Preparation of Niobium(V) Oxide with Controlled Dispersity and Morphology
The effect of the annealing temperature and the chemical history of the precipitate on the morphology and phase composition of Nb 2 O 5 powder was investigated. The precipitate Nb 2 O 5 · n H 2 O and gel-like niobium citrate were obtained by solution methods. The synthesis of niobium oxide was condu...
Gespeichert in:
| Veröffentlicht in: | Glass and ceramics 2022-05, Vol.79 (1-2), p.22-27 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 27 |
|---|---|
| container_issue | 1-2 |
| container_start_page | 22 |
| container_title | Glass and ceramics |
| container_volume | 79 |
| creator | Golubeva, N. K. Danilovich, D. P. Nesmelov, D. D. Shabalkin, I. D. |
| description | The effect of the annealing temperature and the chemical history of the precipitate on the morphology and phase composition of Nb
2
O
5
powder was investigated. The precipitate Nb
2
O
5
·
n
H
2
O and gel-like niobium citrate were obtained by solution methods. The synthesis of niobium oxide was conducted at temperatures 600, 1000, and 1200°C. The products of synthesis were analyzed by means of x-ray diffraction, scanning electron microscopy, x-ray microscopy, and differential thermal and thermogravimetric analysis. The annealing of niobium citrate at 600°C makes it possible to obtain niobium oxide particles with average size equal to about 70 nm, which is 4 – 6 times smaller than Nb
2
O
5
obtained from Nb
2
O
5
·
n
H
2
O precipitate. |
| doi_str_mv | 10.1007/s10717-022-00447-8 |
| format | Article |
| fullrecord | <record><control><sourceid>gale_proqu</sourceid><recordid>TN_cdi_proquest_journals_2675379114</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A706930326</galeid><sourcerecordid>A706930326</sourcerecordid><originalsourceid>FETCH-LOGICAL-c2248-51fa93a464494cfb287d643f625f60bf1fdf439be577e068621df0489838caf63</originalsourceid><addsrcrecordid>eNp9kD1PwzAQhi0EEqXwB5giscCQcv6I7YxV-aoElAFYLSexW1dpHOxU0H9PSpDY0A0nnd7n7vQgdI5hggHEdcQgsEiBkBSAMZHKAzTCmaCpzHB2iEZAOU4Fx3CMTmJcA0AuBB2h-UswrQ66c75JvE2enS_cdnP5fpUsvlxlkk_XrZKZb7rg69pUyY2LrQnRdbtEN1Xy5EO78rVf7k7RkdV1NGe_fYze7m5fZw_p4-J-Pps-piUhTKYZtjqnmnHGclbagkhRcUYtJ5nlUFhsK8toXphMCANccoIrC0zmkspSW07H6GLY2wb_sTWxU2u_DU1_UhEuMipyjFmfmgyppa6Nco31XdBlX5XZuNI3xrp-PhXAcwqU7NeSASiDjzEYq9rgNjrsFAa1d6wGx6p3rH4cK9lDdIBiH26WJvz98g_1DeEJfWg</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2675379114</pqid></control><display><type>article</type><title>Preparation of Niobium(V) Oxide with Controlled Dispersity and Morphology</title><source>Springer Nature - Complete Springer Journals</source><creator>Golubeva, N. K. ; Danilovich, D. P. ; Nesmelov, D. D. ; Shabalkin, I. D.</creator><creatorcontrib>Golubeva, N. K. ; Danilovich, D. P. ; Nesmelov, D. D. ; Shabalkin, I. D.</creatorcontrib><description>The effect of the annealing temperature and the chemical history of the precipitate on the morphology and phase composition of Nb
2
O
5
powder was investigated. The precipitate Nb
2
O
5
·
n
H
2
O and gel-like niobium citrate were obtained by solution methods. The synthesis of niobium oxide was conducted at temperatures 600, 1000, and 1200°C. The products of synthesis were analyzed by means of x-ray diffraction, scanning electron microscopy, x-ray microscopy, and differential thermal and thermogravimetric analysis. The annealing of niobium citrate at 600°C makes it possible to obtain niobium oxide particles with average size equal to about 70 nm, which is 4 – 6 times smaller than Nb
2
O
5
obtained from Nb
2
O
5
·
n
H
2
