Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion

The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K al...

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Veröffentlicht in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2022-08, Vol.851, p.143634, Article 143634
Hauptverfasser: Yang, Xiaodong, Zhou, Xiaojie, Yu, Shilun, Zhang, Jian, Lu, Xianzheng, Chen, Xiaomin, Lu, Liwei, Huang, Weiying, Liu, Yaru
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container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
container_volume 851
creator Yang, Xiaodong
Zhou, Xiaojie
Yu, Shilun
Zhang, Jian
Lu, Xianzheng
Chen, Xiaomin
Lu, Liwei
Huang, Weiying
Liu, Yaru
description The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K alloy with more intragranular lamellar LPSO phases and larger interdendritic ones at the initial homogenized status, which induces the lower DRX ratio, finer DRXed grain size, and negligible aging hardening response subsequently. During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy. •Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.
doi_str_mv 10.1016/j.msea.2022.143634
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During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy. •Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2022.143634</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Alloys ; Deformation ; Deformation mode ; Elongation ; Extrusion ; Gadolinium ; Grain orientation ; Grain size ; Heat treating ; High temperature ; LPSO phase ; Magnesium ; Magnesium alloys ; Mechanical properties ; Mechanical property ; Microstructure ; Morphology ; Phases ; Precipitates ; Tensile tests ; Yield strength ; Zinc ; Zirconium base alloys</subject><ispartof>Materials science &amp; engineering. 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A, Structural materials : properties, microstructure and processing</title><description>The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K alloy with more intragranular lamellar LPSO phases and larger interdendritic ones at the initial homogenized status, which induces the lower DRX ratio, finer DRXed grain size, and negligible aging hardening response subsequently. During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy. •Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.</description><subject>Alloys</subject><subject>Deformation</subject><subject>Deformation mode</subject><subject>Elongation</subject><subject>Extrusion</subject><subject>Gadolinium</subject><subject>Grain orientation</subject><subject>Grain size</subject><subject>Heat treating</subject><subject>High temperature</subject><subject>LPSO phase</subject><subject>Magnesium</subject><subject>Magnesium alloys</subject><subject>Mechanical properties</subject><subject>Mechanical property</subject><subject>Microstructure</subject><subject>Morphology</subject><subject>Phases</subject><subject>Precipitates</subject><subject>Tensile tests</subject><subject>Yield strength</subject><subject>Zinc</subject><subject>Zirconium base alloys</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9kMtq3DAUhkVpoNMkL5CVIGtNdfEVsilDOw1MmUKSRbIRsnQUa_BYriRPM6-Qp66Nu-7qcOD_zn_4ELphdM0oK74c1scIas0p52uWiUJkH9CKVaUgWS2Kj2hFa85ITmvxCX2O8UApZRnNV-j9EfroOsANtOrkfMAq4ZMKzo8RJzgOEFQaA0TsLU4t4J-vZGvIM3npycsU7jp_jviPSy02zloI0Cfsepec6vDRh6H1nX91C7_79bDHQ6vitA5hLksew1sKY3S-v0IXVnURrv_NS_T0_dvj5gfZ7bf3m687ogWvEinqXNQcbCOMacomNw2rtKFWgRVK60xwYFWWi8oKzhRowUrLWEOtFdYIW4pLdLvcHYL_PUJM8uDH0E-VkpeTlLxkxZziS0oHH2MAK6ePjyqcJaNydi4PcnYuZ-dycT5BdwsE0_8nB0FG7aDXYFwAnaTx7n_4Xz2YjTs</recordid><startdate>20220823</startdate><enddate>20220823</enddate><creator>Yang, Xiaodong</creator><creator>Zhou, Xiaojie</creator><creator>Yu, Shilun</creator><creator>Zhang, Jian</creator><creator>Lu, Xianzheng</creator><creator>Chen, Xiaomin</creator><creator>Lu, Liwei</creator><creator>Huang, Weiying</creator><creator>Liu, Yaru</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0002-3110-764X</orcidid><orcidid>https://orcid.org/0000-0003-3369-008X</orcidid></search><sort><creationdate>20220823</creationdate><title>Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion</title><author>Yang, Xiaodong ; Zhou, Xiaojie ; Yu, Shilun ; Zhang, Jian ; Lu, Xianzheng ; Chen, Xiaomin ; Lu, Liwei ; Huang, Weiying ; Liu, Yaru</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c328t-695392efb3ddb7b5db18cd0faef3acc432e184538f321aec317f11b0ff3fd3f73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Alloys</topic><topic>Deformation</topic><topic>Deformation mode</topic><topic>Elongation</topic><topic>Extrusion</topic><topic>Gadolinium</topic><topic>Grain orientation</topic><topic>Grain size</topic><topic>Heat treating</topic><topic>High temperature</topic><topic>LPSO phase</topic><topic>Magnesium</topic><topic>Magnesium alloys</topic><topic>Mechanical properties</topic><topic>Mechanical property</topic><topic>Microstructure</topic><topic>Morphology</topic><topic>Phases</topic><topic>Precipitates</topic><topic>Tensile tests</topic><topic>Yield strength</topic><topic>Zinc</topic><topic>Zirconium base alloys</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Xiaodong</creatorcontrib><creatorcontrib>Zhou, Xiaojie</creatorcontrib><creatorcontrib>Yu, Shilun</creatorcontrib><creatorcontrib>Zhang, Jian</creatorcontrib><creatorcontrib>Lu, Xianzheng</creatorcontrib><creatorcontrib>Chen, Xiaomin</creatorcontrib><creatorcontrib>Lu, Liwei</creatorcontrib><creatorcontrib>Huang, Weiying</creatorcontrib><creatorcontrib>Liu, Yaru</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science &amp; engineering. 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A, Structural materials : properties, microstructure and processing</jtitle><date>2022-08-23</date><risdate>2022</risdate><volume>851</volume><spage>143634</spage><pages>143634-</pages><artnum>143634</artnum><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>The tensile behavior at (−100)-300 °C of the extruded and peak-aged Mg-5Gd-3Y-xZn-0.5Zr (x = 1 and 2 wt%, designated as VWZ531K and VWZ532K) alloys was investigated in the aspects of microstructural evolution, deformation modes, mechanical properties, etc. The higher Zn content endows the VWZ532K alloy with more intragranular lamellar LPSO phases and larger interdendritic ones at the initial homogenized status, which induces the lower DRX ratio, finer DRXed grain size, and negligible aging hardening response subsequently. During extrusion, precipitation of intragranular LPSO phases occurred in the VWZ531K alloy and partial DRXed grains formed a special texture component with the c-axis aligning parallel to the extrusion direction. However, the VWZ532K alloy experienced the dissolution of intragranular LPSO and dynamic precipitation of β phases. During tensile tests, deformation modes (including twinning, basal slip and non-basal slip) were modified by the testing temperature, grain orientation, LPSO morphology, etc. Compared with the β′ precipitates, LPSO phases are more thermostable to maintain the high-temperature strength, which induce the higher tensile yield strength of the peak-aged VWZ532K alloy (182 MPa) at 300 °C. The larger volume fraction of tension twins and lamellar LPSO phases result in the abnormal high elongation (17.9%) at −100 °C for the VWZ531K alloy. •Initial LPSO morphology affects the DRX ratio, grain size, and aging response.•Phase dissolution and dynamic precipitation both occur during extrusion.•Partial DRXed grains exhibit a special texture component.•LPSO phases are more thermostable to maintain the high-temperature strength.•Tension twins and non-basal slip lead to an abnormal high elongation at −100 °C.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2022.143634</doi><orcidid>https://orcid.org/0000-0002-3110-764X</orcidid><orcidid>https://orcid.org/0000-0003-3369-008X</orcidid></addata></record>
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ispartof Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2022-08, Vol.851, p.143634, Article 143634
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source ScienceDirect Journals (5 years ago - present)
subjects Alloys
Deformation
Deformation mode
Elongation
Extrusion
Gadolinium
Grain orientation
Grain size
Heat treating
High temperature
LPSO phase
Magnesium
Magnesium alloys
Mechanical properties
Mechanical property
Microstructure
Morphology
Phases
Precipitates
Tensile tests
Yield strength
Zinc
Zirconium base alloys
title Tensile behavior at various temperatures of the Mg-Gd-Y-Zn-Zr alloys with different initial morphologies of LPSO phases prior to extrusion
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