Preparation of Nb3Al powder by chemical reaction in molten salts
Nb 3 Al nanoparticles were directly synthesized by metallothermic reduction process in the molten salts with m NbCl 5 – n AlCl 3 powders as raw materials and sodium as reducing reagent. The effects of different feeding material orders, soaking time, Nb content in raw materials, and 3NbCl 5 –AlCl 3 c...
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| Veröffentlicht in: | Rare metals 2022-05, Vol.41 (5), p.1671-1676 |
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| container_issue | 5 |
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| container_title | Rare metals |
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| creator | Wang, Na Huang, Cai-Yun Zhang, Yao Zhu, Hong-Min |
| description | Nb
3
Al nanoparticles were directly synthesized by metallothermic reduction process in the molten salts with
m
NbCl
5
–
n
AlCl
3
powders as raw materials and sodium as reducing reagent. The effects of different feeding material orders, soaking time, Nb content in raw materials, and 3NbCl
5
–AlCl
3
content in molten salts on the obtained Nb
3
Al powder were discussed. The as-prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). It is found that the only phase Nb
3
Al nanoparticles are obtained by controlling the variation of the feeding material orders, soaking time, and Nb content in raw materials. And the morphologies of as-prepared nanoparticles change owning to different 3NbCl
5
–AlCl
3
contents in molten salts. |
| doi_str_mv | 10.1007/s12598-015-0523-4 |
| format | Article |
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3
Al nanoparticles were directly synthesized by metallothermic reduction process in the molten salts with
m
NbCl
5
–
n
AlCl
3
powders as raw materials and sodium as reducing reagent. The effects of different feeding material orders, soaking time, Nb content in raw materials, and 3NbCl
5
–AlCl
3
content in molten salts on the obtained Nb
3
Al powder were discussed. The as-prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). It is found that the only phase Nb
3
Al nanoparticles are obtained by controlling the variation of the feeding material orders, soaking time, and Nb content in raw materials. And the morphologies of as-prepared nanoparticles change owning to different 3NbCl
5
–AlCl
3
contents in molten salts.</description><identifier>ISSN: 1001-0521</identifier><identifier>EISSN: 1867-7185</identifier><identifier>DOI: 10.1007/s12598-015-0523-4</identifier><language>eng</language><publisher>Beijing: Nonferrous Metals Society of China</publisher><subject>Aluminum chloride ; Biomaterials ; Chemical reactions ; Chemical reduction ; Chemistry and Materials Science ; Electron microscopes ; Electron microscopy ; Energy ; Materials Engineering ; Materials Science ; Metallic Materials ; Microscopy ; Molten salts ; Nanoparticles ; Nanoscale Science and Technology ; Niobium ; Physical Chemistry ; Raw materials ; Reagents ; Reduction (metal working)</subject><ispartof>Rare metals, 2022-05, Vol.41 (5), p.1671-1676</ispartof><rights>The Nonferrous Metals Society of China and Springer-Verlag Berlin Heidelberg 2015</rights><rights>The Nonferrous Metals Society of China and Springer-Verlag Berlin Heidelberg 2015.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c386t-eb910d76f35506836f6c15ea366706195a55079cf4e38b341dc4dc7bfe0606e23</citedby><cites>FETCH-LOGICAL-c386t-eb910d76f35506836f6c15ea366706195a55079cf4e38b341dc4dc7bfe0606e23</cites><orcidid>0000-0003-1637-9206</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s12598-015-0523-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s12598-015-0523-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27926,27927,41490,42559,51321</link.rule.ids></links><search><creatorcontrib>Wang, Na</creatorcontrib><creatorcontrib>Huang, Cai-Yun</creatorcontrib><creatorcontrib>Zhang, Yao</creatorcontrib><creatorcontrib>Zhu, Hong-Min</creatorcontrib><title>Preparation of Nb3Al powder by chemical reaction in molten salts</title><title>Rare metals</title><addtitle>Rare Met</addtitle><description>Nb
3
Al nanoparticles were directly synthesized by metallothermic reduction process in the molten salts with
m
NbCl
5
–
n
AlCl
3
powders as raw materials and sodium as reducing reagent. The effects of different feeding material orders, soaking time, Nb content in raw materials, and 3NbCl
5
–AlCl
3
content in molten salts on the obtained Nb
3
Al powder were discussed. The as-prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). It is found that the only phase Nb
3
Al nanoparticles are obtained by controlling the variation of the feeding material orders, soaking time, and Nb content in raw materials. And the morphologies of as-prepared nanoparticles change owning to different 3NbCl
5
–AlCl
3
