944&rft_id=info:doi/10.1016/j.mseb.2022.116092&rft_dat=%3Cproquest_cross%3E2778060658%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2778060658&rft_id=info:pmid/&rft_els_id=S0921510722004809&rfr_iscdi=true