Synthesis of spherical LiNi1/3Co1/3Mn1/3O2 cathode materials for Li-ion batteries
Spherical LiNi1/3Co1/3Mn1/3O2 was successfully prepared by controlled crystallization. The preparation started with the spherical coprecipitate of Ni1/3Co1/3Mn1/3CO3 from NiSO4, CoSO4, MnSO4, NH4HCO3, and NH3·H2O, followed by pyrolysis of Ni1/3Co1/3Mn1/3CO3 at 600°C for 3 h. The X-ray diffraction an...
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| Veröffentlicht in: | Ionics 2006-05, Vol.12 (1), p.77-80 |
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| creator | Li, Jiangang He, Xiangming Fan, Maosong Zhao, Rusong Jiang, Changyin Wan, Chunrong |
| description | Spherical LiNi1/3Co1/3Mn1/3O2 was successfully prepared by controlled crystallization. The preparation started with the spherical coprecipitate of Ni1/3Co1/3Mn1/3CO3 from NiSO4, CoSO4, MnSO4, NH4HCO3, and NH3·H2O, followed by pyrolysis of Ni1/3Co1/3Mn1/3CO3 at 600°C for 3 h. The X-ray diffraction analysis showed that the homogeneous cubic (Ni1/3Co1/3Mn1/3)3O4 was obtained after the pyrolysis. Spherical LiNi1/3Co1/3Mn1/3O2 was obtained by sintering of the mixture of as-obtained (Ni1/3Co1/3Mn1/3)3O4 and LiOH·H2O at 900°C for 6 h in air. As-prepared spherical LiNi1/3Co1/3Mn1/3O2 presented initial discharge capacity of 162.9 mA h g−1 and capacity retention of 98% at 50th cycle. |
| doi_str_mv | 10.1007/s11581-006-0006-6 |
| format | Article |
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The preparation started with the spherical coprecipitate of Ni1/3Co1/3Mn1/3CO3 from NiSO4, CoSO4, MnSO4, NH4HCO3, and NH3·H2O, followed by pyrolysis of Ni1/3Co1/3Mn1/3CO3 at 600°C for 3 h. The X-ray diffraction analysis showed that the homogeneous cubic (Ni1/3Co1/3Mn1/3)3O4 was obtained after the pyrolysis. Spherical LiNi1/3Co1/3Mn1/3O2 was obtained by sintering of the mixture of as-obtained (Ni1/3Co1/3Mn1/3)3O4 and LiOH·H2O at 900°C for 6 h in air. As-prepared spherical LiNi1/3Co1/3Mn1/3O2 presented initial discharge capacity of 162.9 mA h g−1 and capacity retention of 98% at 50th cycle.</description><identifier>ISSN: 0947-7047</identifier><identifier>EISSN: 1862-0760</identifier><identifier>DOI: 10.1007/s11581-006-0006-6</identifier><language>eng</language><publisher>Heidelberg: Springer Nature B.V</publisher><subject>Ammonia ; Crystallization ; Electrode materials ; Lithium ; Lithium-ion batteries ; Pyrolysis ; Rechargeable batteries</subject><ispartof>Ionics, 2006-05, Vol.12 (1), p.77-80</ispartof><rights>Springer-Verlag 2006.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c203t-90f924e5f377866091fe20b91a5569b395cbf299d3925bec09ba80327c3af3783</citedby><cites>FETCH-LOGICAL-c203t-90f924e5f377866091fe20b91a5569b395cbf299d3925bec09ba80327c3af3783</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Li, Jiangang</creatorcontrib><creatorcontrib>He, Xiangming</creatorcontrib><creatorcontrib>Fan, Maosong</creatorcontrib><creatorcontrib>Zhao, Rusong</creatorcontrib><creatorcontrib>Jiang, Changyin</creatorcontrib><creatorcontrib>Wan, Chunrong</creatorcontrib><title>Synthesis of spherical LiNi1/3Co1/3Mn1/3O2 cathode materials for Li-ion batteries</title><title>Ionics</title><description>Spherical LiNi1/3Co1/3Mn1/3O2 was successfully prepared by controlled crystallization. The preparation started with the spherical coprecipitate of Ni1/3Co1/3Mn1/3CO3 from NiSO4, CoSO4, MnSO4, NH4HCO3, and NH3·H2O, followed by pyrolysis of Ni1/3Co1/3Mn1/3CO3 at 600°C for 3 h. The X-ray diffraction analysis showed that the homogeneous cubic (Ni1/3Co1/3Mn1/3)3O4 was obtained after the pyrolysis. Spherical LiNi1/3Co1/3Mn1/3O2 was obtained by sintering of the mixture of as-obtained (Ni1/3Co1/3Mn1/3)3O4 and LiOH·H2O at 900°C for 6 h in air. As-prepared spherical LiNi1/3Co1/3Mn1/3O2 presented initial discharge capacity of 162.9 mA h g−1 and capacity retention of 98% at 50th cycle.