Synthesis of graphene-like porous carbon from biomass for electrochemical energy storage applications
Graphene-like porous carbon (GLC) was synthesized from walnut shell (WSh) by carbonization and thermochemical activation process. The obtained samples of graphene-like porous carbon based on walnut shell (GLC-WSh) were characterized by physicochemical analysis in order to optimize the synthesis proc...
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| Veröffentlicht in: | Diamond and related materials 2021-11, Vol.119, p.108560, Article 108560 |
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| creator | Yeleuov, Mukhtar Daulbayev, Chingis Taurbekov, Azamat Abdisattar, Alisher Ebrahim, Rabi Kumekov, Serik Prikhodko, Nikolay Lesbayev, Bakytzhan Batyrzhan, Karakozov |
| description | Graphene-like porous carbon (GLC) was synthesized from walnut shell (WSh) by carbonization and thermochemical activation process. The obtained samples of graphene-like porous carbon based on walnut shell (GLC-WSh) were characterized by physicochemical analysis in order to optimize the synthesis process. The optimum condition of GLC-WSh synthesis was determined to meet the basic requirements for various applications such as an active material for supercapacitors, lithium-ion battery, as energy-intensive additives in order to increase the efficiency of high-energy rocket fuels, and as a membrane for desalination of seawater. The Raman spectra confirmed the presence of few-layer graphene in GLC-WSh with on average number of 5–7 graphene layers. The specific surface area (SSA) was determined using nitrogen adsorption/desorption analysis. The SSA is 2800 m2 g−1 according to Brunauer-Emmett-Teller method. The mass yield of GLC-WSh from the initial mass of the WSh was 21%. The synthesized GLC-WSh powder was applied as an active material for an electrochemical double layer capacitor. Electrochemical characterization showed a high specific capacitance value of 263 F/ g and columbic efficiency of 99.4% at a gravimetric current density of 1000 mA/ g.
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•Synthesis of biowaste derived graphene like porous carbon from walnut shell by simple chemical method•Analysis of supercapacitor properties•Detailed analysis of galvanometric charging-discharging properties |
| doi_str_mv | 10.1016/j.diamond.2021.108560 |
| format | Article |
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•Synthesis of biowaste derived graphene like porous carbon from walnut shell by simple chemical method•Analysis of supercapacitor properties•Detailed analysis of galvanometric charging-discharging properties</description><identifier>ISSN: 0925-9635</identifier><identifier>EISSN: 1879-0062</identifier><identifier>DOI: 10.1016/j.diamond.2021.108560</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Additives ; Biomass energy production ; Biowaste derived ; Carbon ; Desalination ; Electrochemical analysis ; Electrochemical double layer capacitor ; Energy storage ; Few-layer graphene ; Graphene ; Graphene-like porous carbon ; Lithium-ion batteries ; Optimization ; Raman spectra ; Rechargeable batteries ; Rocket propellants ; Seawater ; Synthesis ; Walnut shell ; Walnuts</subject><ispartof>Diamond and related materials, 2021-11, Vol.119, p.108560, Article 108560</ispartof><rights>2021 Elsevier B.V.</rights><rights>Copyright Elsevier BV Nov 2021</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c403t-a2ac8116edd7a6663fec74551c4ce6e534079c4f677052af606b14291420e2383</citedby><cites>FETCH-LOGICAL-c403t-a2ac8116edd7a6663fec74551c4ce6e534079c4f677052af606b14291420e2383</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.diamond.2021.108560$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Yeleuov, Mukhtar</creatorcontrib><creatorcontrib>Daulbayev, Chingis</creatorcontrib><creatorcontrib>Taurbekov, Azamat</creatorcontrib><creatorcontrib>Abdisattar, Alisher</creatorcontrib><creatorcontrib>Ebrahim, Rabi</creatorcontrib><creatorcontrib>Kumekov, Serik</creatorcontrib><creatorcontrib>Prikhodko, Nikolay</creatorcontrib><creatorcontrib>Lesbayev, Bakytzhan</creatorcontrib><creatorcontrib>Batyrzhan, Karakozov</creatorcontrib><title>Synthesis