A new promising Pt(Mo2C) catalyst for hydrogen evolution reaction prepared by galvanic displacement reaction
A new method for the synthesis of Pt(Mo 2 C) catalysts using the redox reaction between Mo 2 C and solution containing potassium tetracholoplatinate (II) is proposed. The obtained catalyst samples are characterized by SEM, XRD, XPS, and CV methods. As shown by microscopic studies, platinum nanoclust...
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| Veröffentlicht in: | Journal of solid state electrochemistry 2022-10, Vol.26 (10), p.2183-2193 |
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| container_title | Journal of solid state electrochemistry |
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| creator | Kuznetsov, Vitaly V. Podlovchenko, Boris I. Frolov, Kirill V. Volkov, Mikhail A. Khanin, Dmitry A. |
| description | A new method for the synthesis of Pt(Mo
2
C) catalysts using the redox reaction between Mo
2
C and solution containing potassium tetracholoplatinate (II) is proposed. The obtained catalyst samples are characterized by SEM, XRD, XPS, and CV methods. As shown by microscopic studies, platinum nanoclusters are dispersed over the surface of carbide particles. The synthesized catalysts demonstrate a high catalytic activity towards hydrogen evolution reaction (HER) in 0.5 M sulphuric acid solution. Such activity is observed even at very low platinum loadings. |
| doi_str_mv | 10.1007/s10008-022-05222-x |
| format | Article |
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2
C) catalysts using the redox reaction between Mo
2
C and solution containing potassium tetracholoplatinate (II) is proposed. The obtained catalyst samples are characterized by SEM, XRD, XPS, and CV methods. As shown by microscopic studies, platinum nanoclusters are dispersed over the surface of carbide particles. The synthesized catalysts demonstrate a high catalytic activity towards hydrogen evolution reaction (HER) in 0.5 M sulphuric acid solution. Such activity is observed even at very low platinum loadings.</description><identifier>ISSN: 1432-8488</identifier><identifier>EISSN: 1433-0768</identifier><identifier>DOI: 10.1007/s10008-022-05222-x</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Analytical Chemistry ; Catalysts ; Catalytic activity ; Characterization and Evaluation of Materials ; Chemical synthesis ; Chemistry ; Chemistry and Materials Science ; Condensed Matter Physics ; Electrochemistry ; Energy Storage ; Hydrogen evolution reactions ; Molybdenum carbide ; Nanoclusters ; Original Paper ; Physical Chemistry ; Platinum ; Redox reactions ; Sulfuric acid ; X ray photoelectron spectroscopy</subject><ispartof>Journal of solid state electrochemistry, 2022-10, Vol.26 (10), p.2183-2193</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2022</rights><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2022.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-3067ea81971d7d63f5753736397e0768cca8765205560d89cb30b6cde9204be33</citedby><cites>FETCH-LOGICAL-c319t-3067ea81971d7d63f5753736397e0768cca8765205560d89cb30b6cde9204be33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10008-022-05222-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10008-022-05222-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Kuznetsov, Vitaly V.</creatorcontrib><creatorcontrib>Podlovchenko, Boris I.</creatorcontrib><creatorcontrib>Frolov, Kirill V.</creatorcontrib><creatorcontrib>Volkov, Mikhail A.</creatorcontrib><creatorcontrib>Khanin, Dmitry A.</creatorcontrib><title>A new promising Pt(Mo2C) catalyst for hydrogen evolution reaction prepared by galvanic displacement reaction</title><title>Journal of solid state electrochemistry</title><addtitle>J Solid State Electrochem</addtitle><description>A new method for the synthesis of Pt(Mo
2
C) catalysts using the redox reaction between Mo
2
