The assessment of honeycomb structure UiO-66 and amino functionalized UiO-66 metal–organic frameworks to modify the morphology and performance of Pebax®1657-based gas separation membranes for CO2 capture applications
A new type of honeycomb structured UiO-66 metal–organic frameworks (MOF) was synthesized and amino functionalized followed by employing them to prepare mixed matrix membranes (MMM). The influences of dimethylformamide (DMF) and H 2 O/ethanol (70/30 wt.%) blend were firstly investigated on morphology...
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| Veröffentlicht in: | Environmental science and pollution research international 2020-11, Vol.27 (32), p.40618-40632 |
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| creator | Sarmadi, Rasoul Salimi, Mahmoud Pirouzfar, Vahid |
| description | A new type of honeycomb structured UiO-66 metal–organic frameworks (MOF) was synthesized and amino functionalized followed by employing them to prepare mixed matrix membranes (MMM). The influences of dimethylformamide (DMF) and H
2
O/ethanol (70/30 wt.%) blend were firstly investigated on morphology, structure, and CO
2
/CH
4
separation efficiency of Pebax®1657 membranes. Based on the transmission electron microscopy (TEM) analysis, the synthesized MOF has 15 nm in diameter. DMF led to the formation of a more crystalline (based on X-ray diffraction (XRD) analysis) and more porous structure. Higher CO
2
permeability and CO
2
/CH
4
selectivity were observed as DMF was employed to fabricate neat membranes. Scanning electron microscopy (SEM) exhibited MOF agglomeration as the UiO-66 was used while the nanoparticle dispersion was enhanced when UiO-66-NH
2
was exploited. Fourier transform infrared spectroscopy (FTIR) confirmed the successful MOF incorporation into the MMMs. Ultimately, the gas separation experiments showed that CO
2
permeability was enhanced compared to the neat membrane by 44.7% and 49.4% as 10 wt.% UiO-66 and UiO-66-NH
2
were used, respectively. Moreover, the Pebax®1657-UiO-66-NH
2
MMMs exhibited 71.7% and 34.5% improvement in selectivity of CO
2
/N
2
and CO
2
/CH
4
, respectively, owing to enhancing CO
2
–OH interactions while the CO
2
/O
2
was declined by 8.8%. |
| doi_str_mv | 10.1007/s11356-020-09927-2 |
| format | Article |
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2
O/ethanol (70/30 wt.%) blend were firstly investigated on morphology, structure, and CO
2
/CH
4
separation efficiency of Pebax®1657 membranes. Based on the transmission electron microscopy (TEM) analysis, the synthesized MOF has 15 nm in diameter. DMF led to the formation of a more crystalline (based on X-ray diffraction (XRD) analysis) and more porous structure. Higher CO
2
permeability and CO
2
/CH
4
selectivity were observed as DMF was employed to fabricate neat membranes. Scanning electron microscopy (SEM) exhibited MOF agglomeration as the UiO-66 was used while the nanoparticle dispersion was enhanced when UiO-66-NH
2
was exploited. Fourier transform infrared spectroscopy (FTIR) confirmed the successful MOF incorporation into the MMMs. Ultimately, the gas separation experiments showed that CO
2
permeability was enhanced compared to the neat membrane by 44.7% and 49.4% as 10 wt.% UiO-66 and UiO-66-NH
2
were used, respectively. Moreover, the Pebax®1657-UiO-66-NH
2
MMMs exhibited 71.7% and 34.5% improvement in selectivity of CO
2
/N
2
and CO
2
/CH
4
, respectively, owing to enhancing CO
2
–OH interactions while the CO
2
/O
2
was declined by 8.8%.</description><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-020-09927-2</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Aquatic Pollution ; Atmospheric Protection/Air Quality Control/Air Pollution ; Carbon dioxide ; Carbon sequestration ; Dimethylformamide ; Earth and Environmental Science ; Ecotoxicology ; Electron microscopy ; Environment ; Environmental Chemistry ; Environmental Health ; Environmental science ; Ethanol ; Fourier analysis ; Fourier transforms ; Gas separation ; Honeycomb structures ; Infrared spectroscopy ; Membrane permeability ; Membranes ; Metal-organic frameworks ; Methane ; Microscopy ; Morphology ; Nanoparticles ; Permeability ; Research Article ; Scanning electron microscopy ; Selectivity ; Synthesis ; Transmission electron microscopy ; Waste Water Technology ; Water Management ; Water Pollution Control ; X-ray diffraction</subject><ispartof>Environmental science and pollution research international, 2020-11, Vol.27 (32), p.40618-40632</ispartof><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020</rights><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3482-c21e5146536f898937ac59d7a6c73713ffa4f6d5545ad944f3d3e4a6768773733</citedby><cites>FETCH-LOGICAL-c3482-c21e5146536f898937ac59d7a6c73713ffa4f6d5545ad944f3d3e4a6768773733</cites><orcidid>0000-0002-8227-8801</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-020-09927-2$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-020-09927-2$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Sarmadi, Rasoul</creatorcontrib><creatorcontrib>Salimi, Mahmoud</creatorcontrib><creatorcontrib>Pirouzfar, Vahid</creatorcontrib><title>The assessment of honeycomb structure UiO-66 and amino functionalized UiO-66 metal–organic frameworks to modify the morphology and performance of Pebax®1657-based gas separation membranes for CO2 capture applications</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><description>A new type of honeycomb structured UiO-66 metal–organic frameworks (MOF) was synthesized and amino functionalized followed by employing them to prepare mixed matrix membranes (MMM). The influences of dimethylformamide (DMF) and H
2
O/ethanol (70/30 wt.%) blend were firstly investigated on morphology, structure, and CO
2
/CH
4
separation efficiency of Pebax®1657 membranes. Based on the transmission electron microscopy (TEM) analysis, the synthesized MOF has 15 nm in diameter. DMF led to the formation of a more crystalline (based on X-ray diffraction (XRD) analysis) and more porous structure. Higher CO
2
permeability and CO
2
/CH
4
selectivity were observed as DMF was employed to fabricate neat membranes. Scanning electron microscopy (SEM) exhibited MOF agglomeration as the UiO-66 was used while the nanoparticle dispersion was enhanced when UiO-66-NH
2
was exploited. Fourier transform infrared spectroscopy (FTIR) confirmed the successful MOF incorporation into the MMMs. Ultimately, the gas separation experiments showed that CO
2
permeability was enhanced compared to the neat membrane by 44.7% and 49.4% as 10 wt.% UiO-66 and UiO-66-NH
2
were used, respectively. Moreover, the Pebax®1657-UiO-66-NH
2
MMMs exhibited 71.7% and 34.5% improvement in selectivity of CO
2
/N
2
and CO
2
/CH
4
, respectively, owing to enhancing CO
2
–OH interactions while the CO
2
/O
2
was declined by 8.8%.</description><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Carbon dioxide</subject><subject>Carbon sequestration</subject><subject>Dimethylformamide</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Electron microscopy</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Environmental science</subject><subject>Ethanol</subject><subject>Fourier analysis</subject><subject>Fourier transforms</subject><subject>Gas separation</subject><subject>Honeycomb structures</subject><subject>Infrared spectroscopy</subject><subject>Membrane permeability</subject><subject>Membranes</subject><subject>Metal-organic frameworks</subject><subject>Methane</subject><subject>Microscopy</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Permeability</subject><subject>Research Article</subject><subject>Scanning electron microscopy</subject><subject>Selectivity</subject><subject>Synthesis</subject><subject>Transmission electron microscopy</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><subject>X-ray diffraction</subject><issn>0944-1344</issn><issn>1614-7499</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kU2O1DAQhSPESNMMc4FZWWJt8F_sZIla_EkjNYuZdVTt2N0ZYju4EkGz4g7cg0NwDXacBHc3iB2rWtT33ivVq6obzp5zxswL5FzWmjLBKGtbYah4VK245ooa1baPqxVrlaJcKnVZPUF8YIUs2Kr6ebd3BBAdYnBxJsmTfYruYFPYEpzzYuclO3I_bKjWBGJPIAwxEb9EOw8pwjh8cf3ffXAzjL--fkt5B3GwxGcI7lPKH5DMiYTUD_5A5pIYUp72aUy7w8lzctmnHCBad7zgvdvC5x_fua4N3QIW_x0gQTdBhmNoyQnbDNEhKTKy3ghiYTodCtM0DvZE4dPqwsOI7vrPvKruX7-6W7-lt5s379Yvb6mVqhHUCu5qrnQttW_appUGbN32BrQ10nDpPSiv-7pWNfTljV720inQRjemAFJeVc_OvlNOHxeHc_eQllxeg53QwjSG14oVSpwpmxNidr6b8hAgHzrOumOJ3bnErlTTnUrsRBHJswgLHHcu_7P-j-o3DaGkeQ</recordid><startdate>20201101</startdate><enddate>20201101</enddate><creator>Sarmadi, 