Conformal coating of powders by magnetron sputtering
Applying a thin film coating to powder under vacuum conditions requires mechanical agitation of the powder to achieve a uniform coating on the surfaces of the powder particles. In this work, we develop a piston-crank mechanism for agitating powder, using mathematic descriptions of system behavior (d...
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Veröffentlicht in: | Surface & coatings technology 2022-04, Vol.436, p.128242, Article 128242 |
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creator | Priedeman, Jonathan L. Thompson, Gregory B. |
description | Applying a thin film coating to powder under vacuum conditions requires mechanical agitation of the powder to achieve a uniform coating on the surfaces of the powder particles. In this work, we develop a piston-crank mechanism for agitating powder, using mathematic descriptions of system behavior (dynamics, forces, and stresses) as well as operational experience to improve the design. The viability of the system is demonstrated by applying tungsten onto spherical copper powder to produce uniform, conformal coatings. The capability of the agitation system is compared to coatings produced using alternative agitation methods, revealing that the piston-crank mechanism produces a larger coating volume per energy input than these other techniques.
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•A piston-crank mechanism can be used to agitate powders in a vacuum.•Process scalability is improved fourfold over previous conformal coating methods.•Mechanical design aspects are specified. |
doi_str_mv | 10.1016/j.surfcoat.2022.128242 |
format | Article |
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•A piston-crank mechanism can be used to agitate powders in a vacuum.•Process scalability is improved fourfold over previous conformal coating methods.•Mechanical design aspects are specified.</description><identifier>ISSN: 0257-8972</identifier><identifier>EISSN: 1879-3347</identifier><identifier>DOI: 10.1016/j.surfcoat.2022.128242</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Agitation ; Coatings ; Design ; Magnetron sputtering ; Powder ; Spherical powders ; Thin film coatings ; Thin films</subject><ispartof>Surface & coatings technology, 2022-04, Vol.436, p.128242, Article 128242</ispartof><rights>2022 Elsevier B.V.</rights><rights>Copyright Elsevier BV Apr 25, 2022</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c340t-e67bc50a846335abcec62f23a514bea807ae97423157f4543b885e390f0309e43</citedby><cites>FETCH-LOGICAL-c340t-e67bc50a846335abcec62f23a514bea807ae97423157f4543b885e390f0309e43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.surfcoat.2022.128242$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3548,27922,27923,45993</link.rule.ids></links><search><creatorcontrib>Priedeman, Jonathan L.</creatorcontrib><creatorcontrib>Thompson, Gregory B.</creatorcontrib><title>Conformal coating of powders by magnetron sputtering</title><title>Surface & coatings technology</title><description>Applying a thin film coating to powder under vacuum conditions requires mechanical agitation of the powder to achieve a uniform coating on the surfaces of the powder particles. In this work, we develop a piston-crank mechanism for agitating powder, using mathematic descriptions of system behavior (dynamics, forces, and stresses) as well as operational experience to improve the design. The viability of the system is demonstrated by applying tungsten onto spherical copper powder to produce uniform, conformal coatings. The capability of the agitation system is compared to coatings produced using alternative agitation methods, revealing that the piston-crank mechanism produces a larger coating volume per energy input than these other techniques.
[Display omitted]
•A piston-crank mechanism can be used to agitate powders in a vacuum.•Process scalability is improved fourfold over previous conformal coating methods.•Mechanical design aspects are specified.</description><subject>Agitation</subject><subject>Coatings</subject><subject>Design</subject><subject>Magnetron sputtering</subject><subject>Powder</subject><subject>Spherical powders</subject><subject>Thin film coatings</subject><subject>Thin films</subject><issn>0257-8972</issn><issn>1879-3347</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNqFkE1LxDAURYMoOI7-BSm4bs1nk-yUQUdhwI2uQ5p5GVpmmpqkyvx7O1TXrt7m3nN5B6FbgiuCSX3fVWmM3gWbK4oprQhVlNMztCBK6pIxLs_RAlMhS6UlvURXKXUYYyI1XyC-Cr0P8WD3xYnQ9rsi-GII31uIqWiOxcHuesgx9EUaxpwhTpFrdOHtPsHN712ij-en99VLuXlbv64eN6VjHOcSatk4ga3iNWPCNg5cTT1lVhDegFVYWtCSU0aE9Fxw1iglgGnsMcMaOFuiu5k7xPA5QsqmC2Psp0lD65orzTVjU6qeUy6GlCJ4M8T2YOPREGxOhkxn_gyZkyEzG5qKD3MRph--WogmuRZ6B9s2gstmG9r_ED-dwXGi</recordid><startdate>20220425</startdate><enddate>20220425</enddate><creator>Priedeman, Jonathan L.</creator><creator>Thompson, Gregory B.</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20220425</creationdate><title>Conformal coating of powders by magnetron sputtering</title><author>Priedeman, Jonathan L. ; Thompson, Gregory B.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c340t-e67bc50a846335abcec62f23a514bea807ae97423157f4543b885e390f0309e43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Agitation</topic><topic>Coatings</topic><topic>Design</topic><topic>Magnetron sputtering</topic><topic>Powder</topic><topic>Spherical powders</topic><topic>Thin film coatings</topic><topic>Thin films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Priedeman, Jonathan L.</creatorcontrib><creatorcontrib>Thompson, Gregory B.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Surface & coatings technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Priedeman, Jonathan L.</au><au>Thompson, Gregory B.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Conformal coating of powders by magnetron sputtering</atitle><jtitle>Surface & coatings technology</jtitle><date>2022-04-25</date><risdate>2022</risdate><volume>436</volume><spage>128242</spage><pages>128242-</pages><artnum>128242</artnum><issn>0257-8972</issn><eissn>1879-3347</eissn><abstract>Applying a thin film coating to powder under vacuum conditions requires mechanical agitation of the powder to achieve a uniform coating on the surfaces of the powder particles. In this work, we develop a piston-crank mechanism for agitating powder, using mathematic descriptions of system behavior (dynamics, forces, and stresses) as well as operational experience to improve the design. The viability of the system is demonstrated by applying tungsten onto spherical copper powder to produce uniform, conformal coatings. The capability of the agitation system is compared to coatings produced using alternative agitation methods, revealing that the piston-crank mechanism produces a larger coating volume per energy input than these other techniques.
[Display omitted]
•A piston-crank mechanism can be used to agitate powders in a vacuum.•Process scalability is improved fourfold over previous conformal coating methods.•Mechanical design aspects are specified.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.surfcoat.2022.128242</doi></addata></record> |
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subjects | Agitation Coatings Design Magnetron sputtering Powder Spherical powders Thin film coatings Thin films |
title | Conformal coating of powders by magnetron sputtering |
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