Novel Zero Headspace Solid-Liquid Extraction for the Recovery of Polyphenolic Fractions from Grape Pomace
Grape pomace (GP) is a good source of high-value compounds as up to 60% of grape polyphenols remain in it after wine-making. To overcome traditional membrane technologies’ d rawbacks, such as fouling, a novel Zero Head Space extraction (ZHE) procedure was developed. The reaction vessel comprised a f...
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| Veröffentlicht in: | Processes 2022-06, Vol.10 (6), p.1112 |
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| creator | Orozco-Flores, Laura Salas, Erika González-Sánchez, Guillermo Chávez-Flores, David Ramírez-García, Raúl Rocha-Gutiérrez, Beatriz Peralta-Pérez, María Ballinas-Casarrubias, María |
| description | Grape pomace (GP) is a good source of high-value compounds as up to 60% of grape polyphenols remain in it after wine-making. To overcome traditional membrane technologies’ d rawbacks, such as fouling, a novel Zero Head Space extraction (ZHE) procedure was developed. The reaction vessel comprised a filtration device with a nitrocellulose membrane. The separation was performed at 50 lb/in2 and 23 °C, with no headspace during the process. Water and methanol (both acidifie d) were evaluated as solvents during two extraction stages for the recovery and fractionation of polyphenols. Aqueous extract (AE) was mainly constituted by monomeric polyphenols while Methanol extract (ME) presented less soluble compounds, as well as a higher concentration of total anthocyanin content than AE. Additional methanolic (CE) and acetone (CAE) extractions of residual GP showed CE presented a similar profile to ME (at a lower concentration), indicating ZHE efficiency at extracting polyphenols in GP. CAE presented a non-resolved hump, characteristic of high proanthocyanidins’ polydispersity. ZHE rendered a monomeric fraction in ME (mean Degree of Polymerization, mDP of 1.38). Residual GP (cake) extractions demonstrated oligomeric polyphenol retention; mDP up to 3.05 when acetone was used. Fractionation of GP polyphenols was successfully established using a Zero Head space extractor. |
| doi_str_mv | 10.3390/pr10061112 |
| format | Article |
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To overcome traditional membrane technologies’ d rawbacks, such as fouling, a novel Zero Head Space extraction (ZHE) procedure was developed. The reaction vessel comprised a filtration device with a nitrocellulose membrane. The separation was performed at 50 lb/in2 and 23 °C, with no headspace during the process. Water and methanol (both acidifie d) were evaluated as solvents during two extraction stages for the recovery and fractionation of polyphenols. Aqueous extract (AE) was mainly constituted by monomeric polyphenols while Methanol extract (ME) presented less soluble compounds, as well as a higher concentration of total anthocyanin content than AE. Additional methanolic (CE) and acetone (CAE) extractions of residual GP showed CE presented a similar profile to ME (at a lower concentration), indicating ZHE efficiency at extracting polyphenols in GP. CAE presented a non-resolved hump, characteristic of high proanthocyanidins’ polydispersity. ZHE rendered a monomeric fraction in ME (mean Degree of Polymerization, mDP of 1.38). Residual GP (cake) extractions demonstrated oligomeric polyphenol retention; mDP up to 3.05 when acetone was used. Fractionation of GP polyphenols was successfully established using a Zero Head space extractor.</description><identifier>ISSN: 2227-9717</identifier><identifier>EISSN: 2227-9717</identifier><identifier>DOI: 10.3390/pr10061112</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Acetone ; Acidification ; Anthocyanins ; Cellulose esters ; Cellulose nitrate ; Chromatography ; Degree of polymerization ; Efficiency ; Fractionation ; Grapes ; Headspace ; Membranes ; Methanol ; Phytochemicals ; Polydispersity ; Polyphenols ; Pore size ; Recovery ; Seeds ; Solvents ; Wineries & vineyards</subject><ispartof>Processes, 2022-06, Vol.10 (6), p.1112</ispartof><rights>2022 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). 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ZHE rendered a monomeric fraction in ME (mean Degree of Polymerization, mDP of 1.38). Residual GP (cake) extractions demonstrated oligomeric polyphenol retention; mDP up to 3.05 when acetone was used. 