</description><subject>Ammonia</subject><subject>Crystallization</subject><subject>Electrode materials</subject><subject>Lithium</subject><subject>Lithium-ion batteries</subject><subject>Pyrolysis</subject><subject>Rechargeable batteries</subject><issn>0947-7047</issn><issn>1862-0760</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNotkMFKAzEQhoMoWKsP4C3gOXaS7CaboyxqhWoR9RyyaUK3tJuabA99e6fUQ_7AzDcz8BFyz-GRA-hZ4bxuOANQ-DDUBZnwRgkGWsElmYCpNNNQ6WtyU8oGEcWFnpDPr-MwrkPpC02Rlv065N67LV30Hz2fyTZhvA8YS0G9G9dpFejOjUi5baExZSRZnwbaufFUDeWWXEXshbv_f0p-Xp6_2zlbLF_f2qcF8wLkyAxEI6pQR6l1oxQYHoOAznBX18p00tS-i8KYlTSi7oIH07kGpNBeOpxp5JQ8nPfuc_o9hDLaTTrkAU9aoVRVIVJJpPiZ8jmVkkO0-9zvXD5aDvZkzp7NWTRiT-askn8_G14x</recordid><startdate>20060501</startdate><enddate>20060501</enddate><creator>Li, Jiangang</creator><creator>He, Xiangming</creator><creator>Fan, Maosong</creator><creator>Zhao, Rusong</creator><creator>Jiang, Changyin</creator><creator>Wan, Chunrong</creator><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20060501</creationdate><title>Synthesis of spherical LiNi1/3Co1/3Mn1/3O2 cathode materials for Li-ion batteries</title><author>Li, Jiangang ; He, Xiangming ; Fan, Maosong ; Zhao, Rusong ; Jiang, Changyin ; Wan, Chunrong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c203t-90f924e5f377866091fe20b91a5569b395cbf299d3925bec09ba80327c3af3783</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Ammonia</topic><topic>Crystallization</topic><topic>Electrode materials</topic><topic>Lithium</topic><topic>Lithium-ion batteries</topic><topic>Pyrolysis</topic><topic>Rechargeable batteries</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, Jiangang</creatorcontrib><creatorcontrib>He, Xiangming</creatorcontrib><creatorcontrib>Fan, Maosong</creatorcontrib><creatorcontrib>Zhao, Rusong</creatorcontrib><creatorcontrib>Jiang, Changyin</creatorcontrib><creatorcontrib>Wan, Chunrong</creatorcontrib><collection>CrossRef</collection><jtitle>Ionics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, Jiangang</au><au>He, Xiangming</au><au>Fan, Maosong</au><au>Zhao, Rusong</au><au>Jiang, Changyin</au><au>Wan, Chunrong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of spherical LiNi1/3Co1/3Mn1/3O2 cathode materials for Li-ion batteries</atitle><jtitle>Ionics</jtitle><date>2006-05-01</date><risdate>2006</risdate><volume>12</volume><issue>1</issue><spage>77</spage><epage>80</epage><pages>77-80</pages><issn>0947-7047</issn><eissn>1862-0760</eissn><abstract>Spherical LiNi1/3Co1/3Mn1/3O2 was successfully prepared by controlled crystallization. The preparation started with the spherical coprecipitate of Ni1/3Co1/3Mn1/3CO3 from NiSO4, CoSO4, MnSO4, NH4HCO3, and NH3·H2O, followed by pyrolysis of Ni1/3Co1/3Mn1/3CO3 at 600°C for 3 h. The X-ray diffraction analysis showed that the homogeneous cubic (Ni1/3Co1/3Mn1/3)3O4 was obtained after the pyrolysis. Spherical LiNi1/3Co1/3Mn1/3O2 was obtained by sintering of the mixture of as-obtained (Ni1/3Co1/3Mn1/3)3O4 and LiOH·H2O at 900°C for 6 h in air. As-prepared spherical LiNi1/3Co1/3Mn1/3O2 presented initial discharge capacity of 162.9 mA h g−1 and capacity retention of 98% at 50th cycle.</abstract><cop>Heidelberg</cop><pub>Springer Nature B.V</pub><doi>10.1007/s11581-006-0006-6</doi><tpages>4</tpages></addata></record> |
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| subjects | Ammonia Crystallization Electrode materials Lithium Lithium-ion batteries Pyrolysis Rechargeable batteries |
| title | Synthesis of spherical LiNi1/3Co1/3Mn1/3O2 cathode materials for Li-ion batteries |
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