Evaluation of the CP-Sil 88 and SP-2560 GC Columns Used in the Recently Approved AOCS Official Method Ce 1h-05: Determination of cis-, trans-, Saturated, Monounsaturated, and Polyunsaturated Fatty Acids in Vegetable or Non-ruminant Animal Oils and Fats by Capillary GLC Method
The AOCS Official Method Ce 1h‐05 was recently approved at the 96th AOCS Annual Meeting (2005) by the Uniform Methods Committee as the official method for determining cis and trans FA in vegetable or non‐ruminant fats and oils. A series of experiments was undertaken using a margarine (hydrogenated s...
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| Veröffentlicht in: | Journal of the American Oil Chemists' Society 2006-06, Vol.83 (6), p.475-488 |
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| creator | Ratnayake, W.M.N Hansen, S.L Kennedy, M.P |
| description | The AOCS Official Method Ce 1h‐05 was recently approved at the 96th AOCS Annual Meeting (2005) by the Uniform Methods Committee as the official method for determining cis and trans FA in vegetable or non‐ruminant fats and oils. A series of experiments was undertaken using a margarine (hydrogenated soybean oil) sample containing approximately 34% total trans FA (28% 18∶1 trans, 6% 18∶2 trans, and 0.2% 18∶3 trans), a low‐trans oil (ca. 7% total trans FA), and a proposed system suitability mixture (12∶0, 9c−18∶1, 11c−18;1, 9c,12c,15c−18∶3, 11c−20∶1, and 21∶0) in an effort to evaluate and optimize the separation on the 100‐m SP‐2560 and CP‐Sil 88 flexible fused‐silica capillary GC columns recommended for the analysis. Different carrier gases and flow rates were used during the evaluation, which eventually lead to the final conditions to be used for AOCS Official Method Ce 1h‐05. |
| doi_str_mv | 10.1007/s11746-006-1230-y |
| format | Article |
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A series of experiments was undertaken using a margarine (hydrogenated soybean oil) sample containing approximately 34% total trans FA (28% 18∶1 trans, 6% 18∶2 trans, and 0.2% 18∶3 trans), a low‐trans oil (ca. 7% total trans FA), and a proposed system suitability mixture (12∶0, 9c−18∶1, 11c−18;1, 9c,12c,15c−18∶3, 11c−20∶1, and 21∶0) in an effort to evaluate and optimize the separation on the 100‐m SP‐2560 and CP‐Sil 88 flexible fused‐silica capillary GC columns recommended for the analysis. Different carrier gases and flow rates were used during the evaluation, which eventually lead to the final conditions to be used for AOCS Official Method Ce 1h‐05.</description><identifier>ISSN: 0003-021X</identifier><identifier>EISSN: 1558-9331</identifier><identifier>DOI: 10.1007/s11746-006-1230-y</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer‐Verlag</publisher><subject>animal fats and oils ; Biological and medical sciences ; chemical analysis ; Chromatography ; CP‐Sil 88 ; Fat industries ; Fatty acids ; Flow rates ; Food ; Food industries ; Fundamental and applied biological sciences. Psychology ; gas chromatography ; margarine ; monounsaturated fatty acids ; Oils & fats ; partially hydrogenated fats ; Polyunsaturated fatty acids ; saturated fatty acids ; Silica ; Soybean oil ; Soybeans ; SP‐2560 ; Trans fats ; trans fatty acid analysis ; vegetable oil ; Vegetables</subject><ispartof>Journal of the American Oil Chemists' Society, 2006-06, Vol.83 (6), p.475-488</ispartof><rights>2006 American Oil Chemists' Society (AOCS)</rights><rights>2006 INIST-CNRS</rights><rights>Copyright AOCS Press Jun 2006</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4135-32066ba351d88d8fe48bf370e503a7eaf0d81131eba377f286a60dc158a568d73</citedby><cites>FETCH-LOGICAL-c4135-32066ba351d88d8fe48bf370e503a7eaf0d81131eba377f286a60dc158a568d73</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1007%2Fs11746-006-1230-y$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1007%2Fs11746-006-1230-y$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27903,27904,45553,45554</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=17894496$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Ratnayake, W.M.N</creatorcontrib><creatorcontrib>Hansen, S.L</creatorcontrib><creatorcontrib>Kennedy, M.P</creatorcontrib><title>Evaluation