Design, fabrication, mechanical, and in vitro evaluation of 3D printed ZrO2 reinforced polylactide scaffolds through fused deposition modeling
The design and fabrication of 3D-printed polylactide/ZrO2 composites through fused deposition modelling (FDM) based approach is illustrated in the present study. ZrO2 synthesized through the sol–gel technique and the commercially procured polylactide (PLA) were used as the source for the extrusion o...
Gespeichert in:
| Veröffentlicht in: | Materials chemistry frontiers 2023-01, Vol.7 (3), p.464-475 |
|---|---|
| Hauptverfasser: | , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 475 |
|---|---|
| container_issue | 3 |
| container_start_page | 464 |
| container_title | Materials chemistry frontiers |
| container_volume | 7 |
| creator | M Mushtaq Alam Ezhilan, M Saha, Sunjeet Gopan, Gopika Maheswaran Mani Kannan, S |
| description | The design and fabrication of 3D-printed polylactide/ZrO2 composites through fused deposition modelling (FDM) based approach is illustrated in the present study. ZrO2 synthesized through the sol–gel technique and the commercially procured polylactide (PLA) were used as the source for the extrusion of composite filaments, followed by their 3D printing through FDM methodology. The results from the investigation ensured a maximum of 20 wt% ZrO2 loading in PLA matrix for a facile and smooth extrusion of filaments and their subsequent defect-free 3D printing of desired shape and geometry. The structural analysis of the 3D printed specimens revealed the phase stability of PLA and ZrO2 in composites and the morphological studies ensured the uniform dispersion of ZrO2 particles throughout the PLA matrix. Moreover, the pattern of infill thickness in the 3D-printed specimen is determined as 400 μm, which implied better consistency with the 0.4 mm dimension sized printer nozzle utilized for printing. A gradual reduction in the mechanical strength of PLA/ZrO2 composite as a function of enhanced ZrO2 content is deliberated. The results from in vitro tests revealed the negligible cytotoxicity displayed by the 3D-printed PLA/ZrO2 composite specimens. |
| doi_str_mv | 10.1039/d2qm01014c |
| format | Article |
| fullrecord | <record><control><sourceid>proquest</sourceid><recordid>TN_cdi_proquest_journals_2770621744</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2770621744</sourcerecordid><originalsourceid>FETCH-LOGICAL-p183t-2ead185ea3632e15d3d4d31b4245099e6a91782b523c5d1559580fe1f25546333</originalsourceid><addsrcrecordid>eNotjc1KAzEURoMgWGo3PkHAbUdzk8lkZimtf1DoRjduSprctCnTZJrMFHwJn9mhuvo4cDgfIXfAHoCJ5tHy05EBg9JckQlnkhcghbohs5wPjDFQigsGE_KzxOx3YU6d3iZvdO_jCEc0ex1GbOdUB0t9oGffp0jxrNvhItHoqFjSLvnQo6Vfac1pQh9cTGbkLrbfrTa9t0iz0c7F1mba71Mcdnvqhjw6FruY_SV2jBZbH3a35NrpNuPsf6fk8-X5Y_FWrNav74unVdFBLfqCo7ZQS9SiEhxBWmFLK2Bb8lKypsFKN6BqvpVcGGlBykbWzCE4LmVZCSGm5P6v26V4GjD3m0McUhgvN1wpVnFQZSl-AUS4ZRQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2770621744</pqid></control><display><type>article</type><title>Design, fabrication, mechanical, and in vitro evaluation of 3D printed ZrO2 reinforced polylactide scaffolds through fused deposition modeling</title><source>Royal Society Of Chemistry Journals 2008-</source><creator>M Mushtaq Alam ; Ezhilan, M ; Saha, Sunjeet ; Gopan, Gopika ; Maheswaran Mani ; Kannan, S</creator><creatorcontrib>M Mushtaq Alam ; Ezhilan, M ; Saha, Sunjeet ; Gopan, Gopika ; Maheswaran Mani ; Kannan, S</creatorcontrib><description>The design and fabrication of 3D-printed polylactide/ZrO2 composites through fused deposition modelling (FDM) based approach is illustrated in the present study. ZrO2 synthesized through the sol–gel technique and the commercially procured polylactide (PLA) were used as the source for the extrusion of composite filaments, followed by their 3D printing through FDM methodology. The results from the investigation ensured a maximum of 20 wt% ZrO2 loading in PLA matrix for a facile and smooth extrusion of filaments and their subsequent defect-free 3D printing of desired shape and geometry. The structural analysis of the 3D printed specimens revealed the phase stability of PLA and ZrO2 in composites and the morphological studies ensured the uniform dispersion of ZrO2 particles throughout the PLA matrix. Moreover, the pattern of infill thickness in the 3D-printed specimen is determined as 400 μm, which implied better consistency with the 0.4 mm dimension sized printer nozzle utilized for printing. A gradual reduction in the mechanical strength of PLA/ZrO2 composite as a function of enhanced ZrO2 content is deliberated. The results from in vitro tests revealed the negligible cytotoxicity displayed by the 3D-printed PLA/ZrO2 composite specimens.