Sol-Gel Synthesis of MgO–Al2O3–ZrO2–SiO2 Coatings on Quartz Ceramics
In the work, the MgO–Al 2 O 3 –ZrO 2 –SiO 2 coatings on the surface of quartz ceramics were prepared by sol-gel method. The synthesized materials were examined by X-ray phase and electron microscopic analyses. It is shown that composite gels retain an amorphous structure after thermal treatment at 6...
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| Veröffentlicht in: | Glass physics and chemistry 2022-12, Vol.48 (6), p.669-672 |
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| container_title | Glass physics and chemistry |
| container_volume | 48 |
| creator | Saratovskii, A. S. Evstropiev, S. K. Dukel’skii, K. V. Volynkin, V. M. |
| description | In the work, the MgO–Al
2
O
3
–ZrO
2
–SiO
2
coatings on the surface of quartz ceramics were prepared by sol-gel method. The synthesized materials were examined by X-ray phase and electron microscopic analyses. It is shown that composite gels retain an amorphous structure after thermal treatment at 600°C, and the formation and subsequent transformation of various oxide crystal phases is observed after calcination at temperatures above 900°C. The behavior of the thermal evolution of the structure of the obtained gels is generally similar to the course of structural changes occurring during glasses crystallization. |
| doi_str_mv | 10.1134/S1087659622600831 |
| format | Article |
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2
O
3
–ZrO
2
–SiO
2
coatings on the surface of quartz ceramics were prepared by sol-gel method. The synthesized materials were examined by X-ray phase and electron microscopic analyses. It is shown that composite gels retain an amorphous structure after thermal treatment at 600°C, and the formation and subsequent transformation of various oxide crystal phases is observed after calcination at temperatures above 900°C. The behavior of the thermal evolution of the structure of the obtained gels is generally similar to the course of structural changes occurring during glasses crystallization.</description><identifier>ISSN: 1087-6596</identifier><identifier>EISSN: 1608-313X</identifier><identifier>DOI: 10.1134/S1087659622600831</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Aluminum oxide ; Brief Message ; Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Coatings ; Composites ; Crystallization ; Gels ; Glass ; Heat treatment ; Magnesium oxide ; Materials Science ; Natural Materials ; Physical Chemistry ; Quartz ; Silicon dioxide ; Sol-gel processes ; Thermal evolution ; Zirconium dioxide</subject><ispartof>Glass physics and chemistry, 2022-12, Vol.48 (6), p.669-672</ispartof><rights>Pleiades Publishing, Ltd. 2022. ISSN 1087-6596, Glass Physics and Chemistry, 2022, Vol. 48, No. 6, pp. 669–672. © Pleiades Publishing, Ltd., 2022.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c198t-42030c3946fb16135b2901dd31227c19e088e8a75aa3a5294e1eec86c208e7e43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1087659622600831$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1087659622600831$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Saratovskii, A. S.</creatorcontrib><creatorcontrib>Evstropiev, S. K.</creatorcontrib><creatorcontrib>Dukel’skii, K. V.</creatorcontrib><creatorcontrib>Volynkin, V. M.</creatorcontrib><title>Sol-Gel Synthesis of MgO–Al2O3–ZrO2–SiO2 Coatings on Quartz Ceramics</title><title>Glass physics and chemistry</title><addtitle>Glass Phys Chem</addtitle><description>In the work, the MgO–Al
2
O
3
–ZrO
2
–SiO
2
coatings on the surface of quartz ceramics were prepared by sol-gel method. The synthesized materials were examined by X-ray phase and electron microscopic analyses. It is shown that composite gels retain an amorphous structure after thermal treatment at 600°C, and the formation and subsequent transformation of various oxide crystal phases is observed after calcination at temperatures above 900°C. The behavior of the thermal evolution of the structure of the obtained gels is generally similar to the course of structural changes occurring during glasses crystallization.