of the CP-Sil 88 and SP-2560 GC Columns Used in the Recently Approved AOCS Official Method Ce 1h-05: Determination of cis-, trans-, Saturated, Monounsaturated, and Polyunsaturated Fatty Acids in Vegetable or Non-ruminant Animal Oils and Fats by Capillary GLC Method</title><title>Journal of the American Oil Chemists' Society</title><description>The AOCS Official Method Ce 1h‐05 was recently approved at the 96th AOCS Annual Meeting (2005) by the Uniform Methods Committee as the official method for determining cis and trans FA in vegetable or non‐ruminant fats and oils. A series of experiments was undertaken using a margarine (hydrogenated soybean oil) sample containing approximately 34% total trans FA (28% 18∶1 trans, 6% 18∶2 trans, and 0.2% 18∶3 trans), a low‐trans oil (ca. 7% total trans FA), and a proposed system suitability mixture (12∶0, 9c−18∶1, 11c−18;1, 9c,12c,15c−18∶3, 11c−20∶1, and 21∶0) in an effort to evaluate and optimize the separation on the 100‐m SP‐2560 and CP‐Sil 88 flexible fused‐silica capillary GC columns recommended for the analysis. Different carrier gases and flow rates were used during the evaluation, which eventually lead to the final conditions to be used for AOCS Official Method Ce 1h‐05.</description><subject>animal fats and oils</subject><subject>Biological and medical sciences</subject><subject>chemical analysis</subject><subject>Chromatography</subject><subject>CP‐Sil 88</subject><subject>Fat industries</subject><subject>Fatty acids</subject><subject>Flow rates</subject><subject>Food</subject><subject>Food industries</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>gas chromatography</subject><subject>margarine</subject><subject>monounsaturated fatty acids</subject><subject>Oils & fats</subject><subject>partially hydrogenated fats</subject><subject>Polyunsaturated fatty acids</subject><subject>saturated fatty acids</subject><subject>Silica</subject><subject>Soybean oil</subject><subject>Soybeans</subject><subject>SP‐2560</subject><subject>Trans fats</subject><subject>trans fatty acid analysis</subject><subject>vegetable oil</subject><subject>Vegetables</subject><issn>0003-021X</issn><issn>1558-9331</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>BENPR</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNqFUc9v0zAUDggkxuDGhRNPSNxmeI7jxOVWha0gbbSiFHGL3MTZPLl2sZ2h_Pc4a8W4cXqy_f3y-7LsNcX3FLH6ECitipIgloTmDMn4ODuhnAsyY4w-yU4QkRHM6c9n2fMQbtNRsJyfPHp1fifNIKN2FlwP8UZBvSJrbUAIkLaD9YrkvERY1FA7M-xsgE1QHWh7D_6mWmWjGWG-33t3lx7my3oNy77XrZYGrlS8cR3UCugNQf4RPqmo_E7bv5atDuQMopd2mmsZBy-j6s7gylk32PBwMcVZOTP-cwkXMsZk3uouTJF-qGsV5dYocB6-Okv8MHnZCHOrdynPUptwL5SIAbYj1HKvjZF-hMVlfYz7InvaSxPUy-M8zTYX59_rz-RyufhSzy9JW1DGCcuxLLeScdoJ0YleFWLbswoVRyYrJXvsBKWMqoSpqj4XpSyxaykXkpeiq9hp9vagm1b3a1AhNrdu8DZZNnnFsWBFNYHoAdR6F4JXfbP36St-bCg2U_fNofsmdd9M3Tdj4rw7CsvQStOn5aY1PxArMSuKWZlw1QH3Wxs1_l-4mcrFouKJ-ebA7KVr5LVP6pt1jpQhxRnyYsb-ADmKx8U</recordid><startdate>200606</startdate><enddate>200606</enddate><creator>Ratnayake, W.M.N</creator><creator>Hansen, S.L</creator><creator>Kennedy, M.P</creator><general>Springer‐Verlag</general><general>Springer</general><general>Springer Nature B.V</general><scope>FBQ</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>4T-</scope><scope>7X2</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>88I</scope><scope>8AO</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>KB.</scope><scope>M0K</scope><scope>M0S</scope><scope>M1P</scope><scope>M2O</scope><scope>M2P</scope><scope>MBDVC</scope><scope>PCBAR</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>Q9U</scope></search><sort><creationdate>200606</creationdate><title>Evaluation of the CP-Sil 88 and SP-2560 GC Columns Used in the Recently Approved AOCS Official Method Ce 1h-05: Determination of cis-, trans-, Saturated, Monounsaturated, and Polyunsaturated Fatty Acids in Vegetable or Non-ruminant Animal Oils and Fats by Capillary GLC Method</title><author>Ratnayake, W.M.N ; Hansen, S.L ; Kennedy, M.P</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4135-32066ba351d88d8fe48bf370e503a7eaf0d81131eba377f286a60dc158a568d73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>animal fats and oils</topic><topic>Biological and medical