Influence of process parameters in additive manufacturing of highly reinforced 316L / SiCp composites

[Display omitted] Highly reinforced 316 L / SiCp metal matrix composites (MMC) walls have been additively manufactured by Direct Laser Deposition (DLD) using mixtures with different percentages of 316 L stainless steel powder and SiC particles (SiCp). The effect of the percentages of SiCp of up to 8...

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Veröffentlicht in:Journal of materials processing technology 2022-01, Vol.299, p.117325, Article 117325
Hauptverfasser: Riquelme, A., Sánchez de Rojas Candela, C., Rodrigo, P., Rams, J.
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Sánchez de Rojas Candela, C.
Rodrigo, P.
Rams, J.
description [Display omitted] Highly reinforced 316 L / SiCp metal matrix composites (MMC) walls have been additively manufactured by Direct Laser Deposition (DLD) using mixtures with different percentages of 316 L stainless steel powder and SiC particles (SiCp). The effect of the percentages of SiCp of up to 80 wt.% and DLD conditions on the geometry, microstructure, and hardness of the fabricated structures have been analyzed. SiC particles react with the molten 316 L steel and chromium and iron carbides are formed, and also graphite flakes and nodules are formed in the matrix. This reaction is also responsible for the dilution of the SiCp, which lose their initial shape and size. The incorporation of higher percentages of SiCp reduces the degradation of the particles as the matrix saturates in Si and C, and also enhances the size of the graphite precipitated phases. The different phases formed help to increase the hardness of the composites, and a maximum value of 1085 HV0.1 was obtained for 40 vol.% of SiCp. Increasing further the amount of SiCp reduced the hardness to values of ∼890 HV0.1 as the matrix is saturated in carbides and bigger and more brittle graphite precipitates are formed. The characteristics of the manufactured samples for the different reinforcement percentages used and for the different manufacturing conditions have been analyzed. From this study, the DLD processing maps for the 316 L/SiC MMC metal matrix composites with different content of reinforcement have been developed, and the optimal values of laser power, scanning speed, and layer height have been determined, and it has been observed that the optimum fabrication conditions displace to lower scanning speed for higher SiCp contents in the 316 L matrix. Showing that it is possible to manufacture cermets based on steel with lower density and greater hardness than the steel used.
doi_str_mv 10.1016/j.jmatprotec.2021.117325
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The effect of the percentages of SiCp of up to 80 wt.% and DLD conditions on the geometry, microstructure, and hardness of the fabricated structures have been analyzed. SiC particles react with the molten 316 L steel and chromium and iron carbides are formed, and also graphite flakes and nodules are formed in the matrix. This reaction is also responsible for the dilution of the SiCp, which lose their initial shape and size. The incorporation of higher percentages of SiCp reduces the degradation of the particles as the matrix saturates in Si and C, and also enhances the size of the graphite precipitated phases. The different phases formed help to increase the hardness of the composites, and a maximum value of 1085 HV0.1 was obtained for 40 vol.% of SiCp. Increasing further the amount of SiCp reduced the hardness to values of ∼890 HV0.1 as the matrix is saturated in carbides and bigger and more brittle graphite precipitates are formed. The characteristics of the manufactured samples for the different reinforcement percentages used and for the different manufacturing conditions have been analyzed. From this study, the DLD processing maps for the 316 L/SiC MMC metal matrix composites with different content of reinforcement have been developed, and the optimal values of laser power, scanning speed, and layer height have been determined, and it has been observed that the optimum fabrication conditions displace to lower scanning speed for higher SiCp contents in the 316 L matrix. 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The effect of the percentages of SiCp of up to 80 wt.% and DLD conditions on the geometry, microstructure, and hardness of the fabricated structures have been analyzed. SiC particles react with the molten 316 L steel and chromium and iron carbides are formed, and also graphite flakes and nodules are formed in the matrix. This reaction is also responsible for the dilution of the SiCp, which lose their initial shape and size. The incorporation of higher percentages of SiCp reduces the degradation of the particles as the matrix saturates in Si and C, and also enhances the size of the graphite precipitated phases. The different phases formed help to increase the hardness of the composites, and a maximum value of 1085 HV0.1 was obtained for 40 vol.% of SiCp. Increasing further the amount of SiCp reduced the hardness to values of ∼890 HV0.1 as the matrix is saturated in carbides and bigger and more brittle graphite precipitates are formed. The characteristics of the manufactured samples for the different reinforcement percentages used and for the different manufacturing conditions have been analyzed. From this study, the DLD processing maps for the 316 L/SiC MMC metal matrix composites with different content of reinforcement have been developed, and the optimal values of laser power, scanning speed, and layer height have been determined, and it has been observed that the optimum fabrication conditions displace to lower scanning speed for higher SiCp contents in the 316 L matrix. Showing that it is possible to manufacture cermets based on steel with lower density and greater hardness than the steel used.