Zinc Complex with Tridentate ONO Schiff base Ligand: the Characterization and Nanostructure Thereof
A new Zn(II) coordination complex based on the tridentate ONO Schiff base 2-(((2-methoxyphenyl)imino)methyl)phenolate ligand was synthesized and characterized structurally by using FT-IR, 1 H NMR, 13 C{ 1 H}NMR, UV−Vis and photoluminescence spectroscopies, elemental analysis and single crystal X-ray...
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| Veröffentlicht in: | Russian journal of coordination chemistry 2021-11, Vol.47 (11), p.780-789 |
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| container_title | Russian journal of coordination chemistry |
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| creator | Saber-Tehrani, M. |
| description | A new Zn(II) coordination complex based on the tridentate ONO Schiff base 2-(((2-methoxyphenyl)imino)methyl)phenolate ligand was synthesized and characterized structurally by using FT-IR,
1
H NMR,
13
C{
1
H}NMR, UV−Vis and photoluminescence spectroscopies, elemental analysis and single crystal X-ray crystallography (CIF file CCDC no. 2027332). The molecular structure as well as its supramolecular features was studied using structural, Hirshfeld surface analyses as well as computational studies. The supramolecular arrangement of this coordination complex is directed by a series of hydrogen bonding interactions, including O−H···O, C−H···Br and C−H···π. The C−H···π energies in this compound calculated to be in the range of 5.79–7.99 Å. The compound is also successfully synthesized in three different concentrations by ultrasonic irradiation. The product was characterized by different techniques and the morphology was analyzed using field-emission scanning electron microscopy. The comparison between samples synthesized using ultrasonic irradiation demonstrated that lower concentrations of initial reagents decreased plate size and increased the homogenization of particle size distribution. |
| doi_str_mv | 10.1134/S107032842111004X |
| format | Article |
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1
H NMR,
13
C{
1
H}NMR, UV−Vis and photoluminescence spectroscopies, elemental analysis and single crystal X-ray crystallography (CIF file CCDC no. 2027332). The molecular structure as well as its supramolecular features was studied using structural, Hirshfeld surface analyses as well as computational studies. The supramolecular arrangement of this coordination complex is directed by a series of hydrogen bonding interactions, including O−H···O, C−H···Br and C−H···π. The C−H···π energies in this compound calculated to be in the range of 5.79–7.99 Å. The compound is also successfully synthesized in three different concentrations by ultrasonic irradiation. The product was characterized by different techniques and the morphology was analyzed using field-emission scanning electron microscopy. The comparison between samples synthesized using ultrasonic irradiation demonstrated that lower concentrations of initial reagents decreased plate size and increased the homogenization of particle size distribution.</description><identifier>ISSN: 1070-3284</identifier><identifier>EISSN: 1608-3318</identifier><identifier>DOI: 10.1134/S107032842111004X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Chemical analysis ; Chemistry ; Chemistry and Materials Science ; Coordination compounds ; Crystal structure ; Crystallography ; Emission analysis ; Hydrogen bonding ; Imines ; Inorganic Chemistry ; Irradiation ; Ligands ; Molecular structure ; Morphology ; NMR ; Nuclear magnetic resonance ; Particle size distribution ; Photoluminescence ; Physical Chemistry ; Reagents ; Single crystals ; Synthesis ; Zinc compounds</subject><ispartof>Russian journal of coordination chemistry, 2021-11, Vol.47 (11), p.780-789</ispartof><rights>Pleiades Publishing, Ltd. 2021. ISSN 1070-3284, Russian Journal of Coordination Chemistry, 2021, Vol. 47, No. 11, pp. 780–789. © Pleiades Publishing, Ltd., 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c246t-131d4cbec190b32448f3ffc3bfb18683c08b7848d1fa7bbb850706d242352a9a3</citedby><cites>FETCH-LOGICAL-c246t-131d4cbec190b32448f3ffc3bfb18683c08b7848d1fa7bbb850706d242352a9a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S107032842111004X$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S107032842111004X$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Saber-Tehrani, M.</creatorcontrib><title>Zinc Complex with Tridentate ONO Schiff base Ligand: the Characterization and Nanostructure Thereof</title><title>Russian journal of coordination chemistry</title><addtitle>Russ J Coord Chem</addtitle><description>A new Zn(II) coordination complex based on the tridentate ONO Schiff base 2-(((2-methoxyphenyl)imino)methyl)phenolate ligand was synthesized and characterized structurally by using FT-IR,
1
H NMR,
13
C{
1
