Structural characterization of nickel and zinc aluminate prepared by sol-gel technique
This work concerned on nanocrystalline NiAl2O4 and ZnAl2O4 having spinel structure prepared by Sol–gel technique. The structural and characterization properties for the obtained samples were examined using different measurements such as X-ray diffraction (XRD), Fourier transform infrared spectroscop...
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| creator | Abdulmajeed, Inaam M. Mahdi, Dunia Kamel Ibraheem, Suha H. |
| description | This work concerned on nanocrystalline NiAl2O4 and ZnAl2O4 having spinel structure prepared by Sol–gel technique. The structural and characterization properties for the obtained samples were examined using different measurements such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), finally, Field emission scanning electron microscope (FESEM). The Spinel-type for two prepared compound (NiAl2O4) and (ZnAl2O4) at different calcination temperature examined by XRD. Williamson-Hall Methods used to estimate crystallite size, Average distribution crystallite size of two compound were, 34.2 nm for NiAl2O4 and32.6 for ZnAl2O4, the increase in crystallite size affecting by increasing in calcination temperature for both compounds. |
| doi_str_mv | 10.1063/5.0066247 |
| format | Conference Proceeding |
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Al ; Wasfi, Ahmed S. ; Majeed, Sadeer M. ; Ahmed, Duha S.</contributor><creatorcontrib>Abdulmajeed, Inaam M. ; Mahdi, Dunia Kamel ; Ibraheem, Suha H. ; Al-Karam, Logean Qadri ; Abbas, Muna M. ; Omran, Tarik T. Al ; Wasfi, Ahmed S. ; Majeed, Sadeer M. ; Ahmed, Duha S.</creatorcontrib><description>This work concerned on nanocrystalline NiAl2O4 and ZnAl2O4 having spinel structure prepared by Sol–gel technique. The structural and characterization properties for the obtained samples were examined using different measurements such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), finally, Field emission scanning electron microscope (FESEM). The Spinel-type for two prepared compound (NiAl2O4) and (ZnAl2O4) at different calcination temperature examined by XRD. Williamson-Hall Methods used to estimate crystallite size, Average distribution crystallite size of two compound were, 34.2 nm for NiAl2O4 and32.6 for ZnAl2O4, the increase in crystallite size affecting by increasing in calcination temperature for both compounds.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/5.0066247</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><publisher>Melville: American Institute of Physics</publisher><subject>Crystallites ; Field emission microscopy ; Field emission spectroscopy ; Fourier transforms ; Roasting ; Sol-gel processes ; Spinel ; Structural analysis ; X-ray diffraction</subject><ispartof>AIP conference proceedings, 2021, Vol.2372 (1)</ispartof><rights>Author(s)</rights><rights>2021 Author(s). 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Williamson-Hall Methods used to estimate crystallite size, Average distribution crystallite size of two compound were, 34.2 nm for NiAl2O4 and32.6 for ZnAl2O4, the increase in crystallite size affecting by increasing in calcination temperature for both compounds.</description><subject>Crystallites</subject><subject>Field emission microscopy</subject><subject>Field emission spectroscopy</subject><subject>Fourier transforms</subject><subject>Roasting</subject><subject>Sol-gel processes</subject><subject>Spinel</subject><subject>Structural analysis</subject><subject>X-ray diffraction</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2021</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp90EtLxDAUBeAgCo6jC_9BwJ3Q8aZ5NFnK4AsGXPjAXUiT1MnYaWuaCjO_3uoMuHN1Nx_3cA5C5wRmBAS94jMAIXJWHKAJ4ZxkhSDiEE0AFMtyRt-O0UnfrwByVRRygl6fUhxsGqKpsV2aaGzyMWxNCm2D2wo3wX74GpvG4W1oLDb1sA6NSR530XcmeofLDe7bOnsfWfJ22YTPwZ-io8rUvT_b3yl6ub15nt9ni8e7h_n1IutyoEXGJFjGuWOUl6VTVPHS5BJUpTxRUghSEuaKKneSWOeolAQYsFKaUnrhLaFTdLH728V2jO2TXrVDbMZInXNVcKmIglFd7lRvQ_qtprsY1iZuNAH9s5vmer_bf_irjX9Qd66i31cQblY</recordid><startdate>20211111</startdate><enddate>20211111</enddate><creator>Abdulmajeed, Inaam M.</creator><creator>Mahdi, Dunia Kamel</creator><creator>Ibraheem, Suha H.</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20211111</creationdate><title>Structural characterization of nickel and zinc aluminate prepared by sol-gel technique</title><author>Abdulmajeed, Inaam M. ; Mahdi, Dunia Kamel ; Ibraheem, Suha H.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p2037-480c455d435bbd9395ba2809f9e198661b14d7f2d81cdd38810404b8ab8e6ec13</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Crystallites</topic><topic>Field emission microscopy</topic><topic>Field emission spectroscopy</topic><topic>Fourier transforms</topic><topic>Roasting</topic><topic>Sol-gel processes</topic><topic>Spinel</topic><topic>Structural analysis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Abdulmajeed, Inaam M.</creatorcontrib><creatorcontrib>Mahdi, Dunia Kamel</creatorcontrib><creatorcontrib>Ibraheem, Suha H.</creatorcontrib><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Abdulmajeed, Inaam M.</au><au>Mahdi, Dunia Kamel</au><au>Ibraheem, Suha H.</au><au>Al-Karam, Logean Qadri</au><au>Abbas, Muna M.</au><au>Omran, Tarik T. Al</au><au>Wasfi, Ahmed S.</au><au>Majeed, Sadeer M.</au><au>Ahmed, Duha S.</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Structural characterization of nickel and zinc aluminate prepared by sol-gel technique</atitle><btitle>AIP conference proceedings</btitle><date>2021-11-11</date><risdate>2021</risdate><volume>2372</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>This work concerned on nanocrystalline NiAl2O4 and ZnAl2O4 having spinel structure prepared by Sol–gel technique. The structural and characterization properties for the obtained samples were examined using different measurements such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), finally, Field emission scanning electron microscope (FESEM). The Spinel-type for two prepared compound (NiAl2O4) and (ZnAl2O4) at different calcination temperature examined by XRD. Williamson-Hall Methods used to estimate crystallite size, Average distribution crystallite size of two compound were, 34.2 nm for NiAl2O4 and32.6 for ZnAl2O4, the increase in crystallite size affecting by increasing in calcination temperature for both compounds.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/5.0066247</doi><tpages>6</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | AIP conference proceedings, 2021, Vol.2372 (1) |
| issn | 0094-243X 1551-7616 |
| language | eng |
| recordid | cdi_proquest_journals_2597589190 |
| source | AIP Journals Complete |
| subjects | Crystallites Field emission microscopy Field emission spectroscopy Fourier transforms Roasting Sol-gel processes Spinel Structural analysis X-ray diffraction |
| title | Structural characterization of nickel and zinc aluminate prepared by sol-gel technique |
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