</description><subject>Aluminum oxide</subject><subject>Brief Message</subject><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Coatings</subject><subject>Composites</subject><subject>Crystallization</subject><subject>Gels</subject><subject>Glass</subject><subject>Heat treatment</subject><subject>Magnesium oxide</subject><subject>Materials Science</subject><subject>Natural Materials</subject><subject>Physical Chemistry</subject><subject>Quartz</subject><subject>Silicon dioxide</subject><subject>Sol-gel processes</subject><subject>Thermal evolution</subject><subject>Zirconium dioxide</subject><issn>1087-6596</issn><issn>1608-313X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp1kMFKw0AQhhdRsFYfwFvAc3RmNtndHEvQVqkEiYJ4Cdt0U1PSpO6mh3ryHXxDn8QtFTyIp39gvv8f5mfsHOESkUdXOYKSIk4EkQBQHA_YAAWokCN_PvSzX4e7_TE7cW4JAImU0YDd5V0Tjk0T5Nu2fzWudkFXBfeL7Ovjc9RQxr2-2Iy85HVGQdrpvm4XnmqDh422_XuQGqtXdelO2VGlG2fOfnTInm6uH9NJOM3Gt-loGpaYqD6MCDiUPIlENUOBPJ5RAjifcySSHjGglFFaxlpzHVMSGTSmVKIkUEaaiA_ZxT53bbu3jXF9sew2tvUnC_I_EQcJ4CncU6XtnLOmKta2Xmm7LRCKXWXFn8q8h_Ye59l2Yexv8v-mbwenbQI</recordid><startdate>20221201</startdate><enddate>20221201</enddate><creator>Saratovskii, A. S.</creator><creator>Evstropiev, S. K.</creator><creator>Dukel’skii, K. V.</creator><creator>Volynkin, V. M.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20221201</creationdate><title>Sol-Gel Synthesis of MgO–Al2O3–ZrO2–SiO2 Coatings on Quartz Ceramics</title><author>Saratovskii, A. S. ; Evstropiev, S. K. ; Dukel’skii, K. V. ; Volynkin, V. M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c198t-42030c3946fb16135b2901dd31227c19e088e8a75aa3a5294e1eec86c208e7e43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Aluminum oxide</topic><topic>Brief Message</topic><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Coatings</topic><topic>Composites</topic><topic>Crystallization</topic><topic>Gels</topic><topic>Glass</topic><topic>Heat treatment</topic><topic>Magnesium oxide</topic><topic>Materials Science</topic><topic>Natural Materials</topic><topic>Physical Chemistry</topic><topic>Quartz</topic><topic>Silicon dioxide</topic><topic>Sol-gel processes</topic><topic>Thermal evolution</topic><topic>Zirconium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Saratovskii, A. S.</creatorcontrib><creatorcontrib>Evstropiev, S. K.</creatorcontrib><creatorcontrib>Dukel’skii, K. V.</creatorcontrib><creatorcontrib>Volynkin, V. M.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Glass physics and chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Saratovskii, A. S.</au><au>Evstropiev, S. K.</au><au>Dukel’skii, K. V.</au><au>Volynkin, V. M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Sol-Gel Synthesis of MgO–Al2O3–ZrO2–SiO2 Coatings on Quartz Ceramics</atitle><jtitle>Glass physics and chemistry</jtitle><stitle>Glass Phys Chem</stitle><date>2022-12-01</date><risdate>2022</risdate><volume>48</volume><issue>6</issue><spage>669</spage><epage>672</epage><pages>669-672</pages><issn>1087-6596</issn><eissn>1608-313X</eissn><abstract>In the work, the MgO–Al
2
O
3
–ZrO
2
–SiO
2
coatings on the surface of quartz ceramics were prepared by sol-gel method. The synthesized materials were examined by X-ray phase and electron microscopic analyses. It is shown that composite gels retain an amorphous structure after thermal treatment at 600°C, and the formation and subsequent transformation of various oxide crystal phases is observed after calcination at temperatures above 900°C. The behavior of the thermal evolution of the structure of the obtained gels is generally similar to the course of structural changes occurring during glasses crystallization.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1087659622600831</doi><tpages>4</tpages></addata></record> |
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| ispartof | Glass physics and chemistry, 2022-12, Vol.48 (6), p.669-672 |
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| subjects | Aluminum oxide Brief Message Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Coatings Composites Crystallization Gels Glass Heat treatment Magnesium oxide Materials Science Natural Materials Physical Chemistry Quartz Silicon dioxide Sol-gel processes Thermal evolution Zirconium dioxide |
| title | Sol-Gel Synthesis of MgO–Al2O3–ZrO2–SiO2 Coatings on Quartz Ceramics |
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