</description><identifier>EISSN: 2052-1537</identifier><identifier>DOI: 10.1039/d2qm01014c</identifier><language>eng</language><publisher>London: Royal Society of Chemistry</publisher><subject>3-D printers ; Deposition ; Extrusion ; Filaments ; Fused deposition modeling ; In vitro methods and tests ; Phase stability ; Polylactic acid ; Rapid prototyping ; Sol-gel processes ; Stability analysis ; Structural analysis ; Three dimensional composites ; Three dimensional printing ; Toxicity ; Zirconium dioxide</subject><ispartof>Materials chemistry frontiers, 2023-01, Vol.7 (3), p.464-475</ispartof><rights>Copyright Royal Society of Chemistry 2023</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>M Mushtaq Alam</creatorcontrib><creatorcontrib>Ezhilan, M</creatorcontrib><creatorcontrib>Saha, Sunjeet</creatorcontrib><creatorcontrib>Gopan, Gopika</creatorcontrib><creatorcontrib>Maheswaran Mani</creatorcontrib><creatorcontrib>Kannan, S</creatorcontrib><title>Design, fabrication, mechanical, and in vitro evaluation of 3D printed ZrO2 reinforced polylactide scaffolds through fused deposition modeling</title><title>Materials chemistry frontiers</title><description>The design and fabrication of 3D-printed polylactide/ZrO2 composites through fused deposition modelling (FDM) based approach is illustrated in the present study. ZrO2 synthesized through the sol–gel technique and the commercially procured polylactide (PLA) were used as the source for the extrusion of composite filaments, followed by their 3D printing through FDM methodology. The results from the investigation ensured a maximum of 20 wt% ZrO2 loading in PLA matrix for a facile and smooth extrusion of filaments and their subsequent defect-free 3D printing of desired shape and geometry. The structural analysis of the 3D printed specimens revealed the phase stability of PLA and ZrO2 in composites and the morphological studies ensured the uniform dispersion of ZrO2 particles throughout the PLA matrix. Moreover, the pattern of infill thickness in the 3D-printed specimen is determined as 400 μm, which implied better consistency with the 0.4 mm dimension sized printer nozzle utilized for printing. A gradual reduction in the mechanical strength of PLA/ZrO2 composite as a function of enhanced ZrO2 content is deliberated. The results from in vitro tests revealed the negligible cytotoxicity displayed by the 3D-printed PLA/ZrO2 composite specimens.</description><subject>3-D printers</subject><subject>Deposition</subject><subject>Extrusion</subject><subject>Filaments</subject><subject>Fused deposition modeling</subject><subject>In vitro methods and tests</subject><subject>Phase stability</subject><subject>Polylactic acid</subject><subject>Rapid prototyping</subject><subject>Sol-gel processes</subject><subject>Stability analysis</subject><subject>Structural analysis</subject><subject>Three dimensional composites</subject><subject>Three dimensional printing</subject><subject>Toxicity</subject><subject>Zirconium dioxide</subject><issn>2052-1537</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNotjc1KAzEURoMgWGo3PkHAbUdzk8lkZimtf1DoRjduSprctCnTZJrMFHwJn9mhuvo4cDgfIXfAHoCJ5tHy05EBg9JckQlnkhcghbohs5wPjDFQigsGE_KzxOx3YU6d3iZvdO_jCEc0ex1GbOdUB0t9oGffp0jxrNvhItHoqFjSLvnQo6Vfac1pQh9cTGbkLrbfrTa9t0iz0c7F1mba71Mcdnvqhjw6FruY_SV2jBZbH3a35NrpNuPsf6fk8-X5Y_FWrNav74unVdFBLfqCo7ZQS9SiEhxBWmFLK2Bb8lKypsFKN6BqvpVcGGlBykbWzCE4LmVZCSGm5P6v26V4GjD3m0McUhgvN1wpVnFQZSl-AUS4ZRQ</recordid><startdate>20230130</startdate><enddate>20230130</enddate><creator>M Mushtaq Alam</creator><creator>Ezhilan, M</creator><creator>Saha, Sunjeet</creator><creator>Gopan, Gopika</creator><creator>Maheswaran Mani</creator><creator>Kannan, S</creator><general>Royal Society of Chemistry</general><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20230130</creationdate><title>Design, fabrication, mechanical, and in vitro evaluation of 3D printed ZrO2 reinforced polylactide scaffolds through fused deposition modeling</title><author>M Mushtaq Alam ; Ezhilan, M ; Saha, Sunjeet ; Gopan, Gopika ; Maheswaran Mani ; Kannan, S</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p183t-2ead185ea3632e15d3d4d31b4245099e6a91782b523c5d1559580fe1f25546333</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>3-D printers</topic><topic>Deposition</topic><topic>Extrusion</topic><topic>Filaments</topic><topic>Fused deposition modeling</topic><topic>In vitro methods and tests</topic><topic>Phase stability</topic><topic>Polylactic acid</topic><topic>Rapid prototyping</topic><topic>Sol-gel processes</topic><topic>Stability analysis</topic><topic>Structural analysis</topic><topic>Three dimensional composites</topic><topic>Three dimensional printing</topic><topic>Toxicity</topic><topic>Zirconium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>M Mushtaq Alam</creatorcontrib><creatorcontrib>Ezhilan, M</creatorcontrib><creatorcontrib>Saha, Sunjeet</creatorcontrib><creatorcontrib>Gopan, Gopika</creatorcontrib><creatorcontrib>Maheswaran Mani</creatorcontrib><creatorcontrib>Kannan, S</creatorcontrib><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials chemistry frontiers</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>M Mushtaq Alam</au><au>Ezhilan, M</au><au>Saha, Sunjeet</au><au>Gopan, Gopika</au><au>Maheswaran Mani</au><au>Kannan, S</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Design, fabrication, mechanical, and in vitro evaluation of 3D printed ZrO2 reinforced polylactide scaffolds through fused deposition modeling</atitle><jtitle>Materials chemistry frontiers</jtitle><date>2023-01-30</date><risdate>2023</risdate><volume>7</volume><issue>3</issue><spage>464</spage><epage>475</epage><pages>464-475</pages><eissn>2052-1537</eissn><abstract>The design and fabrication of 3D-printed polylactide/ZrO2 composites through fused deposition modelling (FDM) based approach is illustrated in the present study. ZrO2 synthesized through the sol–gel technique and the commercially procured polylactide (PLA) were used as the source for the extrusion of composite filaments, followed by their 3D printing through FDM methodology. The results from the investigation ensured a maximum of 20 wt% ZrO2 loading in PLA matrix for a facile and smooth extrusion of filaments and their subsequent defect-free 3D printing of desired shape and geometry. The structural analysis of the 3D printed specimens revealed the phase stability of PLA and ZrO2 in composites and the morphological studies ensured the uniform dispersion of ZrO2 particles throughout the PLA matrix. Moreover, the pattern of infill thickness in the 3D-printed specimen is determined as 400 μm, which implied better consistency with the 0.4 mm dimension sized printer nozzle utilized for printing. A gradual reduction in the mechanical strength of PLA/ZrO2 composite as a function of enhanced ZrO2 content is deliberated. The results from in vitro tests revealed the negligible cytotoxicity displayed by the 3D-printed PLA/ZrO2 composite specimens.</abstract><cop>London</cop><pub>Royal Society of Chemistry</pub><doi>10.1039/d2qm01014c</doi><tpages>12</tpages></addata></record> |
| fulltext | fulltext |
| identifier | EISSN: 2052-1537 |
| ispartof | Materials chemistry frontiers, 2023-01, Vol.7 (3), p.464-475 |
| issn | 2052-1537 |
| language | eng |
| recordid | cdi_proquest_journals_2770621744 |
| source | Royal Society Of Chemistry Journals 2008- |
| subjects | 3-D printers Deposition Extrusion Filaments Fused deposition modeling In vitro methods and tests Phase stability Polylactic acid Rapid prototyping Sol-gel processes Stability analysis Structural analysis Three dimensional composites Three dimensional printing Toxicity Zirconium dioxide |
| title | Design, fabrication, mechanical, and in vitro evaluation of 3D printed ZrO2 reinforced polylactide scaffolds through fused deposition modeling |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-11T16%3A34%3A49IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Design,%20fabrication,%20mechanical,%20and%20in%20vitro%20evaluation%20of%203D%20printed%20ZrO2%20reinforced%20polylactide%20scaffolds%20through%20fused%20deposition%20modeling&rft.jtitle=Materials%20chemistry%20frontiers&rft.au=M%20Mushtaq%20Alam&rft.date=2023-01-30&rft.volume=7&rft.issue=3&rft.spage=464&rft.epage=475&rft.pages=464-475&rft.eissn=2052-1537&rft_id=info:doi/10.1039/d2qm01014c&rft_dat=%3Cproquest%3E2770621744%3C/proquest%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2770621744&rft_id=info:pmid/&rfr_iscdi=true |