C and solution containing potassium tetracholoplatinate (II) is proposed. The obtained catalyst samples are characterized by SEM, XRD, XPS, and CV methods. As shown by microscopic studies, platinum nanoclusters are dispersed over the surface of carbide particles. The synthesized catalysts demonstrate a high catalytic activity towards hydrogen evolution reaction (HER) in 0.5 M sulphuric acid solution. Such activity is observed even at very low platinum loadings.</description><subject>Analytical Chemistry</subject><subject>Catalysts</subject><subject>Catalytic activity</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Condensed Matter Physics</subject><subject>Electrochemistry</subject><subject>Energy Storage</subject><subject>Hydrogen evolution reactions</subject><subject>Molybdenum carbide</subject><subject>Nanoclusters</subject><subject>Original Paper</subject><subject>Physical Chemistry</subject><subject>Platinum</subject><subject>Redox reactions</subject><subject>Sulfuric acid</subject><subject>X ray photoelectron spectroscopy</subject><issn>1432-8488</issn><issn>1433-0768</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9UD1PwzAUtBBIlMIfYLLEAkPg2a4_MlYVX1IRDDBbjuOEVGkS7BSaf4_bINhY7t1wd093CJ0TuCYA8iZEBJUApQlwGnF7gCZkxlgCUqjDPaeJmil1jE5CWAEQKQhMUD3HjfvCnW_XVaiaEr_0l08tXVxha3pTD6HHRevx-5D7tnQNdp9tvemrtsHeGbsnnXed8S7H2YBLU3-aprI4r0JXG-vWrul_pafoqDB1cGc_d4re7m5fFw_J8vn-cTFfJpaRtE8YCOmMIqkkucwFK7jkTDLBUul2daw1SgpOgXMBuUptxiATNncphVnmGJuiizE31vrYuNDrVbvxTXypqQQuJVOCRxUdVda3IXhX6M5Xa-MHTUDvVtXjqjquqver6m00sdEUorgpnf-L_sf1DdLvevY</recordid><startdate>20221001</startdate><enddate>20221001</enddate><creator>Kuznetsov, Vitaly V.</creator><creator>Podlovchenko, Boris I.</creator><creator>Frolov, Kirill V.</creator><creator>Volkov, Mikhail A.</creator><creator>Khanin, Dmitry A.</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20221001</creationdate><title>A new promising Pt(Mo2C) catalyst for hydrogen evolution reaction prepared by galvanic displacement reaction</title><author>Kuznetsov, Vitaly V. ; Podlovchenko, Boris I. ; Frolov, Kirill V. ; Volkov, Mikhail A. ; Khanin, Dmitry A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-3067ea81971d7d63f5753736397e0768cca8765205560d89cb30b6cde9204be33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Analytical Chemistry</topic><topic>Catalysts</topic><topic>Catalytic activity</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical synthesis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Condensed Matter Physics</topic><topic>Electrochemistry</topic><topic>Energy Storage</topic><topic>Hydrogen evolution reactions</topic><topic>Molybdenum carbide</topic><topic>Nanoclusters</topic><topic>Original Paper</topic><topic>Physical Chemistry</topic><topic>Platinum</topic><topic>Redox reactions</topic><topic>Sulfuric acid</topic><topic>X ray photoelectron spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kuznetsov, Vitaly V.</creatorcontrib><creatorcontrib>Podlovchenko, Boris I.</creatorcontrib><creatorcontrib>Frolov, Kirill V.</creatorcontrib><creatorcontrib>Volkov, Mikhail A.</creatorcontrib><creatorcontrib>Khanin, Dmitry A.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of solid state electrochemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kuznetsov, Vitaly V.</au><au>Podlovchenko, Boris I.</au><au>Frolov, Kirill V.</au><au>Volkov, Mikhail A.</au><au>Khanin, Dmitry A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A new promising Pt(Mo2C) catalyst for hydrogen evolution reaction prepared by galvanic displacement reaction</atitle><jtitle>Journal of solid state electrochemistry</jtitle><stitle>J Solid State Electrochem</stitle><date>2022-10-01</date><risdate>2022</risdate><volume>26</volume><issue>10</issue><spage>2183</spage><epage>2193</epage><pages>2183-2193</pages><issn>1432-8488</issn><eissn>1433-0768</eissn><abstract>A new method for the synthesis of Pt(Mo
2
C) catalysts using the redox reaction between Mo
2
C and solution containing potassium tetracholoplatinate (II) is proposed. The obtained catalyst samples are characterized by SEM, XRD, XPS, and CV methods. As shown by microscopic studies, platinum nanoclusters are dispersed over the surface of carbide particles. The synthesized catalysts demonstrate a high catalytic activity towards hydrogen evolution reaction (HER) in 0.5 M sulphuric acid solution. Such activity is observed even at very low platinum loadings.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s10008-022-05222-x</doi><tpages>11</tpages></addata></record> |
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| subjects | Analytical Chemistry Catalysts Catalytic activity Characterization and Evaluation of Materials Chemical synthesis Chemistry Chemistry and Materials Science Condensed Matter Physics Electrochemistry Energy Storage Hydrogen evolution reactions Molybdenum carbide Nanoclusters Original Paper Physical Chemistry Platinum Redox reactions Sulfuric acid X ray photoelectron spectroscopy |
| title | A new promising Pt(Mo2C) catalyst for hydrogen evolution reaction prepared by galvanic displacement reaction |
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