of graphene-like porous carbon from biomass for electrochemical energy storage applications</title><title>Diamond and related materials</title><description>Graphene-like porous carbon (GLC) was synthesized from walnut shell (WSh) by carbonization and thermochemical activation process. The obtained samples of graphene-like porous carbon based on walnut shell (GLC-WSh) were characterized by physicochemical analysis in order to optimize the synthesis process. The optimum condition of GLC-WSh synthesis was determined to meet the basic requirements for various applications such as an active material for supercapacitors, lithium-ion battery, as energy-intensive additives in order to increase the efficiency of high-energy rocket fuels, and as a membrane for desalination of seawater. The Raman spectra confirmed the presence of few-layer graphene in GLC-WSh with on average number of 5–7 graphene layers. The specific surface area (SSA) was determined using nitrogen adsorption/desorption analysis. The SSA is 2800 m2 g−1 according to Brunauer-Emmett-Teller method. The mass yield of GLC-WSh from the initial mass of the WSh was 21%. The synthesized GLC-WSh powder was applied as an active material for an electrochemical double layer capacitor. Electrochemical characterization showed a high specific capacitance value of 263 F/ g and columbic efficiency of 99.4% at a gravimetric current density of 1000 mA/ g.
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•Synthesis of biowaste derived graphene like porous carbon from walnut shell by simple chemical method•Analysis of supercapacitor properties•Detailed analysis of galvanometric charging-discharging properties</description><subject>Additives</subject><subject>Biomass energy production</subject><subject>Biowaste derived</subject><subject>Carbon</subject><subject>Desalination</subject><subject>Electrochemical analysis</subject><subject>Electrochemical double layer capacitor</subject><subject>Energy storage</subject><subject>Few-layer graphene</subject><subject>Graphene</subject><subject>Graphene-like porous carbon</subject><subject>Lithium-ion batteries</subject><subject>Optimization</subject><subject>Raman spectra</subject><subject>Rechargeable batteries</subject><subject>Rocket propellants</subject><subject>Seawater</subject><subject>Synthesis</subject><subject>Walnut shell</subject><subject>Walnuts</subject><issn>0925-9635</issn><issn>1879-0062</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNqFkM1Lw0AQxRdRsFb_BGHBc-p-ZCfJSaT4BQUP6nnZbibtxiQbd1Oh_71b2ruHYeDx3hvmR8gtZwvOONy3i9qZ3g_1QjDBk1YqYGdkxsuiyhgDcU5mrBIqq0CqS3IVY8sYF1XOZwQ_9sO0xegi9Q3dBDNuccCsc99IRx_8LlJrwtoPtAm-p2vnexMjbXyg2KGdgrdb7J01HU25sNnTOPlgNkjNOHZJn5wf4jW5aEwX8ea05-Tr-elz-Zqt3l_elo-rzOZMTpkRxpacA9Z1YQBANmiLXCluc4uASuasqGzeQFEwJUwDDNY8F1UahkKWck7ujr1j8D87jJNu_S4M6aQWwBQAlyCTSx1dNvgYAzZ6DK43Ya850weiutUnovpAVB-JptzDMYfphV-HQUfrcLBYu5BQ6Nq7fxr-AH0igpE</recordid><startdate>202111</startdate><enddate>202111</enddate><creator>Yeleuov, Mukhtar</creator><creator>Daulbayev, Chingis</creator><creator>Taurbekov, Azamat</creator><creator>Abdisattar, Alisher</creator><creator>Ebrahim, Rabi</creator><creator>Kumekov, Serik</creator><creator>Prikhodko, Nikolay</creator><creator>Lesbayev, Bakytzhan</creator><creator>Batyrzhan, Karakozov</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>202111</creationdate><title>Synthesis of graphene-like porous carbon from biomass for electrochemical energy storage applications</title><author>Yeleuov, Mukhtar ; Daulbayev, Chingis ; Taurbekov, Azamat ; Abdisattar, Alisher ; Ebrahim, Rabi ; Kumekov, Serik ; Prikhodko, Nikolay ; Lesbayev, Bakytzhan ; Batyrzhan, Karakozov</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c403t-a2ac8116edd7a6663fec74551c4ce6e534079c4f677052af606b14291420e2383</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Additives</topic><topic>Biomass