contents in molten salts.</description><subject>Aluminum chloride</subject><subject>Biomaterials</subject><subject>Chemical reactions</subject><subject>Chemical reduction</subject><subject>Chemistry and Materials Science</subject><subject>Electron microscopes</subject><subject>Electron microscopy</subject><subject>Energy</subject><subject>Materials Engineering</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Microscopy</subject><subject>Molten salts</subject><subject>Nanoparticles</subject><subject>Nanoscale Science and Technology</subject><subject>Niobium</subject><subject>Physical Chemistry</subject><subject>Raw materials</subject><subject>Reagents</subject><subject>Reduction (metal working)</subject><issn>1001-0521</issn><issn>1867-7185</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp1kE1Lw0AQhhdRsFZ_gLcFz6sz2c_cLEWrUNSDnpfNZqMpaRJ3U6T_3tQInjzNMPO8M_AQcolwjQD6JmEmc8MAJQOZcSaOyAyN0kyjkcdjD4CHDZ6Ss5Q2AEIoBTNy-xJD76Ib6q6lXUWfCr5oaN99lSHSYk_9R9jW3jU0Bud_oLql264ZQkuTa4Z0Tk4q16Rw8Vvn5O3-7nX5wNbPq8flYs08N2pgocgRSq0qLiUow1WlPMrguFIaFObSjXOd-0oEbgousPSi9LqoAihQIeNzcjXd7WP3uQtpsJtuF9vxpc2UkEYbjjhSOFE-dinFUNk-1lsX9xbBHkTZSZQdRdmDKCvGTDZl0si27yH-Xf4_9A2oY2lQ</recordid><startdate>20220501</startdate><enddate>20220501</enddate><creator>Wang, Na</creator><creator>Huang, Cai-Yun</creator><creator>Zhang, Yao</creator><creator>Zhu, Hong-Min</creator><general>Nonferrous Metals Society of China</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0003-1637-9206</orcidid></search><sort><creationdate>20220501</creationdate><title>Preparation of Nb3Al powder by chemical reaction in molten salts</title><author>Wang, Na ; Huang, Cai-Yun ; Zhang, Yao ; Zhu, Hong-Min</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c386t-eb910d76f35506836f6c15ea366706195a55079cf4e38b341dc4dc7bfe0606e23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Aluminum chloride</topic><topic>Biomaterials</topic><topic>Chemical reactions</topic><topic>Chemical reduction</topic><topic>Chemistry and Materials Science</topic><topic>Electron microscopes</topic><topic>Electron microscopy</topic><topic>Energy</topic><topic>Materials Engineering</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Microscopy</topic><topic>Molten salts</topic><topic>Nanoparticles</topic><topic>Nanoscale Science and Technology</topic><topic>Niobium</topic><topic>Physical Chemistry</topic><topic>Raw materials</topic><topic>Reagents</topic><topic>Reduction (metal working)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Na</creatorcontrib><creatorcontrib>Huang, Cai-Yun</creatorcontrib><creatorcontrib>Zhang, Yao</creatorcontrib><creatorcontrib>Zhu, Hong-Min</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Rare metals</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Na</au><au>Huang, Cai-Yun</au><au>Zhang, Yao</au><au>Zhu, Hong-Min</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation of Nb3Al powder by chemical reaction in molten salts</atitle><jtitle>Rare metals</jtitle><stitle>Rare Met</stitle><date>2022-05-01</date><risdate>2022</risdate><volume>41</volume><issue>5</issue><spage>1671</spage><epage>1676</epage><pages>1671-1676</pages><issn>1001-0521</issn><eissn>1867-7185</eissn><abstract>Nb
3
Al nanoparticles were directly synthesized by metallothermic reduction process in the molten salts with
m
NbCl
5
–
n
AlCl
3
powders as raw materials and sodium as reducing reagent. The effects of different feeding material orders, soaking time, Nb content in raw materials, and 3NbCl
5
–AlCl
3
content in molten salts on the obtained Nb
3
Al powder were discussed. The as-prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). It is found that the only phase Nb
3
Al nanoparticles are obtained by controlling the variation of the feeding material orders, soaking time, and Nb content in raw materials. And the morphologies of as-prepared nanoparticles change owning to different 3NbCl
5
–AlCl
3
contents in molten salts.</abstract><cop>Beijing</cop><pub>Nonferrous Metals Society of China</pub><doi>10.1007/s12598-015-0523-4</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0003-1637-9206</orcidid></addata></record> |
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| ispartof | Rare metals, 2022-05, Vol.41 (5), p.1671-1676 |
| issn | 1001-0521 1867-7185 |
| language | eng |
| recordid | cdi_proquest_journals_2645878311 |
| source | SpringerNature Journals; Alma/SFX Local Collection |
| subjects | Aluminum chloride Biomaterials Chemical reactions Chemical reduction Chemistry and Materials Science Electron microscopes Electron microscopy Energy Materials Engineering Materials Science Metallic Materials Microscopy Molten salts Nanoparticles Nanoscale Science and Technology Niobium Physical Chemistry Raw materials Reagents Reduction (metal working) |
| title | Preparation of Nb3Al powder by chemical reaction in molten salts |
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