Development of an analytical method to determine phenolic endocrine disrupting chemicals in sewage and sludge by GC/MS
An analytical method has been developed to determine hisphenoi A and five degradation products of alkyiphenoi ethoxylates in sewage and sludge. The parameters of accelerated solvent extraction （ASE） were optimized. C18 cartridge was used to clean up the sewage and the extract of sludge. The sensitiv...
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| Veröffentlicht in: | Chinese science bulletin 2005-12, Vol.50 (23), p.2681-2687 |
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| creator | Gang, Shen Gang, Yu Zhenxiao, Cai Zulin, Zhang |
| description | An analytical method has been developed to determine hisphenoi A and five degradation products of alkyiphenoi ethoxylates in sewage and sludge. The parameters of accelerated solvent extraction （ASE） were optimized. C18 cartridge was used to clean up the sewage and the extract of sludge. The sensitivity of the mass detector was improved by adjusting the voltage of the lens manually. The instrumental detection limit was 3.2-17.8pg. The method detection limits were 2.5-11.4 ng/L and 0.3-2.1ng/g for sewage and sludge analysis respectively. The recovery and relative standard deviation for sewage analysis were 79.2%-111.4% and 6.9% - 12.6%; for sludge analysis were 68.5% - 114.0% and 8.9%-16.0%. Finally this method was applied to determining the phenolic endocrine disrupting chemicals in sewage and sludge from a sewage treatment plant in Beijing. |
| doi_str_mv | 10.1007/BF02899635 |
| format | Article |
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The parameters of accelerated solvent extraction （ASE） were optimized. C18 cartridge was used to clean up the sewage and the extract of sludge. The sensitivity of the mass detector was improved by adjusting the voltage of the lens manually. The instrumental detection limit was 3.2-17.8pg. The method detection limits were 2.5-11.4 ng/L and 0.3-2.1ng/g for sewage and sludge analysis respectively. The recovery and relative standard deviation for sewage analysis were 79.2%-111.4% and 6.9% - 12.6%; for sludge analysis were 68.5% - 114.0% and 8.9%-16.0%. Finally this method was applied to determining the phenolic endocrine disrupting chemicals in sewage and sludge from a sewage treatment plant in Beijing.</description><identifier>ISSN: 1001-6538</identifier><identifier>ISSN: 2095-9273</identifier><identifier>EISSN: 1861-9541</identifier><identifier>EISSN: 2095-9281</identifier><identifier>DOI: 10.1007/BF02899635</identifier><language>eng</language><publisher>Beijing: Springer Nature B.V</publisher><subject>Alkylphenol ethoxylates ; Analytical methods ; Bisphenol A ; Degradation products ; Detection limits ; Disruption ; Endocrine disruptors ; Phenolic compounds ; Phenols ; Sewage analysis ; Sewage disposal ; Sewage treatment plants ; Sludge ; Solvent extraction ; Wastewater treatment plants ; 双酚A ; 含量测定 ; 水质分析 ; 烷基酚乙氧基化物 ; 致内分泌紊乱化学品 ; 色谱-质谱联用</subject><ispartof>Chinese science bulletin, 2005-12, Vol.50 (23), p.2681-2687</ispartof><rights>Science in China Press 2005.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c1318-85caaff98e5d79a51cdc48fb01e4b0da1e3fb5195b971f19540eaee8e7d41d3a3</citedby><cites>FETCH-LOGICAL-c1318-85caaff98e5d79a51cdc48fb01e4b0da1e3fb5195b971f19540eaee8e7d41d3a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/86894X/86894X.jpg</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Gang, Shen</creatorcontrib><creatorcontrib>Gang, Yu</creatorcontrib><creatorcontrib>Zhenxiao, Cai</creatorcontrib><creatorcontrib>Zulin, Zhang</creatorcontrib><title>Development of an analytical method to determine phenolic endocrine disrupting chemicals in sewage and sludge by GC/MS</title><title>Chinese science bulletin</title><addtitle>Chinese Science Bulletin</addtitle><description>An analytical method has been developed to determine hisphenoi A and five degradation products of alkyiphenoi ethoxylates in sewage and sludge. The parameters of accelerated solvent extraction （ASE） were optimized. C18 cartridge was used to clean up the sewage and the extract of sludge. The sensitivity of the mass detector was improved by adjusting the voltage of the lens manually. The instrumental detection limit was 3.2-17.8pg. The method detection limits were 2.5-11.4 ng/L and 0.3-2.1ng/g for sewage and sludge analysis respectively. The recovery and relative standard deviation for sewage analysis were 79.2%-111.4% and 6.9% - 12.6%; for sludge analysis were 68.5% - 114.0% and 8.9%-16.0%. Finally this method was applied to determining the phenolic endocrine disrupting chemicals in sewage and sludge from a sewage treatment plant in Beijing.