O precipitate.</description><identifier>ISSN: 0361-7610</identifier><identifier>EISSN: 1573-8515</identifier><identifier>DOI: 10.1007/s10717-022-00447-8</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Annealing ; Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Composites ; Differential thermal analysis ; Differential thermogravimetric analysis ; Diffraction ; Glass ; Materials Science ; Morphology ; Natural Materials ; Niobium oxides ; Phase composition ; Powders ; Synthesis ; Thermogravimetric analysis ; X ray microscopy ; X-rays</subject><ispartof>Glass and ceramics, 2022-05, Vol.79 (1-2), p.22-27</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2022</rights><rights>COPYRIGHT 2022 Springer</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2022.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c2248-51fa93a464494cfb287d643f625f60bf1fdf439be577e068621df0489838caf63</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10717-022-00447-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10717-022-00447-8$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,778,782,27907,27908,41471,42540,51302</link.rule.ids></links><search><creatorcontrib>Golubeva, N. K.</creatorcontrib><creatorcontrib>Danilovich, D. P.</creatorcontrib><creatorcontrib>Nesmelov, D. D.</creatorcontrib><creatorcontrib>Shabalkin, I. D.</creatorcontrib><title>Preparation of Niobium(V) Oxide with Controlled Dispersity and Morphology</title><title>Glass and ceramics</title><addtitle>Glass Ceram</addtitle><description>The effect of the annealing temperature and the chemical history of the precipitate on the morphology and phase composition of Nb
2
O
5
powder was investigated. The precipitate Nb
2
O
5
·
n
H
2
O and gel-like niobium citrate were obtained by solution methods. The synthesis of niobium oxide was conducted at temperatures 600, 1000, and 1200°C. The products of synthesis were analyzed by means of x-ray diffraction, scanning electron microscopy, x-ray microscopy, and differential thermal and thermogravimetric analysis. The annealing of niobium citrate at 600°C makes it possible to obtain niobium oxide particles with average size equal to about 70 nm, which is 4 – 6 times smaller than Nb
2
O
5
obtained from Nb
2
O
5
·
n
H
2
O precipitate.</description><subject>Annealing</subject><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Differential thermal analysis</subject><subject>Differential thermogravimetric analysis</subject><subject>Diffraction</subject><subject>Glass</subject><subject>Materials Science</subject><subject>Morphology</subject><subject>Natural Materials</subject><subject>Niobium oxides</subject><subject>Phase composition</subject><subject>Powders</subject><subject>Synthesis</subject><subject>Thermogravimetric analysis</subject><subject>X ray microscopy</subject><subject>X-rays</subject><issn>0361-7610</issn><issn>1573-8515</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9kD1PwzAQhi0EEqXwB5giscCQcv6I7YxV-aoElAFYLSexW1dpHOxU0H9PSpDY0A0nnd7n7vQgdI5hggHEdcQgsEiBkBSAMZHKAzTCmaCpzHB2iEZAOU4Fx3CMTmJcA0AuBB2h-UswrQ66c75JvE2enS_cdnP5fpUsvlxlkk_XrZKZb7rg69pUyY2LrQnRdbtEN1Xy5EO78rVf7k7RkdV1NGe_fYze7m5fZw_p4-J-Pps-piUhTKYZtjqnmnHGclbagkhRcUYtJ5nlUFhsK8toXphMCANccoIrC0zmkspSW07H6GLY2wb_sTWxU2u_DU1_UhEuMipyjFmfmgyppa6Nco31XdBlX5XZuNI3xrp-PhXAcwqU7NeSASiDjzEYq9rgNjrsFAa1d6wGx6p3rH4cK9lDdIBiH26WJvz98g_1DeEJfWg</recordid><startdate>20220501</startdate><enddate>20220501</enddate><creator>Golubeva, N. K.</creator><creator>Danilovich, D. P.</creator><creator>Nesmelov, D. D.</creator><creator>Shabalkin, I. D.</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20220501</creationdate><title>Preparation of Niobium(V) Oxide with Controlled Dispersity and Morphology</title><author>Golubeva, N. K. ; Danilovich, D. P. ; Nesmelov, D. D. ; Shabalkin, I. D.