Hardness and Indentation Fracture Toughness in a Novel Silicon Composite Synthesized by Spark Plasma Sintering
A composite of 90 wt pct silicon and 10 wt pct of the multi-component Mo 44 Si 26 Ta 5 Zr 5 Fe 3 Co 12 Y 5 was synthesized using spark plasma sintering at a temperature of 1423 K and applied pressure of 75 MPa. The relative density of the composite following the spark plasma sintering was found to b...
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| Veröffentlicht in: | Metallurgical and materials transactions. A, Physical metallurgy and materials science Physical metallurgy and materials science, 2022-07, Vol.53 (7), p.2680-2688 |
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| container_title | Metallurgical and materials transactions. A, Physical metallurgy and materials science |
| container_volume | 53 |
| creator | Samantaray, B. K. Bakshi, S. R. Rajulapati, K. V. Gollapudi, S. |
| description | A composite of 90 wt pct silicon and 10 wt pct of the multi-component Mo
44
Si
26
Ta
5
Zr
5
Fe
3
Co
12
Y
5
was synthesized using spark plasma sintering at a temperature of 1423 K and applied pressure of 75 MPa. The relative density of the composite following the spark plasma sintering was found to be 99 pct. Indentation fracture toughness measurements in the composite using a Vickers diamond indenter yielded a value of 2.29 MPa m
1/2
which is higher than that of elemental silicon at 1.43 MPa m
1/2
. The second phase provided an average hardness of 14 GPa, while silicon demonstrated hardness of 12 GPa. |
| doi_str_mv | 10.1007/s11661-022-06697-z |
| format | Article |
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44
Si
26
Ta
5
Zr
5
Fe
3
Co
12
Y
5
was synthesized using spark plasma sintering at a temperature of 1423 K and applied pressure of 75 MPa. The relative density of the composite following the spark plasma sintering was found to be 99 pct. Indentation fracture toughness measurements in the composite using a Vickers diamond indenter yielded a value of 2.29 MPa m
1/2
which is higher than that of elemental silicon at 1.43 MPa m
1/2
. The second phase provided an average hardness of 14 GPa, while silicon demonstrated hardness of 12 GPa.</description><identifier>ISSN: 1073-5623</identifier><identifier>EISSN: 1543-1940</identifier><identifier>DOI: 10.1007/s11661-022-06697-z</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Alloys ; Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Diamonds ; Engineering ; Fracture toughness ; Hardness ; Indentation ; Materials Science ; Metallic Materials ; Nanotechnology ; Original Research Article ; Particle size ; Plasma sintering ; Powder metallurgy ; Process controls ; Silicon ; Spark plasma sintering ; Specific gravity ; Stress concentration ; Structural Materials ; Surfaces and Interfaces ; Synthesis ; Thin Films</subject><ispartof>Metallurgical and materials transactions. A, Physical metallurgy and materials science, 2022-07, Vol.53 (7), p.2680-2688</ispartof><rights>The Minerals, Metals & Materials Society and ASM International 2022</rights><rights>The Minerals, Metals & Materials Society and ASM International 2022.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-3361faa0cc1324da9979461c458ce41502ff190c16ba748cb18710cc608479493</citedby><cites>FETCH-LOGICAL-c319t-3361faa0cc1324da9979461c458ce41502ff190c16ba748cb18710cc608479493</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11661-022-06697-z$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11661-022-06697-z$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Samantaray, B. K.</creatorcontrib><creatorcontrib>Bakshi, S. R.</creatorcontrib><creatorcontrib>Rajulapati, K. V.</creatorcontrib><creatorcontrib>Gollapudi, S.</creatorcontrib><title>Hardness and Indentation Fracture Toughness in a Novel Silicon Composite Synthesized by Spark Plasma Sintering</title><title>Metallurgical and materials transactions. A, Physical metallurgy and materials science</title><addtitle>Metall Mater Trans A</addtitle><description>A composite of 90 wt pct silicon and 10 wt pct of the multi-component Mo
44
Si
26
Ta
5
Zr
5
Fe
3
Co
12
Y
5
was synthesized using spark plasma sintering at a temperature of 1423 K and applied pressure of 75 MPa. The relative density of the composite following the spark plasma sintering was found to be 99 pct. Indentation fracture toughness measurements in the composite using a Vickers diamond indenter yielded a value of 2.29 MPa m
1/2
which is higher than that of elemental silicon at 1.43 MPa m
1/2