</description><subject>Additive manufacturing</subject><subject>Austenitic stainless steels</subject><subject>Cermets</subject><subject>Chromium</subject><subject>Dilution</subject><subject>Direct laser deposition</subject><subject>Fe/SiC</subject><subject>Graphite</subject><subject>Hardness</subject><subject>Iron carbides</subject><subject>Laser deposition</subject><subject>Manufacturing</subject><subject>Metal matrix composites</subject><subject>Nodular graphitic structure</subject><subject>Optimization</subject><subject>Particulate composites</subject><subject>Precipitates</subject><subject>Process mapping</subject><subject>Process parameters</subject><subject>Scanning</subject><subject>Silicon carbide</subject><issn>0924-0136</issn><issn>1873-4774</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNqFkEtPwzAQhC0EEqXwHyxxTvDaaR5HqHhUqsQBOFuuvW4dNQ9sp1L_PYmCxJHTHnZmducjhAJLgUH-UKd1o2Lvu4g65YxDClAIvrogCygLkWRFkV2SBat4ljAQ-TW5CaFmDApWlguCm9YeB2w10s7SMUZjCLRXXjUY0QfqWqqMcdGdkDaqHazScfCu3U_6g9sfjmfq0bW28xoNFZBv6QP9cOue6q7pu-AihltyZdUx4N3vXJKvl-fP9VuyfX_drB-3iRZZHhPMBRewQ8Wt0OOvOyG0YaYyIFaFHZeGlTxjAFYXiBpYBWCs5laVJaKpxJLcz7ljke8BQ5R1N_h2PCl5zpjIKs7zUVXOKu27EDxa2XvXKH-WwOQEVdbyD6qcoMoZ6mh9mq04tjg59DJoN9EzzqOO0nTu_5Af4n6GDw</recordid><startdate>202201</startdate><enddate>202201</enddate><creator>Riquelme, A.</creator><creator>Sánchez de Rojas Candela, C.</creator><creator>Rodrigo, P.</creator><creator>Rams, J.</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>H8D</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>202201</creationdate><title>Influence of process parameters in additive manufacturing of highly reinforced 316L / SiCp composites</title><author>Riquelme, A. ; Sánchez de Rojas Candela, C. ; Rodrigo, P. ; Rams, J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c346t-e63231bea2f3c136b33cd0d9d1357f632d0824011fc7eec10911dfc2fa88eed93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Additive manufacturing</topic><topic>Austenitic stainless steels</topic><topic>Cermets</topic><topic>Chromium</topic><topic>Dilution</topic><topic>Direct laser deposition</topic><topic>Fe/SiC</topic><topic>Graphite</topic><topic>Hardness</topic><topic>Iron carbides</topic><topic>Laser deposition</topic><topic>Manufacturing</topic><topic>Metal matrix composites</topic><topic>Nodular graphitic structure</topic><topic>Optimization</topic><topic>Particulate composites</topic><topic>Precipitates</topic><topic>Process mapping</topic><topic>Process parameters</topic><topic>Scanning</topic><topic>Silicon carbide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Riquelme, A.</creatorcontrib><creatorcontrib>Sánchez de Rojas Candela, C.</creatorcontrib><creatorcontrib>Rodrigo, P.</creatorcontrib><creatorcontrib>Rams, J.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of materials processing technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Riquelme, A.</au><au>Sánchez de Rojas Candela, C.</au><au>Rodrigo, P.</au><au>Rams, J.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Influence of process parameters in additive manufacturing of highly reinforced 316L / SiCp composites</atitle><jtitle>Journal of materials processing technology</jtitle><date>2022-01</date><risdate>2022</risdate><volume>299</volume><spage>117325</spage><pages>117325-</pages><artnum>117325</artnum><issn>0924-0136</issn><eissn>1873-4774</eissn><abstract>[Display omitted] Highly reinforced 316 L / SiCp metal matrix composites (MMC) walls have been additively manufactured by Direct Laser Deposition (DLD) using mixtures with different percentages of 316 L stainless steel powder and SiC particles (SiCp). The effect of the percentages of SiCp of up to 80 wt.% and DLD conditions on the geometry, microstructure, and hardness of the fabricated structures have been analyzed. SiC particles react with the molten 316 L steel and chromium and iron carbides are formed, and also graphite flakes and nodules are formed in the matrix. This reaction is also responsible for the dilution of the SiCp, which lose their initial shape and size. The incorporation of higher percentages of SiCp reduces the degradation of the particles as the matrix saturates in Si and C, and also enhances the size of the graphite precipitated phases. The different phases formed help to increase the hardness of the composites, and a maximum value of 1085 HV0.1 was obtained for 40 vol.% of SiCp. Increasing further the amount of SiCp reduced the hardness to values of ∼890 HV0.1 as the matrix is saturated in carbides and bigger and more brittle graphite precipitates are formed. The characteristics of the manufactured samples for the different reinforcement percentages used and for the different manufacturing conditions have been analyzed. From this study, the DLD processing maps for the 316 L/SiC MMC metal matrix composites with different content of reinforcement have been developed, and the optimal values of laser power, scanning speed, and layer height have been determined, and it has been observed that the optimum fabrication conditions displace to lower scanning speed for higher SiCp contents in the 316 L matrix. Showing that it is possible to manufacture cermets based on steel with lower density and greater hardness than the steel used.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jmatprotec.2021.117325</doi></addata></record>
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subjects Additive manufacturing
Austenitic stainless steels
Cermets
Chromium
Dilution
Direct laser deposition
Fe/SiC
Graphite
Hardness
Iron carbides
Laser deposition
Manufacturing
Metal matrix composites
Nodular graphitic structure
Optimization
Particulate composites
Precipitates
Process mapping
Process parameters
Scanning
Silicon carbide
title Influence of process parameters in additive manufacturing of highly reinforced 316L / SiCp composites
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