Influence of Sintering Duration on Crystal Phase and Optical Band Gap of Mn3+ -Doped Willemite-Based Glass-Ceramics
A conventional melt quenching technique was used to successfully fabricate Mn 2 O 3 -doped willemite glass-ceramics (Zn 2 SiO 4 :Mn 3+ ) produced from the ZnO-SLS glasses. The results from XRD revealed that willemite crystallization is improved by increasing the sintering duration. It was revealed t...
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| Veröffentlicht in: | Journal of electronic materials 2022-03, Vol.51 (3), p.1163-1168 |
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| creator | Wei, L. Z. Mun, C. W. Zakaly, H. M. H. Issa, Shams A. M. Zaid, M. H. M. |
| description | A conventional melt quenching technique was used to successfully fabricate Mn
2
O
3
-doped willemite glass-ceramics (Zn
2
SiO
4
:Mn
3+
) produced from the ZnO-SLS glasses. The results from XRD revealed that willemite crystallization is improved by increasing the sintering duration. It was revealed that, as the sintering duration progressed, the phase formation shifted from amorphous to α-Zn
2
SiO
4
crystal. In addition, the structural growth of willemite phases can be seen using FTIR spectroscopy. The results of UV-Vis spectroscopy indicated that the intense absorption occurs in the UV zone, with wavelengths ranging from 250 nm to 400 nm, while the optical band gap showed a decreasing trend from 3.61 eV to 2.52 eV. These results perfectly established that Mn
3+
dopant is potentially beneficial for producing willemite glass-ceramics for optoelectronic applications. |
| doi_str_mv | 10.1007/s11664-021-09378-6 |
| format | Article |
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2
O
3
-doped willemite glass-ceramics (Zn
2
SiO
4
:Mn
3+
) produced from the ZnO-SLS glasses. The results from XRD revealed that willemite crystallization is improved by increasing the sintering duration. It was revealed that, as the sintering duration progressed, the phase formation shifted from amorphous to α-Zn
2
SiO
4
crystal. In addition, the structural growth of willemite phases can be seen using FTIR spectroscopy. The results of UV-Vis spectroscopy indicated that the intense absorption occurs in the UV zone, with wavelengths ranging from 250 nm to 400 nm, while the optical band gap showed a decreasing trend from 3.61 eV to 2.52 eV. These results perfectly established that Mn
3+
dopant is potentially beneficial for producing willemite glass-ceramics for optoelectronic applications.</description><identifier>ISSN: 0361-5235</identifier><identifier>EISSN: 1543-186X</identifier><identifier>DOI: 10.1007/s11664-021-09378-6</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Crystal structure ; Crystallization ; Crystals ; Electronics and Microelectronics ; Energy gap ; Glass ceramics ; Instrumentation ; Materials Science ; Optical and Electronic Materials ; Optoelectronics ; Original Research Article ; Sintering ; Solid State Physics ; Spectrum analysis ; Zinc oxide ; Zinc silicates</subject><ispartof>Journal of electronic materials, 2022-03, Vol.51 (3), p.1163-1168</ispartof><rights>The Minerals, Metals & Materials Society 2021</rights><rights>The Minerals, Metals & Materials Society 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c249t-e2c7994abd1b87090ff2636c3a3ba2b72687fc4d018d0de3ee19e65fd95fd3493</citedby><cites>FETCH-LOGICAL-c249t-e2c7994abd1b87090ff2636c3a3ba2b72687fc4d018d0de3ee19e65fd95fd3493</cites><orcidid>0000-0001-6734-800X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11664-021-09378-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11664-021-09378-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Wei, L. Z.</creatorcontrib><creatorcontrib>Mun, C. W.</creatorcontrib><creatorcontrib>Zakaly, H. M. H.</creatorcontrib><creatorcontrib>Issa, Shams A. M.</creatorcontrib><creatorcontrib>Zaid, M. H. M.</creatorcontrib><title>Influence of Sintering Duration on Crystal Phase and Optical Band Gap of Mn3+ -Doped Willemite-Based Glass-Ceramics</title><title>Journal of electronic materials</title><addtitle>J. Electron. Mater</addtitle><description>A conventional melt quenching technique was used to successfully fabricate Mn
2
O
3
-doped willemite glass-ceramics (Zn
2
SiO
4
:Mn
3+
) produced from the ZnO-SLS glasses. The results from XRD revealed that willemite crystallization is improved by increasing the sintering duration. It was revealed that, as the sintering duration progressed, the phase formation shifted from amorphous to α-Zn
2
SiO
4
crystal. In addition, the structural growth of willemite phases can be seen using FTIR spectroscopy. The results of UV-Vis spectroscopy indicated that the intense absorption occurs in the UV zone, with wavelengths ranging from 250 nm to 400 nm, while the optical band gap showed a decreasing trend from 3.61 eV to 2.52 eV. These results perfectly established that Mn
