Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion
The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K al...
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creator | Yang, Xiaodong Zhou, Xiaojie Yu, Shilun Zhang, Jian Lu, Xianzheng Chen, Xiaomin Lu, Liwei Huang, Weiying Liu, Yaru |
description | The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K alloy with more intragranular lamellar LPSO phases and larger interdendritic ones at the initial homogenized status, which induces the lower DRX ratio, finer DRXed grain size, and negligible aging hardening response subsequently. During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy.
•Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C. |
doi_str_mv | 10.1016/j.msea.2022.143634 |
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•Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2022.143634</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Alloys ; Deformation ; Deformation mode ; Elongation ; Extrusion ; Gadolinium ; Grain orientation ; Grain size ; Heat treating ; High temperature ; LPSO phase ; Magnesium ; Magnesium alloys ; Mechanical properties ; Mechanical property ; Microstructure ; Morphology ; Phases ; Precipitates ; Tensile tests ; Yield strength ; Zinc ; Zirconium base alloys</subject><ispartof>Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2022-08, Vol.851, p.143634, Article 143634</ispartof><rights>2022 Elsevier B.V.</rights><rights>Copyright Elsevier BV Aug 23, 2022</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c328t-695392efb3ddb7b5db18cd0faef3acc432e184538f321aec317f11b0ff3fd3f73</citedby><cites>FETCH-LOGICAL-c328t-695392efb3ddb7b5db18cd0faef3acc432e184538f321aec317f11b0ff3fd3f73</cites><orcidid>0000-0002-3110-764X ; 0000-0003-3369-008X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.msea.2022.143634$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Yang, Xiaodong</creatorcontrib><creatorcontrib>Zhou, Xiaojie</creatorcontrib><creatorcontrib>Yu, Shilun</creatorcontrib><creatorcontrib>Zhang, Jian</creatorcontrib><creatorcontrib>Lu, Xianzheng</creatorcontrib><creatorcontrib>Chen, Xiaomin</creatorcontrib><creatorcontrib>Lu, Liwei</creatorcontrib><creatorcontrib>Huang, Weiying</creatorcontrib><creatorcontrib>Liu, Yaru</creatorcontrib><title>Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion</title><title>Materials science & engineering. A, Structural materials : properties, microstructure and processing</title><description>The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K alloy with more intragranular lamellar LPSO phases and larger interdendritic ones at the initial homogenized status, which induces the lower DRX ratio, finer DRXed grain size, and negligible aging hardening response subsequently. During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy.
•Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.</description><subject>Alloys</subject><subject>Deformation</subject><subject>Deformation mode</subject><subject>Elongation</subject><subject>Extrusion</subject><subject>Gadolinium</subject><subject>Grain orientation</subject><subject>Grain size</subject><subject>Heat treating</subject><subject>High temperature</subject><subject>LPSO phase</subject><subject>Magnesium</subject><subject>Magnesium alloys</subject><subject>Mechanical properties</subject><subject>Mechanical property</subject><subject>Microstructure</subject><subject>Morphology</subject><subject>Phases</subject><subject>Precipitates</subject><subject>Tensile tests</subject><subject>Yield strength</subject><subject>Zinc</subject><subject>Zirconium base