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Salas, Erika ; González-Sánchez, Guillermo ; Chávez-Flores, David ; Ramírez-García, Raúl ; Rocha-Gutiérrez, Beatriz ; Peralta-Pérez, María ; Ballinas-Casarrubias, María</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c295t-16a850f3d70a7c3db10099a7229a7de100eee4be7f998d08326a7ae32723c31e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Acetone</topic><topic>Acidification</topic><topic>Anthocyanins</topic><topic>Cellulose esters</topic><topic>Cellulose nitrate</topic><topic>Chromatography</topic><topic>Degree of polymerization</topic><topic>Efficiency</topic><topic>Fractionation</topic><topic>Grapes</topic><topic>Headspace</topic><topic>Membranes</topic><topic>Methanol</topic><topic>Phytochemicals</topic><topic>Polydispersity</topic><topic>Polyphenols</topic><topic>Pore size</topic><topic>Recovery</topic><topic>Seeds</topic><topic>Solvents</topic><topic>Wineries & vineyards</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Orozco-Flores, Laura</creatorcontrib><creatorcontrib>Salas, Erika</creatorcontrib><creatorcontrib>González-Sánchez, Guillermo</creatorcontrib><creatorcontrib>Chávez-Flores, David</creatorcontrib><creatorcontrib>Ramírez-García, Raúl</creatorcontrib><creatorcontrib>Rocha-Gutiérrez, Beatriz</creatorcontrib><creatorcontrib>Peralta-Pérez, María</creatorcontrib><creatorcontrib>Ballinas-Casarrubias, María</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>ProQuest Biological Science Collection</collection><collection>Biological Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>Processes</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Orozco-Flores, Laura</au><au>Salas, Erika</au><au>González-Sánchez, Guillermo</au><au>Chávez-Flores, David</au><au>Ramírez-García, Raúl</au><au>Rocha-Gutiérrez, Beatriz</au><au>Peralta-Pérez, María</au><au>Ballinas-Casarrubias, María</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Novel Zero Headspace Solid-Liquid Extraction for the Recovery of Polyphenolic Fractions from Grape Pomace</atitle><jtitle>Processes</jtitle><date>2022-06-01</date><risdate>2022</risdate><volume>10</volume><issue>6</issue><spage>1112</spage><pages>1112-</pages><issn>2227-9717</issn><eissn>2227-9717</eissn><abstract>Grape pomace (GP) is a good source of high-value compounds as up to 60% of grape polyphenols remain in it after wine-making. To overcome traditional membrane technologies’ d rawbacks, such as fouling, a novel Zero Head Space extraction (ZHE) procedure was developed. The reaction vessel comprised a filtration device with a nitrocellulose membrane. The separation was performed at 50 lb/in2 and 23 °C, with no headspace during the process. Water and methanol (both acidifie d) were evaluated as solvents during two extraction stages for the recovery and fractionation of polyphenols. Aqueous extract (AE) was mainly constituted by monomeric polyphenols while Methanol extract (ME) presented less soluble compounds, as well as a higher concentration of total anthocyanin content than AE. Additional methanolic (CE) and acetone (CAE) extractions of residual GP showed CE presented a similar profile to ME (at a lower concentration), indicating ZHE efficiency at extracting polyphenols in GP. CAE presented a non-resolved hump, characteristic of high proanthocyanidins’ polydispersity. ZHE rendered a monomeric fraction in ME (mean Degree of Polymerization, mDP of 1.38). Residual GP (cake) extractions demonstrated oligomeric polyphenol retention; mDP up to 3.05 when acetone was used. Fractionation of GP polyphenols was successfully established using a Zero Head space extractor.</abstract><cop>Basel</cop><pub>MDPI AG</pub><doi>10.3390/pr10061112</doi><orcidid>https://orcid.org/0000-0002-9516-0087</orcidid><orcidid>https://orcid.org/0000-0003-1022-4641</orcidid><orcidid>https://orcid.org/0000-0001-6852-0406</orcidid><orcidid>https://orcid.org/0000-0002-8789-4443</orcidid><orcidid>https://orcid.org/0000-0003-2991-3914</orcidid><oa>free_for_read</oa></addata></record> |
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| source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; MDPI - Multidisciplinary Digital Publishing Institute |
| subjects | Acetone Acidification Anthocyanins Cellulose esters Cellulose nitrate Chromatography Degree of polymerization Efficiency Fractionation Grapes Headspace Membranes Methanol Phytochemicals Polydispersity Polyphenols Pore size Recovery Seeds Solvents Wineries & vineyards |
| title | Novel Zero Headspace Solid-Liquid Extraction for the Recovery of Polyphenolic Fractions from Grape Pomace |
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