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2248-51fa93a464494cfb287d643f625f60bf1fdf439be577e068621df0489838caf63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Annealing</topic><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Composites</topic><topic>Differential thermal analysis</topic><topic>Differential thermogravimetric analysis</topic><topic>Diffraction</topic><topic>Glass</topic><topic>Materials Science</topic><topic>Morphology</topic><topic>Natural Materials</topic><topic>Niobium oxides</topic><topic>Phase composition</topic><topic>Powders</topic><topic>Synthesis</topic><topic>Thermogravimetric analysis</topic><topic>X ray microscopy</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Golubeva, N. K.</creatorcontrib><creatorcontrib>Danilovich, D. P.</creatorcontrib><creatorcontrib>Nesmelov, D. D.</creatorcontrib><creatorcontrib>Shabalkin, I. D.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Glass and ceramics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Golubeva, N. K.</au><au>Danilovich, D. P.</au><au>Nesmelov, D. D.</au><au>Shabalkin, I. D.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation of Niobium(V) Oxide with Controlled Dispersity and Morphology</atitle><jtitle>Glass and ceramics</jtitle><stitle>Glass Ceram</stitle><date>2022-05-01</date><risdate>2022</risdate><volume>79</volume><issue>1-2</issue><spage>22</spage><epage>27</epage><pages>22-27</pages><issn>0361-7610</issn><eissn>1573-8515</eissn><abstract>The effect of the annealing temperature and the chemical history of the precipitate on the morphology and phase composition of Nb
2
O
5
powder was investigated. The precipitate Nb
2
O
5
·
n
H
2
O and gel-like niobium citrate were obtained by solution methods. The synthesis of niobium oxide was conducted at temperatures 600, 1000, and 1200°C. The products of synthesis were analyzed by means of x-ray diffraction, scanning electron microscopy, x-ray microscopy, and differential thermal and thermogravimetric analysis. The annealing of niobium citrate at 600°C makes it possible to obtain niobium oxide particles with average size equal to about 70 nm, which is 4 – 6 times smaller than Nb
2
O
5
obtained from Nb
2
O
5
·
n
H
2
O precipitate.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10717-022-00447-8</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0361-7610 |
| ispartof | Glass and ceramics, 2022-05, Vol.79 (1-2), p.22-27 |
| issn | 0361-7610 1573-8515 |
| language | eng |
| recordid | cdi_proquest_journals_2675379114 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Annealing Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Composites Differential thermal analysis Differential thermogravimetric analysis Diffraction Glass Materials Science Morphology Natural Materials Niobium oxides Phase composition Powders Synthesis Thermogravimetric analysis X ray microscopy X-rays |
| title | Preparation of Niobium(V) Oxide with Controlled Dispersity and Morphology |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-16T14%3A33%3A37IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_proqu&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Preparation%20of%20Niobium(V)%20Oxide%20with%20Controlled%20Dispersity%20and%20Morphology&rft.jtitle=Glass%20and%20ceramics&rft.au=Golubeva,%20N.%20K.&rft.date=2022-05-01&rft.volume=79&rft.issue=1-2&rft.spage=22&rft.epage=27&rft.pages=22-27&rft.issn=0361-7610&rft.eissn=1573-8515&rft_id=info:doi/10.1007/s10717-022-00447-8&rft_dat=%3Cgale_proqu%3EA706930326%3C/gale_proqu%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2675379114&rft_id=info:pmid/&rft_galeid=A706930326&rfr_iscdi=true |