Impinging streams application in mass production of rare earth ions doped upconversion luminescence microparticles
Known as one efficient upconversion luminescent material, Rare-earth ions doped natrium yttrium fluoride NaYF 4 :Yb/Re has broad application prospects. However, due to the limitation of the existing preparation methods, it is difficult to realize industrial production. In this paper, the upconversio...
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creator | Li, Ping Zhao, Liuyong Wang, Song Zhang, Xiaohui Jiang, Huaiyuan Liu, Ruizhen Zhao, Nengchuang Cheng, Jian Xu, Caili Zhao, He Lyu, Renliang |
description | Known as one efficient upconversion luminescent material, Rare-earth ions doped natrium yttrium fluoride NaYF
4
:Yb/Re has broad application prospects. However, due to the limitation of the existing preparation methods, it is difficult to realize industrial production. In this paper, the upconversion luminescence microparticles, rare earth ions doped Natrium Yttrium Fluoride NaYF
4
:Yb/Er, were synthesized productively by impinging stream method. Synthesis conditions were optimized as EDTA: Ln to 0.5 and NaF: Ln to 6 (Ln represents the sum of moles of Y, Yb, and Er), reacting temperature and time to 50 °C and 3 h to obtain a high yield of 99.92% and particle with good monodispersity. To get strong upconversion luminescence, the effect of the calcination temperature and the amount of EDTA were investigated. The bright upconversion emissions by excited with laser radiation at 975 nm were found at 510–690 nm. The higher the calcination temperature, the stronger the luminescence and the strongest luminescence occurs when calcined at 600 °C. And the adding of EDTA will decrease the luminescence intensity. However, the sintering of particles at high temperatures and aggregation of particles without EDTA are unfavorable for the application of the products. Based on the above considerations, the optimal calcination temperature was determined at 450 °C, and the ratio of EDTA: Ln is preferred at 0.5. The impinging stream method to prepare upconversion material has the advantages of being simple in the process and equipment, high in output, low in investment, and convenient to be applied and popularized.
Highlights
Mass Production of up-conversion luminescence materials is illustrated.
NaYF
4
:Yb/Er microparticles were synthesized by the novel impinging stream method.
Products with high yield of 99.92% and good mono-dispersity could be obtained at optimal condition.
The hexagonal crystals were obtained by calcinations at 450 °C, and it can emit bright up-conversion emissions of at 510–690 nm. |
doi_str_mv | 10.1007/s10971-021-05675-y |
format | Article |
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4
:Yb/Re has broad application prospects. However, due to the limitation of the existing preparation methods, it is difficult to realize industrial production. In this paper, the upconversion luminescence microparticles, rare earth ions doped Natrium Yttrium Fluoride NaYF
4
:Yb/Er, were synthesized productively by impinging stream method. Synthesis conditions were optimized as EDTA: Ln to 0.5 and NaF: Ln to 6 (Ln represents the sum of moles of Y, Yb, and Er), reacting temperature and time to 50 °C and 3 h to obtain a high yield of 99.92% and particle with good monodispersity. To get strong upconversion luminescence, the effect of the calcination temperature and the amount of EDTA were investigated. The bright upconversion emissions by excited with laser radiation at 975 nm were found at 510–690 nm. The higher the calcination temperature, the stronger the luminescence and the strongest luminescence occurs when calcined at 600 °C. And the adding of EDTA will decrease the luminescence intensity. However, the sintering of particles at high temperatures and aggregation of particles without EDTA are unfavorable for the application of the products. Based on the above considerations, the optimal calcination temperature was determined at 450 °C, and the ratio of EDTA: Ln is preferred at 0.5. The impinging stream method to prepare upconversion material has the advantages of being simple in the process and equipment, high in output, low in investment, and convenient to be applied and popularized.
Highlights
Mass Production of up-conversion luminescence materials is illustrated.
NaYF
4
:Yb/Er microparticles were synthesized by the novel impinging stream method.