energy production</topic><topic>Biowaste derived</topic><topic>Carbon</topic><topic>Desalination</topic><topic>Electrochemical analysis</topic><topic>Electrochemical double layer capacitor</topic><topic>Energy storage</topic><topic>Few-layer graphene</topic><topic>Graphene</topic><topic>Graphene-like porous carbon</topic><topic>Lithium-ion batteries</topic><topic>Optimization</topic><topic>Raman spectra</topic><topic>Rechargeable batteries</topic><topic>Rocket propellants</topic><topic>Seawater</topic><topic>Synthesis</topic><topic>Walnut shell</topic><topic>Walnuts</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yeleuov, Mukhtar</creatorcontrib><creatorcontrib>Daulbayev, Chingis</creatorcontrib><creatorcontrib>Taurbekov, Azamat</creatorcontrib><creatorcontrib>Abdisattar, Alisher</creatorcontrib><creatorcontrib>Ebrahim, Rabi</creatorcontrib><creatorcontrib>Kumekov, Serik</creatorcontrib><creatorcontrib>Prikhodko, Nikolay</creatorcontrib><creatorcontrib>Lesbayev, Bakytzhan</creatorcontrib><creatorcontrib>Batyrzhan, Karakozov</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Diamond and related materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yeleuov, Mukhtar</au><au>Daulbayev, Chingis</au><au>Taurbekov, Azamat</au><au>Abdisattar, Alisher</au><au>Ebrahim, Rabi</au><au>Kumekov, Serik</au><au>Prikhodko, Nikolay</au><au>Lesbayev, Bakytzhan</au><au>Batyrzhan, Karakozov</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of graphene-like porous carbon from biomass for electrochemical energy storage applications</atitle><jtitle>Diamond and related materials</jtitle><date>2021-11</date><risdate>2021</risdate><volume>119</volume><spage>108560</spage><pages>108560-</pages><artnum>108560</artnum><issn>0925-9635</issn><eissn>1879-0062</eissn><abstract>Graphene-like porous carbon (GLC) was synthesized from walnut shell (WSh) by carbonization and thermochemical activation process. The obtained samples of graphene-like porous carbon based on walnut shell (GLC-WSh) were characterized by physicochemical analysis in order to optimize the synthesis process. The optimum condition of GLC-WSh synthesis was determined to meet the basic requirements for various applications such as an active material for supercapacitors, lithium-ion battery, as energy-intensive additives in order to increase the efficiency of high-energy rocket fuels, and as a membrane for desalination of seawater. The Raman spectra confirmed the presence of few-layer graphene in GLC-WSh with on average number of 5–7 graphene layers. The specific surface area (SSA) was determined using nitrogen adsorption/desorption analysis. The SSA is 2800 m2 g−1 according to Brunauer-Emmett-Teller method. The mass yield of GLC-WSh from the initial mass of the WSh was 21%. The synthesized GLC-WSh powder was applied as an active material for an electrochemical double layer capacitor. Electrochemical characterization showed a high specific capacitance value of 263 F/ g and columbic efficiency of 99.4% at a gravimetric current density of 1000 mA/ g.
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•Synthesis of biowaste derived graphene like porous carbon from walnut shell by simple chemical method•Analysis of supercapacitor properties•Detailed analysis of galvanometric charging-discharging properties</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.diamond.2021.108560</doi></addata></record> |
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| subjects | Additives Biomass energy production Biowaste derived Carbon Desalination Electrochemical analysis Electrochemical double layer capacitor Energy storage Few-layer graphene Graphene Graphene-like porous carbon Lithium-ion batteries Optimization Raman spectra Rechargeable batteries Rocket propellants Seawater Synthesis Walnut shell Walnuts |
| title | Synthesis of graphene-like porous carbon from biomass for electrochemical energy storage applications |
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