</description><subject>Alkylphenol ethoxylates</subject><subject>Analytical methods</subject><subject>Bisphenol A</subject><subject>Degradation products</subject><subject>Detection limits</subject><subject>Disruption</subject><subject>Endocrine disruptors</subject><subject>Phenolic compounds</subject><subject>Phenols</subject><subject>Sewage analysis</subject><subject>Sewage disposal</subject><subject>Sewage treatment plants</subject><subject>Sludge</subject><subject>Solvent extraction</subject><subject>Wastewater treatment plants</subject><subject>双酚A</subject><subject>含量测定</subject><subject>水质分析</subject><subject>烷基酚乙氧基化物</subject><subject>致内分泌紊乱化学品</subject><subject>色谱-质谱联用</subject><issn>1001-6538</issn><issn>2095-9273</issn><issn>1861-9541</issn><issn>2095-9281</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNpFkFFLwzAQx4MoOKcvfoKgb0I1aZo2fdTppjDxQX0uaXJZO9umS9rJvr0ZGwgH97_jd3_uDqFrSu4pIdnD05zEIs9Txk_QhIqURjlP6GnQhNAo5Uycowvv16FiNIsnaPsMW2hs30I3YGuw7ELIZjfUSja4haGyGg8WaxjAtXUHuK-gs02tMHTaKrdv6dq7sR_qboVVBe1-1OO6wx5-5QqCoca-GXWQ5Q4vZg_vn5fozAQIro55ir7nL1-z12j5sXibPS4jFfYTkeBKSmNyAVxnueRUaZUIUxIKSUm0pMBMyWnOyzyjJuSEgAQQkOmEaibZFN0efHtnNyP4oVjb0YUDfRGnaSI4YbEI1N2BUs5678AUvatb6XYFJcX-r8X_XwN8c4Qr26024eiilOrH1A0UMcmyhOQx-wPN1Xci</recordid><startdate>200512</startdate><enddate>200512</enddate><creator>Gang, Shen</creator><creator>Gang, Yu</creator><creator>Zhenxiao, Cai</creator><creator>Zulin, Zhang</creator><general>Springer Nature B.V</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>W92</scope><scope>~WA</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>200512</creationdate><title>Development of an analytical method to determine phenolic endocrine disrupting chemicals in sewage and sludge by GC/MS</title><author>Gang, Shen ; Gang, Yu ; Zhenxiao, Cai ; Zulin, Zhang</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c1318-85caaff98e5d79a51cdc48fb01e4b0da1e3fb5195b971f19540eaee8e7d41d3a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>Alkylphenol ethoxylates</topic><topic>Analytical methods</topic><topic>Bisphenol A</topic><topic>Degradation products</topic><topic>Detection limits</topic><topic>Disruption</topic><topic>Endocrine disruptors</topic><topic>Phenolic compounds</topic><topic>Phenols</topic><topic>Sewage analysis</topic><topic>Sewage disposal</topic><topic>Sewage treatment plants</topic><topic>Sludge</topic><topic>Solvent extraction</topic><topic>Wastewater treatment plants</topic><topic>双酚A</topic><topic>含量测定</topic><topic>水质分析</topic><topic>烷基酚乙氧基化物</topic><topic>致内分泌紊乱化学品</topic><topic>色谱-质谱联用</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gang, Shen</creatorcontrib><creatorcontrib>Gang, Yu</creatorcontrib><creatorcontrib>Zhenxiao, Cai</creatorcontrib><creatorcontrib>Zulin, Zhang</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库-工程技术</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>CrossRef</collection><jtitle>Chinese science bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gang, Shen</au><au>Gang, Yu</au><au>Zhenxiao, Cai</au><au>Zulin, Zhang</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development of an analytical method to determine phenolic endocrine disrupting chemicals in sewage and sludge by GC/MS</atitle><jtitle>Chinese science bulletin</jtitle><addtitle>Chinese Science Bulletin</addtitle><date>2005-12</date><risdate>2005</risdate><volume>50</volume><issue>23</issue><spage>2681</spage><epage>2687</epage><pages>2681-2687</pages><issn>1001-6538</issn><issn>2095-9273</issn><eissn>1861-9541</eissn><eissn>2095-9281</eissn><abstract>An analytical method has been developed to determine hisphenoi A and five degradation products of alkyiphenoi ethoxylates in sewage and sludge. The parameters of accelerated solvent extraction （ASE） were optimized. C18 cartridge was used to clean up the sewage and the extract of sludge. The sensitivity of the mass detector was improved by adjusting the voltage of the lens manually. The instrumental detection limit was 3.2-17.8pg. The method detection limits were 2.5-11.4 ng/L and 0.3-2.1ng/g for sewage and sludge analysis respectively. The recovery and relative standard deviation for sewage analysis were 79.2%-111.4% and 6.9% - 12.6%; for sludge analysis were 68.5% - 114.0% and 8.9%-16.0%. Finally this method was applied to determining the phenolic endocrine disrupting chemicals in sewage and sludge from a sewage treatment plant in Beijing.</abstract><cop>Beijing</cop><pub>Springer Nature B.V</pub><doi>10.1007/BF02899635</doi><tpages>7</tpages></addata></record> |
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| source | Alma/SFX Local Collection |
| subjects | Alkylphenol ethoxylates Analytical methods Bisphenol A Degradation products Detection limits Disruption Endocrine disruptors Phenolic compounds Phenols Sewage analysis Sewage disposal Sewage treatment plants Sludge Solvent extraction Wastewater treatment plants 双酚A 含量测定 水质分析 烷基酚乙氧基化物 致内分泌紊乱化学品 色谱-质谱联用 |
| title | Development of an analytical method to determine phenolic endocrine disrupting chemicals in sewage and sludge by GC/MS |
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