Analysis of Spectroscopic, Morphological Characterization and Interaction of Dye Molecules for the Surface Modification of TiB2 Nanoparticles
Nanoparticles of titanium diboride (TiB2) coated with a conductive polymer and subjected to an oxidizing agent was carried out in this research. TiB2 nanoparticles coated with polypyrrole (PPy) were studied using XRD and TEM techniques. Nitrogen adsorption and desorption properties of nanoparticles...
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| Veröffentlicht in: | Journal of nanomaterials 2022-10, Vol.2022 |
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| creator | Mayakannan, S. Rathinam, R. Saminathan, Rajasekaran Deepalakshmi, R. Gopal, Mahesh Hillary, J. Justin Maria Nanthakumar, S. Ganvir, V. Y. Singh, Pallavi |
| description | Nanoparticles of titanium diboride (TiB2) coated with a conductive polymer and subjected to an oxidizing agent was carried out in this research. TiB2 nanoparticles coated with polypyrrole (PPy) were studied using XRD and TEM techniques. Nitrogen adsorption and desorption properties of nanoparticles are covered with modified polypyrrole to understand better the surface zone, structural features, and pore geometries of the nanoparticles. The water-based hazardous anionic Congo red (CR) dye was removed using polypyrrole-coated titanium diboride (PPy@TiB2) nanoparticles. Numerous cutting-edge experimental techniques, including FTIR, FE-SEM, EDXS, and element mapping analysis, were used to confirm the CR color’s adhesion to the PPy@TiB2 nanoadsorbent study. While conducting batch experiments, coated TiB2 nanoadsorbents with polypyrrole enhanced the adsorption behaviour. One of the factors evaluated in the adsorption tests was pH; another was contact time, and a third was dose. At pH=4, 98.75% of Congo red dye was detached using 60 mg of PPy-coated TiB2 nanoadsorbent. Several sorption-desorption cycles were performed on this nanoadsorbent to determine its reusability. An excellent adsorption capacity for water treatment is reported in PPy-coated TiB2 nanoadsorbent. |
| doi_str_mv | 10.1155/2022/1033216 |
| format | Article |
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Justin Maria ; Nanthakumar, S. ; Ganvir, V. Y. ; Singh, Pallavi</creator><contributor>Yahaya, Ridwan ; Ridwan Yahaya</contributor><creatorcontrib>Mayakannan, S. ; Rathinam, R. ; Saminathan, Rajasekaran ; Deepalakshmi, R. ; Gopal, Mahesh ; Hillary, J. Justin Maria ; Nanthakumar, S. ; Ganvir, V. Y. ; Singh, Pallavi ; Yahaya, Ridwan ; Ridwan Yahaya</creatorcontrib><description>Nanoparticles of titanium diboride (TiB2) coated with a conductive polymer and subjected to an oxidizing agent was carried out in this research. TiB2 nanoparticles coated with polypyrrole (PPy) were studied using XRD and TEM techniques. Nitrogen adsorption and desorption properties of nanoparticles are covered with modified polypyrrole to understand better the surface zone, structural features, and pore geometries of the nanoparticles. The water-based hazardous anionic Congo red (CR) dye was removed using polypyrrole-coated titanium diboride (PPy@TiB2) nanoparticles. Numerous cutting-edge experimental techniques, including FTIR, FE-SEM, EDXS, and element mapping analysis, were used to confirm the CR color’s adhesion to the PPy@TiB2 nanoadsorbent study. While conducting batch experiments, coated TiB2 nanoadsorbents with polypyrrole enhanced the adsorption behaviour. One of the factors evaluated in the adsorption tests was pH; another was contact time, and a third was dose. At pH=4, 98.75% of Congo red dye was detached using 60 mg of PPy-coated TiB2 nanoadsorbent. Several sorption-desorption cycles were performed on this nanoadsorbent to determine its reusability. An excellent adsorption capacity for water treatment is reported in PPy-coated TiB2 nanoadsorbent.</description><identifier>ISSN: 1687-4110</identifier><identifier>EISSN: 1687-4129</identifier><identifier>DOI: 10.1155/2022/1033216</identifier><language>eng</language><publisher>New York: Hindawi</publisher><subject>Adsorbents ; Adsorption ; Atoms & subatomic particles ; Binding sites ; Conducting polymers ; Desorption ; Dyes ; Effluents ; Experiments ; Nanocomposites ; Nanomaterials ; Nanoparticles ; Nitrogen ; Oxidation ; Oxidizing agents ; Photocatalysis ; Polymerization ; Polymers ; Polypyrroles ; Surface chemistry ; Titanium ; Titanium diboride ; Water treatment</subject><ispartof>Journal of nanomaterials, 2022-10, Vol.2022</ispartof><rights>Copyright © 2022 S. Mayakannan et al.</rights><rights>Copyright © 2022 S. Mayakannan et al. This is an open access article distributed under the Creative Commons Attribution License (the “License”), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. https://creativecommons.org/licenses/by/4.0</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c230t-b8e1541993513ae682a318a39135c070297a23bffe61b9f48fd9cfb7687e65993</citedby><orcidid>0000-0003-0284-1818 ; 0000-0001-7672-5399 ; 0000-0001-9783-9053 ; 0000-0002-0167-0757</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><contributor>Yahaya, Ridwan</contributor><contributor>Ridwan Yahaya</contributor><creatorcontrib>Mayakannan, S.