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science</topic><topic>Ethanol</topic><topic>Fourier analysis</topic><topic>Fourier transforms</topic><topic>Gas separation</topic><topic>Honeycomb structures</topic><topic>Infrared spectroscopy</topic><topic>Membrane permeability</topic><topic>Membranes</topic><topic>Metal-organic frameworks</topic><topic>Methane</topic><topic>Microscopy</topic><topic>Morphology</topic><topic>Nanoparticles</topic><topic>Permeability</topic><topic>Research Article</topic><topic>Scanning electron microscopy</topic><topic>Selectivity</topic><topic>Synthesis</topic><topic>Transmission electron microscopy</topic><topic>Waste Water Technology</topic><topic>Water Management</topic><topic>Water Pollution Control</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sarmadi, Rasoul</creatorcontrib><creatorcontrib>Salimi, Mahmoud</creatorcontrib><creatorcontrib>Pirouzfar, 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Res</stitle><date>2020-11-01</date><risdate>2020</risdate><volume>27</volume><issue>32</issue><spage>40618</spage><epage>40632</epage><pages>40618-40632</pages><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>A new type of honeycomb structured UiO-66 metal–organic frameworks (MOF) was synthesized and amino functionalized followed by employing them to prepare mixed matrix membranes (MMM). The influences of dimethylformamide (DMF) and H
2
O/ethanol (70/30 wt.%) blend were firstly investigated on morphology, structure, and CO
2
/CH
4
separation efficiency of Pebax®1657 membranes. Based on the transmission electron microscopy (TEM) analysis, the synthesized MOF has 15 nm in diameter. DMF led to the formation of a more crystalline (based on X-ray diffraction (XRD) analysis) and more porous structure. Higher CO
2
permeability and CO
2
/CH
4
selectivity were observed as DMF was employed to fabricate neat membranes. Scanning electron microscopy (SEM) exhibited MOF agglomeration as the UiO-66 was used while the nanoparticle dispersion was enhanced when UiO-66-NH
2
was exploited. Fourier transform infrared spectroscopy (FTIR) confirmed the successful MOF incorporation into the MMMs. Ultimately, the gas separation experiments showed that CO
2
permeability was enhanced compared to the neat membrane by 44.7% and 49.4% as 10 wt.% UiO-66 and UiO-66-NH
2
were used, respectively. Moreover, the Pebax®1657-UiO-66-NH
2
MMMs exhibited 71.7% and 34.5% improvement in selectivity of CO
2
/N
2
and CO
2
/CH
4
, respectively, owing to enhancing CO
2
–OH interactions while the CO
2
/O
2
was declined by 8.8%.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s11356-020-09927-2</doi><tpages>15</tpages><orcidid>https://orcid.org/0000-0002-8227-8801</orcidid><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0944-1344 |
| ispartof | Environmental science and pollution research international, 2020-11, Vol.27 (32), p.40618-40632 |
| issn | 0944-1344 1614-7499 |
| language | eng |
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| source | SpringerNature Journals |
| subjects | Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Carbon dioxide Carbon sequestration Dimethylformamide Earth and Environmental Science Ecotoxicology Electron microscopy Environment Environmental Chemistry Environmental Health Environmental science Ethanol Fourier analysis Fourier transforms Gas separation Honeycomb structures Infrared spectroscopy Membrane permeability Membranes Metal-organic frameworks Methane Microscopy Morphology Nanoparticles Permeability Research Article Scanning electron microscopy Selectivity Synthesis Transmission electron microscopy Waste Water Technology Water Management Water Pollution Control X-ray diffraction |
| title | The assessment of honeycomb structure UiO-66 and amino functionalized UiO-66 metal–organic frameworks to modify the morphology and performance of Pebax®1657-based gas separation membranes for CO2 capture applications |
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