3+
dopant is potentially beneficial for producing willemite glass-ceramics for optoelectronic applications.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Crystal structure</subject><subject>Crystallization</subject><subject>Crystals</subject><subject>Electronics and Microelectronics</subject><subject>Energy gap</subject><subject>Glass ceramics</subject><subject>Instrumentation</subject><subject>Materials Science</subject><subject>Optical and Electronic Materials</subject><subject>Optoelectronics</subject><subject>Original Research Article</subject><subject>Sintering</subject><subject>Solid State Physics</subject><subject>Spectrum analysis</subject><subject>Zinc oxide</subject><subject>Zinc silicates</subject><issn>0361-5235</issn><issn>1543-186X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp9kMFKxDAURYMoOI7-gKuAS4nmJW3aLp2q48DICCq6C2n7qh06bU3axfy9qRXcCQnhPe65gUPIOfAr4Dy6dgBKBYwLYDyRUczUAZlBGEgGsXo_JDMuFbBQyPCYnDi35RxCiGFG3Kop6wGbHGlb0ueq6dFWzQe9Hazpq7ah_qR273pT06dP45CapqCbrq9yv1mMw9J0I_vYyEvKbtsOC_pW1TXuqh7ZwiM-UhvnWIrW7KrcnZKj0tQOz37fOXm9v3tJH9h6s1ylN2uWiyDpGYo8SpLAZAVkccQTXpZCSZVLIzMjskioOCrzoOAQF7xAiQgJqrAsEn9lkMg5uZh6O9t-Deh6vW0H2_gvtVAiDEBEEPmUmFK5bZ2zWOrOVjtj9xq4HuXqSa72cvWPXK08JCfIdaMutH_V_1DfS1V8RQ</recordid><startdate>20220301</startdate><enddate>20220301</enddate><creator>Wei, L. 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Z. ; Mun, C. W. ; Zakaly, H. M. H. ; Issa, Shams A. M. ; Zaid, M. H. M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c249t-e2c7994abd1b87090ff2636c3a3ba2b72687fc4d018d0de3ee19e65fd95fd3493</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Crystal structure</topic><topic>Crystallization</topic><topic>Crystals</topic><topic>Electronics and Microelectronics</topic><topic>Energy gap</topic><topic>Glass ceramics</topic><topic>Instrumentation</topic><topic>Materials Science</topic><topic>Optical and Electronic Materials</topic><topic>Optoelectronics</topic><topic>Original Research Article</topic><topic>Sintering</topic><topic>Solid State Physics</topic><topic>Spectrum analysis</topic><topic>Zinc oxide</topic><topic>Zinc silicates</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wei, L. Z.</creatorcontrib><creatorcontrib>Mun, C. W.</creatorcontrib><creatorcontrib>Zakaly, H. M. H.</creatorcontrib><creatorcontrib>Issa, Shams A. M.</creatorcontrib><creatorcontrib>Zaid, M. H. 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Z.</au><au>Mun, C. W.</au><au>Zakaly, H. M. H.</au><au>Issa, Shams A. M.</au><au>Zaid, M. H. M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Influence of Sintering Duration on Crystal Phase and Optical Band Gap of Mn3+ -Doped Willemite-Based Glass-Ceramics</atitle><jtitle>Journal of electronic materials</jtitle><stitle>J. Electron. Mater</stitle><date>2022-03-01</date><risdate>2022</risdate><volume>51</volume><issue>3</issue><spage>1163</spage><epage>1168</epage><pages>1163-1168</pages><issn>0361-5235</issn><eissn>1543-186X</eissn><abstract>A conventional melt quenching technique was used to successfully fabricate Mn
2
O
3
-doped willemite glass-ceramics (Zn
2
SiO
4
:Mn
3+
) produced from the ZnO-SLS glasses. The results from XRD revealed that willemite crystallization is improved by increasing the sintering duration. It was revealed that, as the sintering duration progressed, the phase formation shifted from amorphous to α-Zn
2
SiO
4
crystal. In addition, the structural growth of willemite phases can be seen using FTIR spectroscopy. The results of UV-Vis spectroscopy indicated that the intense absorption occurs in the UV zone, with wavelengths ranging from 250 nm to 400 nm, while the optical band gap showed a decreasing trend from 3.61 eV to 2.52 eV. These results perfectly established that Mn
3+
dopant is potentially beneficial for producing willemite glass-ceramics for optoelectronic applications.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11664-021-09378-6</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0001-6734-800X</orcidid></addata></record> |
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| recordid | cdi_proquest_journals_2625412717 |
| source | SpringerNature Journals |
| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science Crystal structure Crystallization Crystals Electronics and Microelectronics Energy gap Glass ceramics Instrumentation Materials Science Optical and Electronic Materials Optoelectronics Original Research Article Sintering Solid State Physics Spectrum analysis Zinc oxide Zinc silicates |
| title | Influence of Sintering Duration on Crystal Phase and Optical Band Gap of Mn3+ -Doped Willemite-Based Glass-Ceramics |
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