Products with high yield of 99.92% and good mono-dispersity could be obtained at optimal condition.
The hexagonal crystals were obtained by calcinations at 450 °C, and it can emit bright up-conversion emissions of at 510–690 nm.</description><identifier>ISSN: 0928-0707</identifier><identifier>EISSN: 1573-4846</identifier><identifier>DOI: 10.1007/s10971-021-05675-y</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Ceramics ; Chemistry and Materials Science ; colloids ; Composites ; Erbium ; etc. ; Ethylenediaminetetraacetic acids ; fibers ; Fluorides ; Glass ; High temperature ; Inorganic Chemistry ; Luminescence ; Mass production ; Materials Science ; Metal ions ; Microparticles ; Nanotechnology ; Natural Materials ; Optical and Electronic Materials ; Original Paper: Nano-structured materials (particles ; Rare earth elements ; Roasting ; Sodium compounds ; Temperature ; Upconversion ; Ytterbium ; Yttrium</subject><ispartof>Journal of sol-gel science and technology, 2022, Vol.101 (1), p.215-226</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021</rights><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-ae5cc77feabfc6c72e1e6c1f95e8fffe4a1a7578315c6fca866c8d0c1ece7dc63</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10971-021-05675-y$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10971-021-05675-y$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Li, Ping</creatorcontrib><creatorcontrib>Zhao, Liuyong</creatorcontrib><creatorcontrib>Wang, Song</creatorcontrib><creatorcontrib>Zhang, Xiaohui</creatorcontrib><creatorcontrib>Jiang, Huaiyuan</creatorcontrib><creatorcontrib>Liu, Ruizhen</creatorcontrib><creatorcontrib>Zhao, Nengchuang</creatorcontrib><creatorcontrib>Cheng, Jian</creatorcontrib><creatorcontrib>Xu, Caili</creatorcontrib><creatorcontrib>Zhao, He</creatorcontrib><creatorcontrib>Lyu, Renliang</creatorcontrib><title>Impinging streams application in mass production of rare earth ions doped upconversion luminescence microparticles</title><title>Journal of sol-gel science and technology</title><addtitle>J Sol-Gel Sci Technol</addtitle><description>Known as one efficient upconversion luminescent material, Rare-earth ions doped natrium yttrium fluoride NaYF
4
:Yb/Re has broad application prospects. However, due to the limitation of the existing preparation methods, it is difficult to realize industrial production. In this paper, the upconversion luminescence microparticles, rare earth ions doped Natrium Yttrium Fluoride NaYF
4
:Yb/Er, were synthesized productively by impinging stream method. Synthesis conditions were optimized as EDTA: Ln to 0.5 and NaF: Ln to 6 (Ln represents the sum of moles of Y, Yb, and Er), reacting temperature and time to 50 °C and 3 h to obtain a high yield of 99.92% and particle with good monodispersity. To get strong upconversion luminescence, the effect of the calcination temperature and the amount of EDTA were investigated. The bright upconversion emissions by excited with laser radiation at 975 nm were found at 510–690 nm. The higher the calcination temperature, the stronger the luminescence and the strongest luminescence occurs when calcined at 600 °C. And the adding of EDTA will decrease the luminescence intensity. However, the sintering of particles at high temperatures and aggregation of particles without EDTA are unfavorable for the application of the products. Based on the above considerations, the optimal calcination temperature was determined at 450 °C, and the ratio of EDTA: Ln is preferred at 0.5. The impinging stream method to prepare upconversion material has the advantages of being simple in the process and equipment, high in output, low in investment, and convenient to be applied and popularized.
Highlights
Mass Production of up-conversion luminescence materials is illustrated.
NaYF
4
:Yb/Er microparticles were synthesized by the novel impinging stream method.
Products with high yield of 99.92% and good mono-dispersity could be obtained at optimal condition.