H}NMR, UV−Vis and photoluminescence spectroscopies, elemental analysis and single crystal X-ray crystallography (CIF file CCDC no. 2027332). The molecular structure as well as its supramolecular features was studied using structural, Hirshfeld surface analyses as well as computational studies. The supramolecular arrangement of this coordination complex is directed by a series of hydrogen bonding interactions, including O−H···O, C−H···Br and C−H···π. The C−H···π energies in this compound calculated to be in the range of 5.79–7.99 Å. The compound is also successfully synthesized in three different concentrations by ultrasonic irradiation. The product was characterized by different techniques and the morphology was analyzed using field-emission scanning electron microscopy. The comparison between samples synthesized using ultrasonic irradiation demonstrated that lower concentrations of initial reagents decreased plate size and increased the homogenization of particle size distribution.</description><subject>Chemical analysis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Coordination compounds</subject><subject>Crystal structure</subject><subject>Crystallography</subject><subject>Emission analysis</subject><subject>Hydrogen bonding</subject><subject>Imines</subject><subject>Inorganic Chemistry</subject><subject>Irradiation</subject><subject>Ligands</subject><subject>Molecular structure</subject><subject>Morphology</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Particle size distribution</subject><subject>Photoluminescence</subject><subject>Physical Chemistry</subject><subject>Reagents</subject><subject>Single crystals</subject><subject>Synthesis</subject><subject>Zinc compounds</subject><issn>1070-3284</issn><issn>1608-3318</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kEtLAzEUhYMoWKs_wF3A9WhukpnJuJPBFxS7aAVxMySZpJPSztQkxcevN6WCC3F1L5zvnMs9CJ0DuQRg_GoGpCSMCk4BgBD-coBGUBCRMQbiMO1Jznb6MToJYUlIgvJqhPSr6zWuh_VmZT7wu4sdnnvXmj7KaPD0aYpnunPWYiWDwRO3kH17jWNncN1JL3U03n3J6IYeJwU_yX4I0W913HqD553xZrCn6MjKVTBnP3OMnu9u5_VDNpneP9Y3k0xTXsQMGLRcK6OhIopRzoVl1mqmrAJRCKaJUKXgogUrS6WUyNNPRUs5ZTmVlWRjdLHP3fjhbWtCbJbD1vfpZEPzqhSM5kWVKNhT2g8heGObjXdr6T8bIM2uy-ZPl8lD956Q2H5h_G_y_6ZvKJZ1sg</recordid><startdate>20211101</startdate><enddate>20211101</enddate><creator>Saber-Tehrani, M.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20211101</creationdate><title>Zinc Complex with Tridentate ONO Schiff base Ligand: the Characterization and Nanostructure Thereof</title><author>Saber-Tehrani, M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c246t-131d4cbec190b32448f3ffc3bfb18683c08b7848d1fa7bbb850706d242352a9a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Chemical analysis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Coordination compounds</topic><topic>Crystal structure</topic><topic>Crystallography</topic><topic>Emission analysis</topic><topic>Hydrogen bonding</topic><topic>Imines</topic><topic>Inorganic Chemistry</topic><topic>Irradiation</topic><topic>Ligands</topic><topic>Molecular structure</topic><topic>Morphology</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Particle size distribution</topic><topic>Photoluminescence</topic><topic>Physical Chemistry</topic><topic>Reagents</topic><topic>Single crystals</topic><topic>Synthesis</topic><topic>Zinc compounds</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Saber-Tehrani, M.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of coordination chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Saber-Tehrani, M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Zinc Complex with Tridentate ONO Schiff base Ligand: the Characterization and Nanostructure Thereof</atitle><jtitle>Russian journal of coordination chemistry</jtitle><stitle>Russ J Coord Chem</stitle><date>2021-11-01</date><risdate>2021</risdate><volume>47</volume><issue>11</issue><spage>780</spage><epage>789</epage><pages>780-789</pages><issn>1070-3284</issn><eissn>1608-3318</eissn><abstract>A new Zn(II) coordination complex based on the tridentate ONO Schiff base 2-(((2-methoxyphenyl)imino)methyl)phenolate ligand was synthesized and characterized structurally by using FT-IR,
1
H NMR,
13
C{
1
H}NMR, UV−Vis and photoluminescence spectroscopies, elemental analysis and single crystal X-ray crystallography (CIF file CCDC no. 2027332). The molecular structure as well as its supramolecular features was studied using structural, Hirshfeld surface analyses as well as computational studies. The supramolecular arrangement of this coordination complex is directed by a series of hydrogen bonding interactions, including O−H···O, C−H···Br and C−H···π. The C−H···π energies in this compound calculated to be in the range of 5.79–7.99 Å. The compound is also successfully synthesized in three different concentrations by ultrasonic irradiation. The product was characterized by different techniques and the morphology was analyzed using field-emission scanning electron microscopy. The comparison between samples synthesized using ultrasonic irradiation demonstrated that lower concentrations of initial reagents decreased plate size and increased the homogenization of particle size distribution.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S107032842111004X</doi><tpages>10</tpages></addata></record> |
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| language | eng |
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| source | SpringerLink Journals - AutoHoldings |
| subjects | Chemical analysis Chemistry Chemistry and Materials Science Coordination compounds Crystal structure Crystallography Emission analysis Hydrogen bonding Imines Inorganic Chemistry Irradiation Ligands Molecular structure Morphology NMR Nuclear magnetic resonance Particle size distribution Photoluminescence Physical Chemistry Reagents Single crystals Synthesis Zinc compounds |
| title | Zinc Complex with Tridentate ONO Schiff base Ligand: the Characterization and Nanostructure Thereof |
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