. The second phase provided an average hardness of 14 GPa, while silicon demonstrated hardness of 12 GPa.</description><subject>Alloys</subject><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Diamonds</subject><subject>Engineering</subject><subject>Fracture toughness</subject><subject>Hardness</subject><subject>Indentation</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Nanotechnology</subject><subject>Original Research Article</subject><subject>Particle size</subject><subject>Plasma sintering</subject><subject>Powder metallurgy</subject><subject>Process controls</subject><subject>Silicon</subject><subject>Spark plasma sintering</subject><subject>Specific gravity</subject><subject>Stress concentration</subject><subject>Structural Materials</subject><subject>Surfaces and Interfaces</subject><subject>Synthesis</subject><subject>Thin Films</subject><issn>1073-5623</issn><issn>1543-1940</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp9kEFLwzAUx4MoOKdfwFPAczWvSdPmKMO5wVBh8xyyNN0yu7QmrbB9euMqePP03uH3_z_eD6FbIPdASP4QADiHhKRpQjgXeXI8QyPIGE1AMHIed5LTJOMpvURXIewIISAoHyE3U750JgSsXInnrjSuU51tHJ56pbveG7xq-s32hFiHFX5pvkyNl7a2OlKTZt82wXYGLw-u25pgj6bE6wNetsp_4Ldahb2KtOuMt25zjS4qVQdz8zvH6H36tJrMksXr83zyuEg0BdEllHKolCJaA01ZqYTIBeOgWVZowyAjaVWBIBr4WuWs0Gsocog0JwWLpKBjdDf0tr757E3o5K7pvYsnZcrztGAZQB6pdKC0b0LwppKtt3vlDxKI_PEqB68yepUnr_IYQ3QIhfbnI-P_qv9JfQM_hXvf</recordid><startdate>20220701</startdate><enddate>20220701</enddate><creator>Samantaray, B. 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K. ; Bakshi, S. R. ; Rajulapati, K. V. ; Gollapudi, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-3361faa0cc1324da9979461c458ce41502ff190c16ba748cb18710cc608479493</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Alloys</topic><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Diamonds</topic><topic>Engineering</topic><topic>Fracture toughness</topic><topic>Hardness</topic><topic>Indentation</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Nanotechnology</topic><topic>Original Research Article</topic><topic>Particle size</topic><topic>Plasma sintering</topic><topic>Powder metallurgy</topic><topic>Process controls</topic><topic>Silicon</topic><topic>Spark plasma sintering</topic><topic>Specific gravity</topic><topic>Stress concentration</topic><topic>Structural Materials</topic><topic>Surfaces and Interfaces</topic><topic>Synthesis</topic><topic>Thin Films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Samantaray, B. K.</creatorcontrib><creatorcontrib>Bakshi, S. R.</creatorcontrib><creatorcontrib>Rajulapati, K. 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A, Physical metallurgy and materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Samantaray, B. K.</au><au>Bakshi, S. R.</au><au>Rajulapati, K. V.</au><au>Gollapudi, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Hardness and Indentation Fracture Toughness in a Novel Silicon Composite Synthesized by Spark Plasma Sintering</atitle><jtitle>Metallurgical and materials transactions. A, Physical metallurgy and materials science</jtitle><stitle>Metall Mater Trans A</stitle><date>2022-07-01</date><risdate>2022</risdate><volume>53</volume><issue>7</issue><spage>2680</spage><epage>2688</epage><pages>2680-2688</pages><issn>1073-5623</issn><eissn>1543-1940</eissn><abstract>A composite of 90 wt pct silicon and 10 wt pct of the multi-component Mo
44
Si
26
Ta
5
Zr
5
Fe
3
Co
12
Y
5
was synthesized using spark plasma sintering at a temperature of 1423 K and applied pressure of 75 MPa. The relative density of the composite following the spark plasma sintering was found to be 99 pct. Indentation fracture toughness measurements in the composite using a Vickers diamond indenter yielded a value of 2.29 MPa m
1/2
which is higher than that of elemental silicon at 1.43 MPa m
1/2
. The second phase provided an average hardness of 14 GPa, while silicon demonstrated hardness of 12 GPa.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11661-022-06697-z</doi><tpages>9</tpages></addata></record> |
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| ispartof | Metallurgical and materials transactions. A, Physical metallurgy and materials science, 2022-07, Vol.53 (7), p.2680-2688 |
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| source | SpringerLink Journals - AutoHoldings |
| subjects | Alloys Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Diamonds Engineering Fracture toughness Hardness Indentation Materials Science Metallic Materials Nanotechnology Original Research Article Particle size Plasma sintering Powder metallurgy Process controls Silicon Spark plasma sintering Specific gravity Stress concentration Structural Materials Surfaces and Interfaces Synthesis Thin Films |
| title | Hardness and Indentation Fracture Toughness in a Novel Silicon Composite Synthesized by Spark Plasma Sintering |
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