The hexagonal crystals were obtained by calcinations at 450 °C, and it can emit bright up-conversion emissions of at 510–690 nm.</description><subject>Ceramics</subject><subject>Chemistry and Materials Science</subject><subject>colloids</subject><subject>Composites</subject><subject>Erbium</subject><subject>etc.</subject><subject>Ethylenediaminetetraacetic acids</subject><subject>fibers</subject><subject>Fluorides</subject><subject>Glass</subject><subject>High temperature</subject><subject>Inorganic Chemistry</subject><subject>Luminescence</subject><subject>Mass production</subject><subject>Materials Science</subject><subject>Metal ions</subject><subject>Microparticles</subject><subject>Nanotechnology</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Original Paper: Nano-structured materials (particles</subject><subject>Rare earth elements</subject><subject>Roasting</subject><subject>Sodium compounds</subject><subject>Temperature</subject><subject>Upconversion</subject><subject>Ytterbium</subject><subject>Yttrium</subject><issn>0928-0707</issn><issn>1573-4846</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kE1LxDAQhoMouK7-AU8Bz9WkbZLuURa_YMGLnkOcTtYsbRqTVth_b3YreBMmDAzPOxkeQq45u-WMqbvE2UrxgpX5CalEsT8hCy5UVdRNLU_Jgq3KpmCKqXNykdKOMSZqrhYkvvTB-W0umsaIpk_UhNA5MKMbPHWe9iYlGuLQTnAcDZZGE5GiieMnzZNE2yFgS6cAg__GmA5UN_XOYwL0gLR3EIeQeQcdpktyZk2X8Oq3L8n748Pb-rnYvD69rO83BZSKjYVBAaCURfNhQYIqkaMEblcCG2st1oYbJVRTcQHSgmmkhKZlwBFQtSCrJbmZ9-bjvyZMo94NU_T5S13KshLZW1NnqpypfGJKEa0O0fUm7jVn-uBWz251dquPbvU-h6o5lDLstxj_Vv-T-gGEeoHi</recordid><startdate>2022</startdate><enddate>2022</enddate><creator>Li, Ping</creator><creator>Zhao, Liuyong</creator><creator>Wang, Song</creator><creator>Zhang, Xiaohui</creator><creator>Jiang, Huaiyuan</creator><creator>Liu, Ruizhen</creator><creator>Zhao, Nengchuang</creator><creator>Cheng, Jian</creator><creator>Xu, Caili</creator><creator>Zhao, He</creator><creator>Lyu, Renliang</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope></search><sort><creationdate>2022</creationdate><title>Impinging streams application in mass production of rare earth ions doped upconversion luminescence microparticles</title><author>Li, Ping ; Zhao, Liuyong ; Wang, Song ; Zhang, Xiaohui ; Jiang, Huaiyuan ; Liu, Ruizhen ; Zhao, Nengchuang ; Cheng, Jian ; Xu, Caili ; Zhao, He ; Lyu, Renliang</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-ae5cc77feabfc6c72e1e6c1f95e8fffe4a1a7578315c6fca866c8d0c1ece7dc63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Ceramics</topic><topic>Chemistry and Materials Science</topic><topic>colloids</topic><topic>Composites</topic><topic>Erbium</topic><topic>etc.</topic><topic>Ethylenediaminetetraacetic acids</topic><topic>fibers</topic><topic>Fluorides</topic><topic>Glass</topic><topic>High temperature</topic><topic>Inorganic Chemistry</topic><topic>Luminescence</topic><topic>Mass production</topic><topic>Materials Science</topic><topic>Metal ions</topic><topic>Microparticles</topic><topic>Nanotechnology</topic><topic>Natural Materials</topic><topic>Optical and Electronic Materials</topic><topic>Original Paper: Nano-structured materials (particles</topic><topic>Rare earth elements</topic><topic>Roasting</topic><topic>Sodium compounds</topic><topic>Temperature</topic><topic>Upconversion</topic><topic>Ytterbium</topic><topic>Yttrium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, Ping</creatorcontrib><creatorcontrib>Zhao, Liuyong</creatorcontrib><creatorcontrib>Wang, Song</creatorcontrib><creatorcontrib>Zhang, Xiaohui</creatorcontrib><creatorcontrib>Jiang, Huaiyuan</creatorcontrib><creatorcontrib>Liu, Ruizhen</creatorcontrib><creatorcontrib>Zhao, Nengchuang</creatorcontrib><creatorcontrib>Cheng, Jian</creatorcontrib><creatorcontrib>Xu, Caili</creatorcontrib><creatorcontrib>Zhao, He</creatorcontrib><creatorcontrib>Lyu, Renliang</creatorcontrib><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><jtitle>Journal