alloys</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9kMtq3DAUhkVpoNMkL5CVIGtNdfEVsilDOw1MmUKSRbIRsnQUa_BYriRPM6-Qp66Nu-7qcOD_zn_4ELphdM0oK74c1scIas0p52uWiUJkH9CKVaUgWS2Kj2hFa85ITmvxCX2O8UApZRnNV-j9EfroOsANtOrkfMAq4ZMKzo8RJzgOEFQaA0TsLU4t4J-vZGvIM3npycsU7jp_jviPSy02zloI0Cfsepec6vDRh6H1nX91C7_79bDHQ6vitA5hLksew1sKY3S-v0IXVnURrv_NS_T0_dvj5gfZ7bf3m687ogWvEinqXNQcbCOMacomNw2rtKFWgRVK60xwYFWWi8oKzhRowUrLWEOtFdYIW4pLdLvcHYL_PUJM8uDH0E-VkpeTlLxkxZziS0oHH2MAK6ePjyqcJaNydi4PcnYuZ-dycT5BdwsE0_8nB0FG7aDXYFwAnaTx7n_4Xz2YjTs</recordid><startdate>20220823</startdate><enddate>20220823</enddate><creator>Yang, Xiaodong</creator><creator>Zhou, Xiaojie</creator><creator>Yu, Shilun</creator><creator>Zhang, Jian</creator><creator>Lu, Xianzheng</creator><creator>Chen, Xiaomin</creator><creator>Lu, Liwei</creator><creator>Huang, Weiying</creator><creator>Liu, Yaru</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0002-3110-764X</orcidid><orcidid>https://orcid.org/0000-0003-3369-008X</orcidid></search><sort><creationdate>20220823</creationdate><title>Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion</title><author>Yang, Xiaodong ; Zhou, Xiaojie ; Yu, Shilun ; Zhang, Jian ; Lu, Xianzheng ; Chen, Xiaomin ; Lu, Liwei ; Huang, Weiying ; Liu, Yaru</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c328t-695392efb3ddb7b5db18cd0faef3acc432e184538f321aec317f11b0ff3fd3f73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Alloys</topic><topic>Deformation</topic><topic>Deformation mode</topic><topic>Elongation</topic><topic>Extrusion</topic><topic>Gadolinium</topic><topic>Grain orientation</topic><topic>Grain size</topic><topic>Heat treating</topic><topic>High temperature</topic><topic>LPSO phase</topic><topic>Magnesium</topic><topic>Magnesium alloys</topic><topic>Mechanical properties</topic><topic>Mechanical property</topic><topic>Microstructure</topic><topic>Morphology</topic><topic>Phases</topic><topic>Precipitates</topic><topic>Tensile tests</topic><topic>Yield strength</topic><topic>Zinc</topic><topic>Zirconium base alloys</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Xiaodong</creatorcontrib><creatorcontrib>Zhou, Xiaojie</creatorcontrib><creatorcontrib>Yu, Shilun</creatorcontrib><creatorcontrib>Zhang, Jian</creatorcontrib><creatorcontrib>Lu, Xianzheng</creatorcontrib><creatorcontrib>Chen, Xiaomin</creatorcontrib><creatorcontrib>Lu, Liwei</creatorcontrib><creatorcontrib>Huang, Weiying</creatorcontrib><creatorcontrib>Liu, Yaru</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Xiaodong</au><au>Zhou, Xiaojie</au><au>Yu, Shilun</au><au>Zhang, Jian</au><au>Lu, Xianzheng</au><au>Chen, Xiaomin</au><au>Lu, Liwei</au><au>Huang, Weiying</au><au>Liu, Yaru</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion</atitle><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2022-08-23</date><risdate>2022</risdate><volume>851</volume><spage>143634</spage><pages>143634-</pages><artnum>143634</artnum><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K alloy with more intragranular lamellar LPSO phases and larger interdendritic ones at the initial homogenized status, which induces the lower DRX ratio, finer DRXed grain size, and negligible aging hardening response subsequently. During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy.
•Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2022.143634</doi><orcidid>https://orcid.org/0000-0002-3110-764X</orcidid><orcidid>https://orcid.org/0000-0003-3369-008X</orcidid></addata></record> |
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subjects | Alloys Deformation Deformation mode Elongation Extrusion Gadolinium Grain orientation Grain size Heat treating High temperature LPSO phase Magnesium Magnesium alloys Mechanical properties Mechanical property Microstructure Morphology Phases Precipitates Tensile tests Yield strength Zinc Zirconium base alloys |
title | Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion |
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