sciences</topic><topic>chemical analysis</topic><topic>Chromatography</topic><topic>CP‐Sil 88</topic><topic>Fat industries</topic><topic>Fatty acids</topic><topic>Flow rates</topic><topic>Food</topic><topic>Food industries</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>gas chromatography</topic><topic>margarine</topic><topic>monounsaturated fatty acids</topic><topic>Oils & fats</topic><topic>partially hydrogenated fats</topic><topic>Polyunsaturated fatty acids</topic><topic>saturated fatty acids</topic><topic>Silica</topic><topic>Soybean oil</topic><topic>Soybeans</topic><topic>SP‐2560</topic><topic>Trans fats</topic><topic>trans fatty acid analysis</topic><topic>vegetable oil</topic><topic>Vegetables</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ratnayake, W.M.N</creatorcontrib><creatorcontrib>Hansen, S.L</creatorcontrib><creatorcontrib>Kennedy, M.P</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Docstoc</collection><collection>Agricultural Science Collection</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest Pharma Collection</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Research Library (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>Research Library Prep</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>Materials Science Database</collection><collection>Agricultural Science Database</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Research Library</collection><collection>Science Database</collection><collection>Research Library (Corporate)</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central Basic</collection><jtitle>Journal of the American Oil Chemists' Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ratnayake, W.M.N</au><au>Hansen, S.L</au><au>Kennedy, M.P</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Evaluation of the CP-Sil 88 and SP-2560 GC Columns Used in the Recently Approved AOCS Official Method Ce 1h-05: Determination of cis-, trans-, Saturated, Monounsaturated, and Polyunsaturated Fatty Acids in Vegetable or Non-ruminant Animal Oils and Fats by Capillary GLC Method</atitle><jtitle>Journal of the American Oil Chemists' Society</jtitle><date>2006-06</date><risdate>2006</risdate><volume>83</volume><issue>6</issue><spage>475</spage><epage>488</epage><pages>475-488</pages><issn>0003-021X</issn><eissn>1558-9331</eissn><abstract>The AOCS Official Method Ce 1h‐05 was recently approved at the 96th AOCS Annual Meeting (2005) by the Uniform Methods Committee as the official method for determining cis and trans FA in vegetable or non‐ruminant fats and oils. A series of experiments was undertaken using a margarine (hydrogenated soybean oil) sample containing approximately 34% total trans FA (28% 18∶1 trans, 6% 18∶2 trans, and 0.2% 18∶3 trans), a low‐trans oil (ca. 7% total trans FA), and a proposed system suitability mixture (12∶0, 9c−18∶1, 11c−18;1, 9c,12c,15c−18∶3, 11c−20∶1, and 21∶0) in an effort to evaluate and optimize the separation on the 100‐m SP‐2560 and CP‐Sil 88 flexible fused‐silica capillary GC columns recommended for the analysis. Different carrier gases and flow rates were used during the evaluation, which eventually lead to the final conditions to be used for AOCS Official Method Ce 1h‐05.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer‐Verlag</pub><doi>10.1007/s11746-006-1230-y</doi><tpages>14</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | animal fats and oils Biological and medical sciences chemical analysis Chromatography CP‐Sil 88 Fat industries Fatty acids Flow rates Food Food industries Fundamental and applied biological sciences. Psychology gas chromatography margarine monounsaturated fatty acids Oils & fats partially hydrogenated fats Polyunsaturated fatty acids saturated fatty acids Silica Soybean oil Soybeans SP‐2560 Trans fats trans fatty acid analysis vegetable oil Vegetables |
| title | Evaluation of the CP-Sil 88 and SP-2560 GC Columns Used in the Recently Approved AOCS Official Method Ce 1h-05: Determination of cis-, trans-, Saturated, Monounsaturated, and Polyunsaturated Fatty Acids in Vegetable or Non-ruminant Animal Oils and Fats by Capillary GLC Method |
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