of sol-gel science and technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, Ping</au><au>Zhao, Liuyong</au><au>Wang, Song</au><au>Zhang, Xiaohui</au><au>Jiang, Huaiyuan</au><au>Liu, Ruizhen</au><au>Zhao, Nengchuang</au><au>Cheng, Jian</au><au>Xu, Caili</au><au>Zhao, He</au><au>Lyu, Renliang</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Impinging streams application in mass production of rare earth ions doped upconversion luminescence microparticles</atitle><jtitle>Journal of sol-gel science and technology</jtitle><stitle>J Sol-Gel Sci Technol</stitle><date>2022</date><risdate>2022</risdate><volume>101</volume><issue>1</issue><spage>215</spage><epage>226</epage><pages>215-226</pages><issn>0928-0707</issn><eissn>1573-4846</eissn><abstract>Known as one efficient upconversion luminescent material, Rare-earth ions doped natrium yttrium fluoride NaYF
4
:Yb/Re has broad application prospects. However, due to the limitation of the existing preparation methods, it is difficult to realize industrial production. In this paper, the upconversion luminescence microparticles, rare earth ions doped Natrium Yttrium Fluoride NaYF
4
:Yb/Er, were synthesized productively by impinging stream method. Synthesis conditions were optimized as EDTA: Ln to 0.5 and NaF: Ln to 6 (Ln represents the sum of moles of Y, Yb, and Er), reacting temperature and time to 50 °C and 3 h to obtain a high yield of 99.92% and particle with good monodispersity. To get strong upconversion luminescence, the effect of the calcination temperature and the amount of EDTA were investigated. The bright upconversion emissions by excited with laser radiation at 975 nm were found at 510–690 nm. The higher the calcination temperature, the stronger the luminescence and the strongest luminescence occurs when calcined at 600 °C. And the adding of EDTA will decrease the luminescence intensity. However, the sintering of particles at high temperatures and aggregation of particles without EDTA are unfavorable for the application of the products. Based on the above considerations, the optimal calcination temperature was determined at 450 °C, and the ratio of EDTA: Ln is preferred at 0.5. The impinging stream method to prepare upconversion material has the advantages of being simple in the process and equipment, high in output, low in investment, and convenient to be applied and popularized.
Highlights
Mass Production of up-conversion luminescence materials is illustrated.
NaYF
4
:Yb/Er microparticles were synthesized by the novel impinging stream method.
Products with high yield of 99.92% and good mono-dispersity could be obtained at optimal condition.
The hexagonal crystals were obtained by calcinations at 450 °C, and it can emit bright up-conversion emissions of at 510–690 nm.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10971-021-05675-y</doi><tpages>12</tpages></addata></record> |
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subjects | Ceramics Chemistry and Materials Science colloids Composites Erbium etc. Ethylenediaminetetraacetic acids fibers Fluorides Glass High temperature Inorganic Chemistry Luminescence Mass production Materials Science Metal ions Microparticles Nanotechnology Natural Materials Optical and Electronic Materials Original Paper: Nano-structured materials (particles Rare earth elements Roasting Sodium compounds Temperature Upconversion Ytterbium Yttrium |
title | Impinging streams application in mass production of rare earth ions doped upconversion luminescence microparticles |
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