Preparation of Nanoporous Carbon from a Spherical NbC/C Nanocomposite and Its Properties
Nanoporous carbon (carbide-derived carbon (CDC)) has been prepared via high-temperature chlorination of a spherical NbC/C nanocomposite synthesized by a new process [ 19 ]. The CDC has been characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy in combination with energ...
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| Veröffentlicht in: | Inorganic materials 2022-11, Vol.58 (11), p.1130-1136 |
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| container_title | Inorganic materials |
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| creator | Il’in, E. G. Parshakov, A. S. Kottsov, S. Yu Razumov, M. I. Gryzlov, D. Yu |
| description | Nanoporous carbon (carbide-derived carbon (CDC)) has been prepared via high-temperature chlorination of a spherical NbC/C nanocomposite synthesized by a new process [
19
]. The CDC has been characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy in combination with energy dispersive X-ray analysis, and transmission electron microscopy. Using nitrogen adsorption–desorption measurements, we have determined the average pore size (3.627 nm), pore size distribution, and total pore volume (1.215 cm
3
/g) in the CDC and calculated its specific surface area by the BET method (817.282 m
2
/g). The electrochemical behavior of the nanoporous carbon (CDC) has been studied using half-cell cyclic voltammetry measurements in the potential sweep range from –1.0 to +1.0 V vs. carbon and impedance spectroscopy. |
| doi_str_mv | 10.1134/S002016852211005X |
| format | Article |
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19
]. The CDC has been characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy in combination with energy dispersive X-ray analysis, and transmission electron microscopy. Using nitrogen adsorption–desorption measurements, we have determined the average pore size (3.627 nm), pore size distribution, and total pore volume (1.215 cm
3
/g) in the CDC and calculated its specific surface area by the BET method (817.282 m
2
/g). The electrochemical behavior of the nanoporous carbon (CDC) has been studied using half-cell cyclic voltammetry measurements in the potential sweep range from –1.0 to +1.0 V vs. carbon and impedance spectroscopy.</description><identifier>ISSN: 0020-1685</identifier><identifier>EISSN: 1608-3172</identifier><identifier>DOI: 10.1134/S002016852211005X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Carbon ; Chemistry ; Chemistry and Materials Science ; Electrochemical analysis ; Electron microscopy ; Energy dispersive X ray analysis ; High temperature ; Industrial Chemistry/Chemical Engineering ; Inorganic Chemistry ; Materials Science ; Nanocomposites ; Niobium carbide ; Pore size distribution ; Raman spectroscopy ; X ray analysis</subject><ispartof>Inorganic materials, 2022-11, Vol.58 (11), p.1130-1136</ispartof><rights>Pleiades Publishing, Ltd. 2022. ISSN 0020-1685, Inorganic Materials, 2022, Vol. 58, No. 11, pp. 1130–1136. © Pleiades Publishing, Ltd., 2022. Russian Text © The Author(s), 2022, published in Neorganicheskie Materialy, 2022, Vol. 58, No. 11, pp. 1170–1176.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c198t-4392244e54799868b0124702ad22d658d9124c6ace2fa04242e3358c58e169053</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S002016852211005X$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S002016852211005X$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Il’in, E. G.</creatorcontrib><creatorcontrib>Parshakov, A. S.</creatorcontrib><creatorcontrib>Kottsov, S. Yu</creatorcontrib><creatorcontrib>Razumov, M. I.</creatorcontrib><creatorcontrib>Gryzlov, D. Yu</creatorcontrib><title>Preparation of Nanoporous Carbon from a Spherical NbC/C Nanocomposite and Its Properties</title><title>Inorganic materials</title><addtitle>Inorg Mater</addtitle><description>Nanoporous carbon (carbide-derived carbon (CDC)) has been prepared via high-temperature chlorination of a spherical NbC/C nanocomposite synthesized by a new process [
19
]. The CDC has been characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy in combination with energy dispersive X-ray analysis, and transmission electron microscopy. Using nitrogen adsorption–desorption measurements, we have determined the average pore size (3.627 nm), pore size distribution, and total pore volume (1.215 cm
3
/g) in the CDC and calculated its specific surface area by the BET method (817.282 m
2