</creatorcontrib><creatorcontrib>Rathinam, R.</creatorcontrib><creatorcontrib>Saminathan, Rajasekaran</creatorcontrib><creatorcontrib>Deepalakshmi, R.</creatorcontrib><creatorcontrib>Gopal, Mahesh</creatorcontrib><creatorcontrib>Hillary, J. Justin Maria</creatorcontrib><creatorcontrib>Nanthakumar, S.</creatorcontrib><creatorcontrib>Ganvir, V. Y.</creatorcontrib><creatorcontrib>Singh, Pallavi</creatorcontrib><title>Analysis of Spectroscopic, Morphological Characterization and Interaction of Dye Molecules for the Surface Modification of TiB2 Nanoparticles</title><title>Journal of nanomaterials</title><description>Nanoparticles of titanium diboride (TiB2) coated with a conductive polymer and subjected to an oxidizing agent was carried out in this research. TiB2 nanoparticles coated with polypyrrole (PPy) were studied using XRD and TEM techniques. Nitrogen adsorption and desorption properties of nanoparticles are covered with modified polypyrrole to understand better the surface zone, structural features, and pore geometries of the nanoparticles. The water-based hazardous anionic Congo red (CR) dye was removed using polypyrrole-coated titanium diboride (PPy@TiB2) nanoparticles. Numerous cutting-edge experimental techniques, including FTIR, FE-SEM, EDXS, and element mapping analysis, were used to confirm the CR color’s adhesion to the PPy@TiB2 nanoadsorbent study. While conducting batch experiments, coated TiB2 nanoadsorbents with polypyrrole enhanced the adsorption behaviour. One of the factors evaluated in the adsorption tests was pH; another was contact time, and a third was dose. At pH=4, 98.75% of Congo red dye was detached using 60 mg of PPy-coated TiB2 nanoadsorbent. Several sorption-desorption cycles were performed on this nanoadsorbent to determine its reusability. An excellent adsorption capacity for water treatment is reported in PPy-coated TiB2 nanoadsorbent.</description><subject>Adsorbents</subject><subject>Adsorption</subject><subject>Atoms & subatomic particles</subject><subject>Binding sites</subject><subject>Conducting polymers</subject><subject>Desorption</subject><subject>Dyes</subject><subject>Effluents</subject><subject>Experiments</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Nitrogen</subject><subject>Oxidation</subject><subject>Oxidizing agents</subject><subject>Photocatalysis</subject><subject>Polymerization</subject><subject>Polymers</subject><subject>Polypyrroles</subject><subject>Surface chemistry</subject><subject>Titanium</subject><subject>Titanium diboride</subject><subject>Water treatment</subject><issn>1687-4110</issn><issn>1687-4129</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>RHX</sourceid><sourceid>BENPR</sourceid><recordid>eNo9kMtOwzAQRS0EEqWw4wMssYRQP_LyspRXpQKLlnU0cWziKsTBToTKP_DPOCqwmpk7997FQeickmtKk2TGCGMzSjhnND1AE5rmWRRTJg7_d0qO0Yn3W0LiRCRsgr7nLTQ7bzy2Gq87JXtnvbSdkVf4ybquto19MxIavKjBgeyVM1_QG9tiaCu8bIMQ1PEOBbc7FVKNkkOjPNbW4b5WeD04DXL8VEaHrj_3xtww_Ayt7cD1RobIKTrS0Hh19jun6PX-brN4jFYvD8vFfBVJxkkflbmiSUyF4AnloNKcAac5cEF5IklGmMiA8VJrldJS6DjXlZC6zAIDlSYhNkUX-97O2Y9B-b7Y2sEFEr5gGctiwVNGguty76pNW8GnKTpn3sHtCkqKkXcx8i5-efMfHOxzLg</recordid><startdate>20221015</startdate><enddate>20221015</enddate><creator>Mayakannan, S.</creator><creator>Rathinam, R.</creator><creator>Saminathan, Rajasekaran</creator><creator>Deepalakshmi, R.</creator><creator>Gopal, Mahesh</creator><creator>Hillary, J. 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The water-based hazardous anionic Congo red (CR) dye was removed using polypyrrole-coated titanium diboride (PPy@TiB2) nanoparticles. Numerous cutting-edge experimental techniques, including FTIR, FE-SEM, EDXS, and element mapping analysis, were used to confirm the CR color’s adhesion to the PPy@TiB2 nanoadsorbent study. While conducting batch experiments, coated TiB2 nanoadsorbents with polypyrrole enhanced the adsorption behaviour. One of the factors evaluated in the adsorption tests was pH; another was contact time, and a third was dose. At pH=4, 98.75% of Congo red dye was detached using 60 mg of PPy-coated TiB2 nanoadsorbent. Several sorption-desorption cycles were performed on this nanoadsorbent to determine its reusability. 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| subjects | Adsorbents Adsorption Atoms & subatomic particles Binding sites Conducting polymers Desorption Dyes Effluents Experiments Nanocomposites Nanomaterials Nanoparticles Nitrogen Oxidation Oxidizing agents Photocatalysis Polymerization Polymers Polypyrroles Surface chemistry Titanium Titanium diboride Water treatment |
| title | Analysis of Spectroscopic, Morphological Characterization and Interaction of Dye Molecules for the Surface Modification of TiB2 Nanoparticles |
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