/g). The electrochemical behavior of the nanoporous carbon (CDC) has been studied using half-cell cyclic voltammetry measurements in the potential sweep range from –1.0 to +1.0 V vs. carbon and impedance spectroscopy.</description><subject>Carbon</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Electrochemical analysis</subject><subject>Electron microscopy</subject><subject>Energy dispersive X ray analysis</subject><subject>High temperature</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Inorganic Chemistry</subject><subject>Materials Science</subject><subject>Nanocomposites</subject><subject>Niobium carbide</subject><subject>Pore size distribution</subject><subject>Raman spectroscopy</subject><subject>X ray analysis</subject><issn>0020-1685</issn><issn>1608-3172</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp1kE9Lw0AQxRdRsFY_gLcFz7Gzk91k9yjBP4VSC1XoLWyTjaa02XU2PfjtTa3gQZzLMPN-7w0MY9cCboVI5WQJgCAyrRCFAFCrEzYSGegkFTmestFBTg76ObuIcQMAUmkzYqsFuWDJ9q3vuG_43HY-ePL7yAtL62HZkN9xy5fh3VFb2S2fr4tJ8Q1Wfhd8bHvHbVfzaR_5gnxw1LcuXrKzxm6ju_rpY_b6cP9SPCWz58dpcTdLKmF0n8jUIErplMyN0Zleg0CZA9oasc6Urs0wV5mtHDYWJEp0aap0pbQTmQGVjtnNMTeQ_9i72Jcbv6duOFliPpTKU6MHShypinyM5JoyULuz9FkKKA8PLP88cPDg0RMHtntz9Jv8v-kLF6Rv9w</recordid><startdate>20221101</startdate><enddate>20221101</enddate><creator>Il’in, E. G.</creator><creator>Parshakov, A. S.</creator><creator>Kottsov, S. Yu</creator><creator>Razumov, M. I.</creator><creator>Gryzlov, D. Yu</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20221101</creationdate><title>Preparation of Nanoporous Carbon from a Spherical NbC/C Nanocomposite and Its Properties</title><author>Il’in, E. G. ; Parshakov, A. S. ; Kottsov, S. Yu ; Razumov, M. I. ; Gryzlov, D. Yu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c198t-4392244e54799868b0124702ad22d658d9124c6ace2fa04242e3358c58e169053</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Carbon</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Electrochemical analysis</topic><topic>Electron microscopy</topic><topic>Energy dispersive X ray analysis</topic><topic>High temperature</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Inorganic Chemistry</topic><topic>Materials Science</topic><topic>Nanocomposites</topic><topic>Niobium carbide</topic><topic>Pore size distribution</topic><topic>Raman spectroscopy</topic><topic>X ray analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Il’in, E. G.</creatorcontrib><creatorcontrib>Parshakov, A. S.</creatorcontrib><creatorcontrib>Kottsov, S. Yu</creatorcontrib><creatorcontrib>Razumov, M. I.</creatorcontrib><creatorcontrib>Gryzlov, D. Yu</creatorcontrib><collection>CrossRef</collection><jtitle>Inorganic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Il’in, E. G.</au><au>Parshakov, A. S.</au><au>Kottsov, S. Yu</au><au>Razumov, M. I.</au><au>Gryzlov, D. Yu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation of Nanoporous Carbon from a Spherical NbC/C Nanocomposite and Its Properties</atitle><jtitle>Inorganic materials</jtitle><stitle>Inorg Mater</stitle><date>2022-11-01</date><risdate>2022</risdate><volume>58</volume><issue>11</issue><spage>1130</spage><epage>1136</epage><pages>1130-1136</pages><issn>0020-1685</issn><eissn>1608-3172</eissn><abstract>Nanoporous carbon (carbide-derived carbon (CDC)) has been prepared via high-temperature chlorination of a spherical NbC/C nanocomposite synthesized by a new process [
19
]. The CDC has been characterized by X-ray diffraction, Raman spectroscopy, scanning electron microscopy in combination with energy dispersive X-ray analysis, and transmission electron microscopy. Using nitrogen adsorption–desorption measurements, we have determined the average pore size (3.627 nm), pore size distribution, and total pore volume (1.215 cm
3
/g) in the CDC and calculated its specific surface area by the BET method (817.282 m
2
/g). The electrochemical behavior of the nanoporous carbon (CDC) has been studied using half-cell cyclic voltammetry measurements in the potential sweep range from –1.0 to +1.0 V vs. carbon and impedance spectroscopy.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S002016852211005X</doi><tpages>7</tpages></addata></record> |
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| subjects | Carbon Chemistry Chemistry and Materials Science Electrochemical analysis Electron microscopy Energy dispersive X ray analysis High temperature Industrial Chemistry/Chemical Engineering Inorganic Chemistry Materials Science Nanocomposites Niobium carbide Pore size distribution Raman spectroscopy X ray analysis |
| title | Preparation of Nanoporous Carbon from a Spherical NbC/C Nanocomposite and Its Properties |
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